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HomeMy WebLinkAboutContract 36477- - CONT Between CITY OF FORT WORTH and CITY SECRETARY 1./ ,JI 17n CONTRACT NO.~----/ ACCUTEST LABORATORIES GULF COAST, INC. For ENVIRONMENTAL LADORA TORY ANALYSIS SERVICES Environmental Management Department November 2007 ~. , ' City of Fort Worth, Texas Mayor and Council Communication COUNCIL ACTION: Approved on 11/27/2007 DATE: Tuesday, November 27 , 2007 LOG NAME: 52ACCUTEST REFERENCE NO.: **C-22540 SUBJECT: Authorize Execution of a Professional Services Contract with Accutest Laboratories Gulf Coast for Laboratory Analytical Services RECOMMENDATION: It is recommended that the City Council authorize the City Manager to execute a professional service contract with Accutest Laboratories Gulf Coast for laboratory analytical serv ices . DISCUSSION: The Department of Environmental Management (DEM) requires a professional services contract for the furnishing of all labor, materials and equipment necessary for performing environmental laboratory analyses of air, soil , water and asbestos samples to be taken on various projects and inspections . The cost for the laboratory analytical services will not exceed $100 ,000 per year. The proposed agreement will commence November 1, 2007 , and expire October 31 , 2008, with two one-year options to renew . Renewal may be effected by written notification by the City Manager or his designated representative to the contractor within 30 days of the expiration of the prior term and does not require specific City Council approval , provided the City Council has appropriated sufficient funds to satisfy the City's obligations during the renewal term. DEM requested proposals for environmental laboratory analysis on July 27 , 2007 . Proposal packages were received on September 6, 2007 , from the following firms: Accutest Laboratories Gulf Coast Armstrong Forensic laboratory , Inc . Pace Analytical Services TestAmerica Inc. TraceAnalysis, Inc . The proposals were evaluated based on a pre-determined combination of qualitative and quantitative (bid point) measures and a determination was made of the top five laboratories submitting proposals . These measures included the evaluation of such factors as experience , qualifications of personnel, testing capabilities, cost and subcontractors . The top laboratory was then audited . Based on the total point distribution of the measures and the lab audit results , staff is recommending the contract be awarded to Accutest Laboratories Gulf Coast. Accutest Laboratories Gulf Coast, is in compliance with the City's M/WBE Ordinance by committing to 1 o percent M/WBE participation. The City's goal for this project is 1 O percent. FISCAL INFORMATION/CERTIFICATION: Logname: 52ACCUTEST Page 1 of 2 The Finance Director certifies that funds are available in the current operating budget , as appropriated , of the Env i ronmental Management Fund . TO Fund/Account/Centers Submitted for Cit~ Manager's Office by...;. Originating Degartment Head: Additional Information Contact: Logname : 52ACCUTEST FROM Fund/Account/Centers R103 53 1060 0524106 Libby Watson (6183) Brian Boerner (664 7) Michael Gange (6569) $100 ,000 .00 Page 2 of2 STATE OF TEXAS § § COUNTIES OF TARRANT, DENTON § AND WISE § CONTRACT FOR ENVIRONMENTAL LABO RA TORY ANALYSIS SERVICES WITH ACCUTEST LABORATORIES GULF COAST, INC. This Contract is entered into by and between the City of Fort Worth, Texas a home-rule municipal corporation situated in Tarrant, Denton and Wise Counties , Texas , hereinafter called "City," acting herein through Libby Watson, its duly authorized Assistant City Manager, and Accutest Laboratories Gulf Coast, Inc., hereinafter called "Contractor," by and through HARR.'Y BEHZA DI , its duly authorized PresidentNice President. In consideration of the mutual promises and benefits of this Contract, the City and Contractor agree as follows: 1. TERM The initial term of this Contract shall be for a period of twelve (12) months , beginning November 1, 2007 and expiring October 31 , 2008. In addition to the initial term , City shall have the right to renew this Contract for up to two (2) consecutive one (1) year renewal terms. The City Council shall approve renewal of this Contract by the City Manager executing a renewal agreement and with the City Council appropriating funds. CRL 2. SCOPE OF CONTRACTOR'S SERVICES A. Contractor shall provide all labor, materials , and equipment necessary for performing laboratory analysis of air, soil , water, sludge, sediment, tissue , asbestos , and any other type of sample taken by City or by the Contractor at the request of the City . B. Contractor shall perform, in a good and professional manner, the services listed in this Contract, and those identified in the City 's Request for Proposal DEM 07-04 :LAB dated July 27 , 2007 and for the unit price as listed in the Contractor responds to City 's Request for Proposal. The Contractor's response is attached hereto as Exhibit "A " and incorporated into this Contract as if fully set forth herein. Any conflict between such documents and the main body of this Contract shall be governed by the terms of the Contract. La boratory Analytical Services Contract 12 06 .07v3 1 C . All samples shall be collected by City personnel unless otherwise directed and requested by the City . Contractor will provide all sample containers , preservatives , and returnable shipping containers , as well as delivery and pick- up of samples at no additional charge to the City. D . Contractor 's handling instructions and chain-of-custody protocols shall be in accordance with all Federal and State statutes , rules and regulations for laboratory methods and quality assurance . E. Contractor shall be responsible for the disposal of the samples and such disposal shall be in accordance with all Federal and State statutes , rules and regulations. F . Contractor shall provide each type of test and each type of test method specified in Exhibit "A ". If necessary , Contractor shall provide any alternate procedure or supporting laboratories required which is requested by the City is such request is reasonably available . G . Analytical results requested at a Standard Tum Around Time (TAT) must be returned to the city within seven (7) calendar days after receipt of sample(s). Analytical results requested at a Rush TAT must be returned to the city within three (3) calendar days after receipt of sample(s). Analytical results requested at an Emergency TAT must be returned to the city within twenty-four (24) hours after receipt of sample(s). H. Contractor agrees that it has and will maintain during the term of this Contract, current and appropriate Federal , State, and local licenses and permits to perform the services contained in this Contract. In addition, Contractor agrees to require any of its subcontractors used to perform this Contract to have and maintain current and appropriate Federal, State and local licenses and permits to perform this Contract. I. Contractor certifies that it has and will maintain, during the term of this Contract, the required insurance listed in Section 5 during the term of this Contract. 3 . SCOPE OF CITY SERVICES The City agrees to perform the following services : C RL A. Designate a City representative to provide timely direction to the Contractor and render City decisions. B . Coordinate with City facilities , City departments , and any tenants. La boratory An alytica l Se rvices Contract 12 .06 .07v3 2 4. COMPENSATION A. In consideration for the work performed by Contractor under this Contract, City shall pay Contractor a sum not to exceed one hundred thousand dollars ($100,000). Payment shall be based on the unit price charges contained in Exhibit A. Payments will be made within thirty (30) days of receiving a correct invoice from Contractor. The City is responsible for notifying Contractor of any questions concerning an invoice , and shall not be required to pay Contractor until such questions have been resolved. B. Payment shall be based on the unit price charges contained in exhibit A , however, if a service and its associated cost is not listed in exhibit A , the parties will attempt to negotiate a unit price for providingthat service. If the parties are unable to come to an agreement within fourteen (14) calendar days , the Contractor acknowledges and agrees that the City will obtain disposal services for the waste elsewhere. C. Periodically during the performance of this Contract, the Contractor's Project Manager shall inform the City 's representatives of his/her best estimate of the expenses incurred to that time. In the event that the estimate approximates the "not to exceed" price, Contractor shall prepare to cease its operations unless and until the Contract is amended and an authorized representative of the City directs Contractor to perform additional work. D. Contractor shall receive no compensation for delays or hindrances to the work, except when direct and unavoidable extra cost to Contractor was caused by City 's failure to provide information, if any, which it is required to do . When extra compensation is claimed, a written statement thereof shall be presented to the City. 5 . INSURANCE The Contractor certifies that it has , at a minimum, current insurance coverage as detailed below and will maintain it throughout the terms of this Contract. Prior to commencing work, Contractor shall deliver to the City certificates documenting this coverage. The City may elect to have the Contract submit its entire policy for inspection. CRL A. Commercial General Liability Insurance -$5 ,000 ,000 each occurrence. B. Professional Liability Insurance -$5 ,000 ,000 each claim. C . Automobile Liability Insurance - a) Coverage on vehicles involved in the work performed under this Pricing Agreement: La boratory Analyt ical Services Contract 12.06 .07v3 3 CRL + $1 ,000 ,000 per accident on a combined single limit basis or: + $500 ,000 Bodily injury/person + $1 ,000 ,000 Bodily injury/accident • $250 ,000 Property damage b) The named insured and employees of Pricing Agreement shall be covered under this policy. The City of Fort Worth shall be named an Additional insured, as its interests may appear. Liability for damage occurring while loading , unloading and transporting materials collected under the Pricing Agreement shall be included under this policy. D. Worker's Compensation - a) Statutory limits for Worker 's Compensation plus b) Employer 's liability at a minimum: + $1 ,000 ,000 each accident; + $1 ,000 ,000 disease -policy limit; and + $500 ,000 disease -each employee. E. Environmental Impairment Liability (EIL) and/or Pollution Liability - $2 ,000 ,000 per occurrence . EIL coverage(s) must be included in policies listed in items A and B above; or, such insurance shall be provided under separate policy(s). Liability for damage occurring while loading , unloading and transporting materials collected under the Pricing Agreement shall be included under the Automobile Liability insurance or other policy(s). F. The following shall pertain to all applicable policies of insurance listed above: 1. Additional Insured Clause: "The City of Fort Worth , its officers , agents , employees , and representatives are added as additional insureds as respects operations and activities of, or on behalf of the named insured , performed under Pricing Agreement with the City of Fort Worth." Exception ... the additional insured requirement does not appl y to Workers ' Compensation policies. 2. Subcontractors shall be covered under the Primary Laboratory 's insurance policies or they shall provide their own insurance coverage ; and , in the latter case , documentation of co verage shall be submitted to the Primary Laboratory prior to the commencement of work and the Primary Laboratory shall deliver such to the City. 3. Prior to commencing work under this Pricing Agreement , the Laboratory shall deliver to the City of Fort Worth in surance certificate(s) documenting the insurance required and terms and clauses required. Laboratory Analyt ical Services Contract 12.06 .07v3 4 CRL 4. Each insurance policy required by this Pricing Agreement shall contain the following clauses: "This insurance shall not be canceled, limited in scope or coverage, or non-renewed until after thirty (30) Days prior written notice has been given to the Director of Environmental Management, City of Fort Worth, 1000 Throckmorton, Fort Worth , Texas 76102." 5. The insurers for all policies must be licensed/approved to do business in the State of Texas. Except for workers ' compensation, all insurers must have a minimum rating of A: VII in the current A. M. Best Key Rating Guide or have reasonably equivalent financial strength and solvency to the satisfaction of Risk Management. If the rating is below that required , written approval of Risk Management is required. 6 . The deductible or self-insured retention (SIR) affecting the coverage required shall be acceptable to and approved in writing by the Risk Manager of the City of Fort Worth in regards to asset value and stockholders equity. In lieu of traditional insurance, alternative coverage maintained through insurance pools or risk retention groups must be also approved by the City 's Risk Manager. 7. Waiver of rights of recovery (subrogation) in favor of the City of Fort Worth. 8. Such insurance policies shall be primary, without right of contribution and not subject to any offset by any other insurance carried by the City. 9. If insurance policies are not written for specified coverage limits , Umbrella or Excess Liability insurance for any differences is required. Excess Liability shall follow form of the primary coverage . 10. Unless otherwise stated, all required insurance shall be written on the "occurrence basis"". If coverage is underwritten on a claims-made basis, the retroactive date shall be coincident with or prior to the date of the Pricing Agreement and the certificate of insurance shall state that the coverage is claims-made and the retroactive date. The insurance coverage shall be maintained for the duration of the Pricing Agreement and for five (5) years following completion of the service provided under the Pricing Agreement or for the warranty period , whichever is longer. An annual certificate of insurance submitted to the City shall evidence such insurance coverage . 11. City, at its sole discretion, reserves the right to review the insurance requirements and to make reasonable adjustments to insurance coverage 's and their limits when deemed necessary and prudent by the City based upon changes in statutory law, court decision or the claims history of the industry as well as of the Laboratory to the City of Fort Worth. In the event the City requires the La boratory Analytical Serv ic es Contract 12 .06 .07v3 5 insurance limits to be increased or changes in policy categories or types of coverage , the City shall provide written notice to the Laboratory party . The Laboratory party will have ninety days from the date of notice to compl y with the additional requirements . 6 . INDEMNIFICATION A . For the purposes of this Contract, the following words and phrases shall be defined as follows: CRL 1. Environmental Damages shall mean all claims , judgments, damages , losses , penalties , fines , liabilities (including strict liability), encumbrances , liens , costs , and expenses of investigation and defense of any claim , whether or not such claim is ultimatel y defeated , and of any good faith settlement of judgment, of whatever kind or nature , contingent or otherwise , matured or unmatured, foreseeable or unforeseeable , including but without limitation reasonable attorney's fees and disbursements and consultant's fees , any of which are incurred as a result of the existence of a violation of Environmental Requirements pertaining to the services performed under this Contract, and including without limitation: a. Damages for personal injury and death , or injury to property or natural resources; b. Fees incurred for the services of attorneys , consultants, Contractors , experts , laboratories and investigation or remediation resulting from any violation of Environmental Requirements including, but not limited to , the preparation of any feasibility studies or reports of the performance of any cleanup , remediation , removal , response , abatement, containment, closure , restoration or monitoring work required by any Federal , State or local governmental agency or political subdivision, or otherwise expended in connection with the existence of such monitoring wells or violations or Environmental Requirements , and including without limitation any attorney's fees , costs and expenses incurred in enforcing this Contract or collecting any sums due hereunder ; and c. Liability to any third person or governmental agenc y to indemnify such person or agency for costs expended in connection with the items referenced in subparagraph (b) herein. 2. Environmental Requirements shall mean all applicable statutes , regulations , rules , plans, authorizations , concessions, franchises , and similar items , as they are now or as they may later be amended , of all governmental agencies , departments , commissions , boards , bureaus , or instrumentalities of the United States, states , and political subdivisions thereof and all applicable judicial , administrative , and regulatory decrees , judgments, and orders relating to the protection of human health or the environment, including without limitation : La boratory Analyt ical Serv ices Contract 12 .06 07v3 6 B . C. D. CRL a. All requirements, including, but not limited to , those pertammg to reporting , licensing , emissions, discharges , releases , or threatened releases of hazardous materials , pollutants , contaminants or hazardous or toxic substances, materials , or wastes whether solid , liquid , or gaseous in nature , into the air, surface water, groundwater, storm water , or land , or relating to the manufacture , processing , distribution , use , treatment , storage , disposal , transport , or handling of pollutants , contaminants , or hazardous or toxic substances, materials , or wastes, whether solid, liquid , or gaseous in nature; and b. All requirements pertaining to the protection of the health and safety of employees or the public . Professional Services Indemnification. CONTRACTOR SHALL RELEASE, INDEMNIFY, REIMBURSE, DEFEND, AND HOLD HARMLESS, CITY, ITS OFFICERS, AGENTS, SERVANTS AND EMPLOYEES, FROM AND AGAINST ANY AND ALL CLAIMS OR SUITS FOR PROPERTY DAMAGE OR LOSS AND/OR PERSONAL INJURY, INCLUDING DEATH, TO ANY AND ALL PERSONS, ARISING OUT OF THE WORK AND SERVICES TO BE PERFORMED HEREUNDER BY CONTRACTOR, ITS OFFICERS, AGENTS, EMPLOYEES, CONTRACTORS, SUBCONTRACTORS, LICENSEES, OR INVITEES, INCLUDING DAMAGES, LOSS, INJURY OR DEATH TO THE EXTENT CAUSED BY ANY NEGLIGENT ERROR, OMISSION, DEFECT, OR DEFICIENCY IN THE PERFORMANCE OF CONTRACTOR'S SERVICES OR IN THE PREPARATION OF ENVIRONMENTAL CONSULTANT SERVICES DOCUMENTS IN ACCORDANCE WITH THIS CONTRACT. General Indemnification. CONTRACTOR DOES HEREBY RELEASE, INDEMNIFY, REIMBURSE, DEFEND, AND HOLD HARMLESS THE CITY, ITS OFFICERS, AGENTS, SERVANTS, AND EMPLOYEES FROM AND AGAINST ANY AND ALL LIABILITY, CLAIMS, SUITS, DEMANDS, OR CAUSES OF ACTION WHICH MAY ARISE DUE TO ANY LOSS OR DAMAGE TO PERSONAL PROPERTY, OR PERSONAL INJURY, AND/OR DEATH OCCURRING AS A CONSEQUENCE OF THE PERFORMANCE OF THIS CONTRACT, WHEN SUCH INJURIES, DEATH, OR DAMAGES ARE CAUSED BY THE NEGLIGENCE OF CONTRACTOR, ITS OFFICERS, AGENTS, OR EMPLOYEES, OR SUBCONTRACTORS, OR THE JOINT NEGLIGENCE OF CONTRACTOR, ITS AGENTS, OR EMPLOYEES, OR SUBCONTRACTORS, AND ANY OTHER PERSON OR ENTITY, EXCLUDING ALL PARTIES INDEMNIFIED HEREUNDER. Environmental Indemnification. CONTRACTOR DOES HEREBY RELEASE, INDEMNIFY, REIMBURSE, DEFEND, AND HOLD HARMLESS THE CITY, ITS OFFICERS, AGENTS, SERVANTS, AND EMPLOYEES FROM Laboratory Analytical Services Co ntract 12 .06 .07v3 7 AND AGAINST ANY AND ALL ENVIRONMENTAL DAMAGES AND THE VIOLATION OF ANY AND ALL ENVIRONMENTAL REQUIREMENTS RESULTING FROM THE HANDLING, COLLECTION, TRANSPORTATION, STORAGE, DISPOSAL, TREATMENT, RECOVERY, AND/OR REUSE, BY ANY PERSON, OF THE MATERIAL UNDER THIS CONTRACT, TO THE EXTENT SAID ENVIRONMENTAL DAMAGES OR THE VIOLATION OF SAID ENVIRONMENTAL REQUIREMENTS WERE THE RESULT OF ANY ACT OR OMISSION OF CONTRACTOR, ITS OFFICERS, AGENTS, EMPLOYEES, OR SUBCONTRACTORS, OR THE JOINT ACT OR OMISSION OF CONTRACTOR, ITS OFFICERS, AGENTS, EMPLOYEES, OR SUBCONTRACTORS AND ANY OTHER PERSON OR ENTITY EXCLUDING ALL PARTIES INDEMNIFIED HEREUNDER. E . The obligations of the Contractor under this section shall include , but not be limited to , the burden and expense of defending all claims , suits , and administrative proceedings (with counsel reasonably approved by the indemnified parties ), even if such claims , suits or proceedings are groundless , false , or fraudulent , and in conducting all negotiations of any description , and paying and discharging , when and as the same become due , any and all judgments, penalties or other sums due against such indemnified persons. F . Upon learning of a claim , lawsuit , or other liability which Contractor is required hereunder to indemnify, the City shall provide Contractor with reasonably timely notice of same. G. The obligations of the Contractor under this section shall survive the expiration of this Contract and the discharge of all other obligations owed by the parties to each other hereunder. H . In all of its Contracts with subcontractors for the performance of any work under this Contract, Contractor shall require the subcontractors to indemnify the City in a manner consistent with this section. I. In the event that a written claim for damages against Contractor or any of its subcontractors remains unsettled at the time all work on the project has been completed to the satisfaction of the City Manager, as evidenced by a final inspection , final payment to Contractor shall not be recommended by the City Manager for a period of thirty (30) days after the date of such final inspection, unless the Contractor submits written evidence satisfactory to the City Manager that the claim has been settled and a release has been obtained from the claimant involved . CRL 1. If the claim concerned remains unsettled at the expiration of the said thirty-day period, the Contractor may be deemed by the City Manager to be entitled to a semi-final payment for work completed , such semi-final payment to be in an amount equal to the total dollar amount then due less La boratory An a lytical Services Contract 12 .06 .07v3 8 the dollar value of any written claims pending against the Contractor arising out of the performance of such work. 2 . The City Manager shall not recommend final payment to Contractor if a claim for damages is outstanding for a period of six (6) months following the date of the acceptance of the work performed unless the Contractor submits evidence in writing , satisfactory to the City Manager, that: 1. The claim has been settled and a release has been obtained from the claimant involved; or 11. Good faith efforts have been made to settle such outstanding claims, and such good faith efforts have failed . 3. If condition (i) above is met at any time within the six (6) month period, the City Manager shall recommend that the final payment to Contractor be made . If condition (ii) above is met at any time within the six (6) month period, the City Manager may recommend that final payment to Contractor be made . At the expiration of the six ( 6) month period, the City Manager may recommend that final payment be made if all other work has been performed and all other obligations of the Contractor have been met to the satisfaction of the City Manager. 7. WARRANTY Contractor warrants that it understands the currently known hazards and suspected hazards which are presented to persons, property and the environment by providing the laboratory service as referred to in the Contractor 's Scope of Services. Contractor further warrants that it will perform all services under this Contract in a safe , efficient and lawful manner using industry accepted practices , and in full compliance with all applicable State and Federal laws governing its activities and is under no restraint or order which would prohibit performance of services under this Contract. 8. LICENSES, PERMITS AND FEES Contractor agrees to obtain, pay for , and maintain all licenses, permits , certificates , inspections and all other approvals and fees required by law or otherwise necessary to perform the services prescribed hereunder. C R L La boratory An al yt ical Servi ces Contract 12.06 .07v3 9 9. DEFAULT A. Contractor shall not be deemed to be in default because of any failure to perform under this Contract, if the failure arises from causes beyond the control and without the fault or negligence of Contractor. Such causes shall include acts of God, acts of the public enemy, acts of Government, in either its sovereign or contractual capacity , fires , flood , epidemics , quarantine restrictions , strikes , freight embargoes , and unusually severe weather for the geographic area. B. If the failure to perform is caused by the failure of a subcontractor of Contractor 's to perform, and if such failure was beyond the control of both the Contractor and the subcontractor, without their fault or negligence, Contractor shall not be deemed to be in default unless the subcontracted supplies or services were reasonably obtainable from other sources. C . If Contractor fails to begin work herein provided for within the time specified above , or to complete such work within the time specified above , within the true meaning of this Contract, City shall have the right to take charge of and complete the work in such a manner as it may deem appropriate. If City exceeds the costs detailed in the attached documents , City may deliver to Contractor a written itemized statement of the total excess costs, and Contractor shall reimburse City for such excess costs without delay . D. Alternatively, if at any time during the term of this Contract the work of Contractor fails to meet the specifications of the Contract documents , City may notify Contractor of the deficiency in writing . Failure of Contractor to correct such deficiency and complete the work required under this Contract to the satisfaction of City within ten ( 10) days after written notification shall result in termination of this Contract. All costs and attorneys fees incurred by City in the enforcement of any provision of this Contract shall be paid by Contractor. E. The remedies provided for herein are in addition to any other remedies available to City elsewhere in this Contract or by Federal , State or local laws or regulations . 10 . TERMINATION A. City may terminate this Contract with or without cause upon thirty (30) days prior written notice to the Contractor, provided that such termination shall be without prejudice to any other remedy the parties may have. In the event of termination, any work in progress will continue to completion unless specified otherwise in the notice of termination . The City shall pay for any such work in progress , and reasonable closure costs , that is completed by Contractor and accepted by the City. CRL La boratory Analyti cal Servi ces Contract 12 .06 .07v3 10 B. If the City terminates this Contract under paragraph A above , City shall pay Contractor for all services performed prior to the termination notice. C. All completed or partially completed original documents prepared under this Contract shall become the property of the City w hen the Contract is terminated , and may be used by the City in any manner it desires ; provided, however, that the Contractor shall not be liable for the use of such documents for any purpose other than as described when requested. D. In the event either party defaults in the performance of any of its obligations under this Contract, misrepresent s to the other a material fact , or fails to notify the other party of any material fact which would affect the party 's performance of its obligations hereunder, the non-defaulting party shall have the right to terminate this Contract upon gi ving the defaulting party written notice describing the breach or omission in reasonable detail. The defaulting party shall have a thirty (30) day period commencing upon the date of notice of default in which to effect a cure . If the defaulting party fails to effect a cure within the aforesaid thirty (30) day period, or if the default cannot be cured, the Contract shall terminate as of the date provided in the notice of default. E . The remedies prov ided for herein are in addition to any other remedies available to City elsewhere in this Contract or by law. 11. INDEPENDENT CONTRACTOR The City agrees to hire Contractor as an independent Contractor, and not as an officer, servant, or employee of the City. Contractor shall have the exclusive right to control the details of the work performed hereunder, and all persons performing same , and shall be solely responsible for the negligent acts and omissions of its officers , agents , employees , and subcontractors. Nothing herewith shall be construed as creating a partnership or joint venture between the City and Contractor, its officers , agents , employees, and subcontractors ; and the doctrine of respondent superior has no application as between the City and Contractor. 12 . MINORITY AND WOMEN BUSINESS ENTERPRISES In keeping with the City 's Minority/Women Business Enterprise (MWBE) ordinance, Contractor agrees a minimum of ten percent (10%) of the total dollar value of this Contract will be paid as compensation to certified M/WBE firms . Monthly reporting is required to the City of Fort Worth -M/WBE Office, 1000 Throckmorton Street, Fort Worth, Texas 76102. Proof of payment for all invoices from M/WBE firms will be required . Final payment to the Contractor under this Contract may be withheld pending M/WBE Office approval of documentation. CRL La boratory Analyt ical Serv ices Co ntract 12.06 .07v3 11 13. MODIFICATION No modification of this Contract shall be binding on Contractor or the City unless set out in writing and signed by both parties. Modifications shall be in the same format as the final specification showing the change or addition of a task, project schedule, deliverable document(s), and schedule of payments. 14. RIGHT TO AUDIT City and Contractor agree that, until the expiration of three (3) years after the final payment under this Contract, the City shall have access to and the right to examine any reasonably pertinent books, documents, papers and records of the Contractor involving transactions relating to this Contract. Contractor further agrees to include in all its subcontracts hereunder a provision to the effect that the subcontractor agrees that the City shall , until the expiration of three (3) years after final payment under the subcontract, have access to papers and records of such subcontractor involving transactions relating to the subcontract. The term "subcontract" as used herein includes purchase orders. 15 . NON-DISCRIMINATION A. During the performance of this Contract, Contractor agrees not to discriminate against any employee or applicant for employment because of race , religion, color, sex or national origin, except where religion, sex or national origin is a bona fide occupational qualification reasonably necessary to the normal operation of the Contractor. Contractor agrees to post in conspicuous places, available to employees and applicants for employment, notices setting forth the provisions of the non- discrimination clause. B. Contractor also agrees that in all solicitations or advertisements for employees placed by or on behalf of this Contract, that Contractor is an equal opportunity employer. C . Notices, advertisements, and solicitations placed in accordance with federal law, rule or regulation shall be deemed sufficient for the purpose of meeting the requirements of this section. 16 . GOVERNING LAW The City and Contractor agree that the validity and construction of this Contract shall be governed by the laws of the State of Texas, except where preempted by federal law. C RL La boratory Analyt ical Servi ces Contra ct 12.06 .07v3 12 17. SEVERABILITY The provisions of this Contract are severable ; and if for any reason any one or more of the provisions contained herein are held to be invalid , illegal or unenforceable in any respect, the invalidity, illegality or unenforceability shall not affect any other provision of this Contract, and this Contract shall remain in effect and be construed as if the invalid , illegal or unenforceable provision had never been contained in the Contract. 18. RIGHTS AND REMEDIES NOT WAIVED In no event shall the making by the City of any payment to Contractor constitute or be construed as a waiver by the City of any breach of covenant, or any default which may then exist, on the part of Contractor, and the making of any such payment by the City while any such breach or default exists shall in no way impair or prejudice any right or remedy available to the City with respect to such breach or default. Any waiver by either party of any provision or condition of the Contract shall not be construed or decreed to be a waiver of any other provision or condition of this Contract, nor a waiver of a subsequent breach of the same provision or condition, unless such waiver be expressed in writing by the party to be bound. 19. VENUE Venue of any suit or cause of action under this Contract shall lie in Tarrant County, Texas . 20. NOTICES Any notices , bills, invoices or reports required by this Contract shall be sufficient if sent by the parties in the United States mail, postage paid, to the address noted below: If to the City: If to the Contractor: CRL Lab oratory Analyti cal Services Contract 12 .06.07 v3 Michael Gange Department of Environmental Management City of Fort Worth 1000 Throckmorton Fort Worth, Texas 76102-6311 Gregory Grandits 10165 Harwin Dr. Houston, Texas 77036 13 21. ENTIRETY This Contract the Contract documents and any other documents incorporated by reference herein contain all the terms and conditions agreed to by the City and Contractor, and no other Contracts, oral or otherwise , regarding the subject matter of this Contract or any part thereof shall have any validity or bind any of the parties hereto. 22. ASSIGNMENT The City and Contractor bind themselves and any successors and assigns to this Contract. Contractor shall not assign, sublet, or transfer its interest in this Contract without written consent of the City. Nothing herein shall be construed as creating any personal liability on the part of any officer or agent of the City, nor shall it be construed as giving any rights or benefits hereunder to anyone other than the City and Contractor. IN WITNESS THEREOF, on this date of 3 ), ])~ , 200 f the City of Fort Worth and Contractor have executed this Contract in triplicate in Tarrant County, Texas. CITY OF FORT WORTH Libby atson Assistant City Manager ATTEST: ~~~ City Secretary APPROVED AS TO FORM AND LEGALITY: Assistant City Attorney CRL La boratory Analyt ical Services Contrac t 12.06 .07v3 ACCUTEST LABO RA TORIES GULF COAST, INC. tfµ~ WITNE SS : CORPORATE SEAL: coatract Author i ~io• , \-aJ-ul Date 14 CONTRACTOR COMPLIANCE WITH WORKERS' COMPENSATION LAW Pursuant to V.T.C .A. Labor Code §406 .96 (2000), as amended , Contractor certifies that it provides workers' compensation insurance coverage for all of its employees employed on City of Fort Worth Department · of Environmental Management Project: DEM 07-04: Environmental Laboratory Analysis Services .. CONTRACTOR Accutest Laboratories Gulf Coast, Inc. By: ;-/11 /2/</ 13G fl);(/-/)/ Title V· f· o/Juqfy'tJv-[? Date (2 f !;( (t1] STATE OF =FEXAS 1-)tYL<..j ,u § COUNTY OF +ARRAN, 6L1e ~ Before me, the undersigned authority , on this day personally appeared ,..1..:.~-=k......A,.;=~:;;;;a..Li.,=·~-· known to me to be the person whose name is subscribed to the i g instrument , and acknowledged to me that he executed the same as the act and dee of for the purposes and consideration therein expressed and in the capacity therein stated . Given Under My Hand and Seal of Office this J / 5 'd ay of i~ . , 20 (5 7 ....------·-·---.....---... ,,,,~~::t,,,, NANCY J . COUGHLIN /.,m~ ~,i\ Notary Public · State of Florida ! , * • §My Commission Expires Jan 6, 2010 \~ ="~i Commission # 00497896 ,,i OF f\.V",,' • ,,,.,,.,,, Bonded By National Notary Assn. :c:Z: 1-0 o:::.u5 o - a!:~ w .,_o >o:::(.!:) w o z ut.L..cn Wt.L..4: a::::o :c >-·c.> 1-CX: 0~ I ' ,, >-,· . • ' , , I.• i PROPOSAL PACKAGE CITY OF FORT WORTH ENVIRONMENTAL MANAGEMENT DEPARTMENT 1000 THROCKMORTON 0 0 6 <( -D I 0.. L.&.J V> ,..... C=> c:::, ...... _, FORT WORTH , TEXAS 76102 FORTWO PROJECT: DEM 07-04: LAB PROFESSIONAL SERVICES CONTRACT FOR ENVIRONMENTAL LABORATORY ANALYSIS July 27, 2007 /7ccv rc--t-r ~/l/Jo/efl10R1L"--S ~Ell z/101 Company Name • /tJ/o5 /.,//9/?W//V £)/<_, Address /-/OU 5 ro;.J ,-x 770 $l, P si enWice Pres ident -Signature JI 3 -t7? /-'f ?a.7' CJ /5/07 0 ------------Telephone Date J / J,. d1 I -'/?'?D Fax Laboralories Table of Contents 2.1 Proposal Document Checklist 2.2 Acknowledgement Request For Proposal Addenda 2.3 Minority & Women Business Enterprises 2.4 Proposal Summary 2.5 Cost Estimate 2.6 Provider's Company Experience 2. 7 Provider's Personnel Qualifications & Experience 2.8 Organizational Chart 2.9 Providers License and Certificates 2.10 Subcontractor Information and Qualifications 2.11 Statement of Residency 2.12 Nondiscrimination 2.13 Prevailing Wage Rates 2.14 Insurance Certificates 2.15 Contractor Legal and Compliance History 2.16 Lab Quality Control and Quality Assurance 2.17 Document Control 2.18 Financial Statement 2.19 Other 2 .1 PROPOSAL DOCUMENT CHECKLIST All Proposal Documents , including this Checklist , should be completed in full and submitted in a sealed envelope, in the requested order, to be considered as a responsive submittal. Proposal Documents Initial if Included 2.1 PROPOSAL DOCUMENT CHECKLIST p .7./7. 2.2 ACKNOWLEDGE REQUEST FOR PROPOSAL ADDENDA -fiJl=_ 2.3 MINORITY & WOMEN BUSINESS ENTERPRISES . 2.4 PROPOSAL SUMMARY J7· T.Y7· 2 .5 COST ESTIMATE p. r.P- 2.6 PROVIDER 'S COMPANY EXPERIENCE i?-r.;J· ' 2.7 PROVIDER 'S PERSONNEL QUALIFICATIONS & EXPERIENCE F · T,;l· 2.8 ORGANIZATIONAL CHART .fl-1f7, 2.9 PROVIDERS LICENSE AND CERTIFICATES ·() .1?f7· 2.10 SUBCONTRACTOR INFORMATION AND QUALIFICATIONS /!· r.r-7 · 2.11 STATEMENT OF RESIDENCY f?. --r.17- ' 'f). r:17· 2.12 NONDESCRIMINATION ) 2.13 PREVAILING WAGE RATES /V/7 2 .1 4 INSURANCE CERTIFICATES /7 · 1-r?. 2.15 CONTRACTOR LEGAL AND COMPLIANCE HISTORY 1'7· r:77- 2.16 LAB QUALITY CONTROL AND QUALITY ASSURANCE p .-r.J? I 2 .1 7 DOCUMENT CONTROL p ,.,-:-(1, 2.18 FINANCIAL STATEMENT ?· r.<7- 2 .19 OTHER p.T.77 I understand that all of these items will be reviewed, and any items not included may result in my Submittal being considered non-responsive. Name: Gl<-c/ftJfi)/ r (5/f/J,UO /T; ----~--------- T itle : ,6' V 5 / M ~ .J J ,OF'l/. ,#ft?/f..//l6E/< Company: ,ACC v-r.,E:'§/ A/16o;e/) TO~ /CJ 2-2 2.2 ACKNOWLEDGEMENT OF RECEIPT OF REQUEST FOR PROPOSAL ADDENDUM 2.2 .1 Check if applicable / The undersigned acknowledges the receipt of the following addendum(a) to the Request for Proposals , and has attached all addenda following this page. (Add lines if necessary). Addendum Number 1 9/r/01 (Date received) Addendum Number 2 ---------- (Date received) Addendum Number 3 ---------- (Date received) 2.2.2 Check if applicable __ The undersigned acknowledges the receipt of no addenda to the Request for Proposals . PROVIDER: /9C'Ct/ Tt:FT L/J/57<>£/JTo~/l:J Company Name . /o/C5 ;1/lt'f. WIN IJ/f .f"I/IT~ /Sfl Address 11ovsrow IX 7 ?DJ& City , State , Zip 0 BY : Gfi£60flY T G/?/INOJT.S (print or type name of signatory) ~T.~ (Signature) ;Jt/5J/JE5S /.).£ J/. /lJ/INlr 6 E-~ Title (print or type) 2·3 FI\V IRO I\MENTAL MANAGEMENT ADDENDUM#! TO: Interested Bidders FROM: Derek Senter Environmental Management Department DATE: August 30 , 2007 RE: Addendum # I to Reference No. DEM07-04 :LAB General Comments: • Bids are due on Thursday, September 6 , 2007 by I :30 p .m. at the City of Fort Worth Purchasing Division , I 000 Throckmorton , Fort Worth , Texas 76102 . ONE (I) original cop y of the Request for Proposal (RFP) and three (3) complete bound copi es M U ST be submitted to be considered RESPONSIVE. Questions and Responses: ltem #J: Item #2: Please disregard section 2.13 including Table 03. This section is not applicable to thi s contract. Please replac e Section 2 .11 with the following page. HUB SUBCONTRACTING PLAN HISTORICALLY UNDERUTILIZED BUSINESS LETTER OF INTENT Accutest Laboratories acknowledges if chosen as a analytical provider it's responsibility under this contract to utilize Minority and Woman Business Enterprises (M/WBE) with a minimum 10% goal of the revenue received . Accutest Laboratories has teamed with Xenco Laboratories who will be a subcontractor for Accutest Laboratories under this contract to meet our M/WBE goals. Subcontractor Information: Name of Subcontractor/Supplier: Xenco. Address: 11381 Meadow Lane, Suite L -Houston, TX -77092-2647 Phone: 281-589-0692 Is the subcontractor a ce1iified HUB? Contact: Kelly Steinberg, kelly.steinberg @ xenco.com If yes , enter the Certificate number: HMMB33717Y0308 -~X~_Yes Expected dollar amount of contract with subcontractor/supplier: $10,000.00 Percentage amount of contract with subcontractor/supplier: % lQ No Description of materials/services performed under agreement with the subcontractor for amount indicated above: Xenco Laboratories, Inc. will serve as a subcontractor for Accutest Laboratories as a back-up laboratory for overflow work and analytical parameters that our of Accutest Laboratories' normal scope of services On a monthly basis Accutest Laboratories will assess the workload received from this contract and target future projects for the following month to be subcontracted based on the subcontract goal intended for this contract. Accutest Laboratories will monitor our M/WBE plan monthly and make the necessary adjustments to our subcontract work to Xenco to assure we meet compliance. NCTRCA Minority Business Enterprise Certificati on Xenco Lab orato ri es , In c has filed with the Agency the appropriate Affidavit and is hereby certified to provide scrvice(s) in the following areas: Minority Business Enterprise 541380: Testing Laboratories ; 1,h. C t·fi . . l"d b i • March 2007 d d d . . I' t' 1s er 1 1catton is va 1 .. cg nnmg an s uperse c any registra ti on or 1s mg previously issued. This certification must be updated annually by submission of an Annual Update Affidavit At any time there is a charge in ownership or control of the firm, notification must be made immedia tely to the North Central Texas Regional Certification Agency. Certificate expiration _______ M_a_r_c_h ____ , 20~ Issued date March 20 07 -----------------' -- CERTfflCATION NO. HMMB33717Y0308 NCTRCA North Central Texas Regional Certification Agency March 09, 2007 Eduardo Builes Xenco Laboratories, Inc 11381 Meadowglen Lane, Suite L Houston TX 77082 RE: MBE Certification Affidavit No. 8092 Dear Mr . Builes: Congratulations! Your firm has been certified by the North Central Texas Regional Certification Agency ("Agency") as a: Minority Business Enterprise (MBE) in the following area(s): 541380; Testing Laboratories; Your Certification Identification Number is HMMB33717Y0308 . This number should be used on bids, requests for proposals and other correspondence with any entities regarding your MBE status. Moreover, you should provide your certification number to prospective bidders and proposers on any projects as evidence of your certification status as a MBE. Changes such as expansion of business services, ownership, phone number, etc. should be immediately communicated to us. Your certification is valid for one year, to remain certified, MBEs are required to update all pertinent information prior to the expiration of their certification. The Agency and any of our member entities reserve the right to re-evaluate a firm's certification status at anytime that they determine such re-evaluation is warranted. Thank you for your participation in the Agency's Disadvantaged, Minority and Woman- Owned Business Certification Program. Please contact me at metro (817) 640-0606 if you have any questions or if I can be of assistance to you. Very truly yours, tW~~ LaRhonda Hytchye Interim Agency Director 624 Six Flags Drive, Suite 216 , Arlington, TX 76011 • Metro (817) 640-0606 • Fax (817) 640-6315 • www .nctrca .org 2.4 PROPOSAL SUMMARY TO THE CITY OF FORT WORTH: The undersigned hereby proposes to furnish the equipment , labor materials , superintendence, and any other items or services necessary to perform laboratory analytical services for the City of Fort Worth which include , but are not limited to , the analysis of air , soil , water , sludge , sediment, tissue , mold , and asbestos samples . Corporate laboratory equipment and personnel are capable of performing each type of procedure listed in the Project Data either at this location or through subcontracts. All Proposal Documents have been submitted in one sealed envelope. Unit prices are provided within the Proposal Documents . This Proposal Summary and the accompanying Proposal Documents are intended to be complete and will remain valid for sixty (60) days from the date of submittal. PROVIDER: fl CCI/ T .t.:ST L/1/Jll/?I/ 70/?I-Ef (Company Name) /0/bS fl~A.JPI/V tJ~. rt11TE ISO (Address) r1ovf,0 N ) TX 77 D3t (City , State , Zip) 713-o( 7/-Y ?oo Phone) BY : C /(..t,=60/\Y T. GAJ/lAl(} I T.J (Print or type name of signa~/\ ~/.~ (Signature) /ft/f/N~.fI L)EI/.. /17,9/Jtcl6E~ Title (print or type) ? l:f-~ "7 /-'1'710 (FAX) . 2 .5 COST ESTIMATE The Table below identifies various types of analysis ; laboratories shall provide a cost per test for each type of analys is included in Table 01 . . Place an asterisk next to each analysis for which a metal digestion charge will apply. If this notation is not provided it will be assumed a metal digestion charge is included in the line item or is not required and will not be charged. If the laboratory uses -an alternate test method, cross out the test method specified and insert the alternate test method using red ink. All TCLP/SPLP extraction charges must be included in the TCLP/SPLP line items. All sample containers , preservatives, shipping containers in addition to providing pickup and delivery service will be provided at no additional charge to the City. Additionally, the Laboratory shall attach their Standard Price List at the end of this section along with any applicable discount rate (percentage off standard) that applies to the City of Fort Worth projects. Table 01 Test and 0 Me~hod 2 3 BTEX & MTBE (EPA 8021B) 4 BTEX & MTBE (EPA 8260 ) 5 MTBE (8021 B) 6 MTBE (8260 ) 7 TPH (TX 1005 ) 8 TPH (TX 1006) 10 TPH (EPA 8015 DRO/GRO) 11 PAH (EPA 8310) 12 PAH (EPA 8270) 14 Oil & Grease (EPA1664) ,15 PCB's (EPA 8082 ) ,.16 TCLP/SPLP Benzene (EPA 1311/1312/8020) 17 TCLP/SPLP Benzene (EP A 1311/1312/8260) 2-7 Item 19 20 21 22 23 24 25 26 27 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 Pesticides , Chlorinated (EPA 8081) TCLP/SPLP Pesticides (EPA 1311/1312/8081) Pesticides , Organophosphorus (EPA 8141) Herbicides (EPA 8151 ) Volatiles, voes (EPA 8260B) TCLP/SPLP voes (EPA 1311/1312/8260B) Semi Volatiles , SVOCs (EPA 8270) TCLP/SPLP SVOCs EPA (1311/1312/827 0 ) TCLP/SPLP Full (pesticides , herbicides , voe, SVOC , & Metals Acid Extractable (EPA 625/8270C) TCLP/SPLP 8 RCRA Metals EPA 1311/1312/6010B/6020 TCLP/SPLP 13 PP Metals (E PA 1311 /1312/601 OB/6020 TCLP/SPLP, one metal (EPA 1311/1312/6010B/6020) Total 8 RCRA Metals (EPA 601 OB/6020 ) Total 13 PP Metals (EPA6010/ 6020) Alumnium (EPA 6010/6020 ) Antimony (EPA 6010/6020 ) Arsenic (EPA 6010/6020) Barium (EPA 6010/6020) Beryllium ((EPA 6010/6020) Boron (EPA 6010/6020) Cadmium (EPA 6010/6020 ) Calcium (EPA 6010/6020 ) Chromium (EPA 6010/6020) Chromium VI (EPA 6010/6020 ) Cobalt (EPA 6010/6020) Copper (EPA 6010/6020) Iron (EPA 6010/6020) Lead (EPA 6010/6020) Magnesium (EPA 6010/6020 ) Manganese (EPA 6010/6020 ) Mercury (EPA 747 0/7471 ) Molybnium (EPA 6010/6020) Nickel (EPA 6010/6020) Potassium (EPA 6010/6020) 2-8 Item Number 54 55 56 57 58 59 60 61 65 66 67 68 69 70 71 74 75 76 85 86 87 88 89 90 91 92 93 94 95 "fest and Method Selenium (EPA 6010/6020) Silver (EPA 6010/6020) Sodium (EPA 6010/6020 ) Thallium (EPA 6010/6020) Tin (EPA 6010/6020 ) Titanium (EPA 6010/6020) Vanadium (EPA 6010/6020) Zinc (EPA 6010/6020) RGI (SW846 Various Methods) Corrosive , Steel (EPA 1110) Corrosive , pH (EPA 9045 ) Reactivity, Cyanide (EPA 9010) Reactivity, Sulfide (EPA 9030) pH (EPA 90408) lgnitability (Flash Point) by SW 1010 Paint Filter (EPA 9095) BTU BOD (Std Meth 52108) COD (EPA410.4) Fecal Coliform (Std Method 9221 E) Fecal Streptococcus (Std Method 9230 C) Corrosivity , pH (EPA 150 .1) Sulfate (EPA 375.2 or 300 .0) TDS (EPA 160.1) Total hardness as CaC03 (Std Method 2340 B or C) Total Trihalomethanes (EPA 501) Turbidity (EPA 180 .1) Alumnium (EPA 200 .7/200 .8) Copper (EPA 200.7/200.8) Iron (EPA 200.7/200 .8) Manganese (EPA 200 .7 /200 .8) Mercury (EPA 245.1) Silver (EPA 200.7/200 .8) Zinc (EPA 200 .7/200.8) 2-9 t!ll!I l"dACCUTES"t' 8/8/2006 Accutest Laboratories Gulf Coast, Inc. Schedule of Services for City of Ft. Worth Contact: Greg Grandits , 281-808-6360 Test Description Method Aqueous ~". ~< ~:1 <: ~~-, t~ ,, ~lJ 1~\~ 1: t\, ,'< E~ ... ~~ x.;4' J.,.,.""11±1..t: ., ,;,..; "« ""',. , l Volatiles -MS 624/8260 8 $85.00 Sem iv olatiles -MS 625/8270C $195 .00 Orqanochlorine Pesticides 608/8081A $95.00 Polychlorinated Biohenyls (PCBsl 608/8082 $50.00 BTEX Only 624/8260 $35.00 BTEX + MTBE 624 /8260 $40.00 BTE X / GRO Combo 8015 $55.00 TPH -1005 TCEQ-1005 $50 .00 TPH -1006 TCEQ -1006 $200 .00 Gasoline Range Organics (GRO\ 8015 $35 .00 Diesel Range Organics (ORO /ORO) 8015 $60.00 Pol ynuclear Aromatic HYdrocarbons 625/8270 $135.00 Pol ynuclear Aromatic Hydrocarbons S IMS-8270 * $85.00 Polynuclear Aromatic Hydroca rbons 8310 $95 .00 Herb icides /FULL LISTI 8151 $110.00 * If added to 8270 full scan analysis ,::::: % -'X "'v"'*. '\ .. ' » t'' j "' :; j ~-• /~"-' ~---.&.\,,~"==•• o '"''*•=O,H, ,,_ Individual Metal by ICP 200.7/60108 $9 .00 RCRA Metals (8) (digestion included) EPA/SW-846 $8 5 .00 Chromium , Hexavalent 7196 $30 .00 Mercury (includes diaest ion l 245.1/7470/7471 $20 .00 Metals Diaestion E PA/SW-846 $5 .00 -··-r ~,, " " "" '·"~·w C:'ft""" E&,~ ~-.*'"'~~~®.t:.l:~rn«>< 0 ' l • """'"\"'~""'"' "~ '" « -/.~NS Full TCLP/SPLP Pka SW-846 $595.00 TCLP/SPLP MetalsNOCs/SVOCs Pack SW-846 $390 .00 TCLP /SPLP Extraction only 1311/1312 $2 5 .00 TCLP /SPLP ZHE Ex traction only 1311/1312 $25 .00 TCLP /SPLP voes (w l o extraction l 8260 B $80 .00 TCLP /SPLP SVOCs (w/o extraction l 8270C $175 .00 TCLP /SPLP Pesticides (w /o extraction) 8081A $90 .00 TCLP /SPLP Herbicides (w /o extract ion) 8151A $115 .00 TCLP /SPLP Metals (wlo ex1raction) 6010B/7470A $8 5 .00 -~rt.LmlaBlf ,, ' ·:!3::", ' '. l ~;li:i::;:ios,®~""":o:.:& ;:,;J,;1)J~ £'"""'""' <""' "· RCI Package (all below) SW-846 $90 .00 Reacti ve Cyanide SW-846 $30 .00 Reacti ve Sulfide SW-846 $30 .00 Corrosivity SW-846 $10.00 lanitabilitv SW -846 $20 .0 0 -1-__ L_M/_ .. ~-=mm.'0M,"'-""""~ _ 1 :·.:: ~_.g """A. "''" ! is " Alkalin ity 310 .1 $20.00 Biocarbonate S M18 -4500 $20.00 Biochemical Oxyaen Demand (BOD) 405 .1 $35.00 Chloride 325.3/9252 $15 .00 Ch lorine , Residual 330.5/9076 $35.00 Page 1 Soil .. -. " ·=· $85 .00 $195 .00 $95 .00 $50.00 $35 .00 $40 .00 $5 5 .00 $50.00 $200.00 $35.00 $60.00 $135.00 $85.00 $95.00 $110.00 , .. w = "" " --~· ''"' .: •• ~;;J $9.00 $85 .00 $40.00 $20 .00 $5 .00 -· . $605 .00 $400.00 $30.00 $30 .00 $80.00 $175 .00 $90 .00 $1 15 .00 $85 .00 '' $90 .00 $30.00 $30.00 $10.00 $20 .00 $20 .00 $2 0 .00 $3 5 .00 $20.00 N/A Chemical Oxvaen Demand /COD) 410.1 $30.00 Co lor , Apparent Conductance , Specific Cvanide, Amenable Cvanide , Total Fluoride Hardness , Total Nitroaen, Ammonia Nitroaen, Total Kieldahl Nitroaen, Total Orqanic Nitroqen , Nitrate Nitroqen , Nitrite Nitrogen , Nitrate-Nitrite Oil & Grease IPH Phenolics , Tot al Phosphate , Ortho Phosphorus, Total Silica, Dissolved Solids, Total Solids , Total Disso lv ed Solids , Total Suspended Solids , Total Volati le Sulfate Sulfide TOC Total Organic Halides Turbidity Same Day 24 Hour TAT 110.2 120.1 335.1 /9020 335.2/9010 340 .2 130.2 350.1 351.2 SM 18 4500NM 353 .2 354.1 353 .2 1664/9 071 150.1 420 .1/9066 365 .2 365.3 370 .1 160 .3 160.1 160 .2 160.4 375 .4/9038 376.1 415.1/9060 9020 180 .1 $20.00 $15.00 $40.00 $40.00 $20.00 $20.00 $30.00 $35.00 $35.00 $30.00 $30 .00 $35 .00 $45.00 $7 .00 $30 .00 $25 .00 $25 .00 $30 .00 $15 .00 $15 .0 0 $15 .00 $20 .00 $20.00 $20 .00 $35 .00 $100 .00 $15 .00 200 % 90% 48 Hour TAT 75% 3 Da y TAT 40 % 4-5 Day TAT 15% 7-10 Day TAT 0 % Prices reflect a 7 working day turnaround Rush turnaround ma y not be possib le for some parameters (particularl y some TCLP parameters) On-line data access availab le via Lab link (password required) El ectronic delive rabl es available upon request@ no additional charge $30 .00 N/A $25.00 $40.00 $40 .00 $25 .00 $20 .00 $30 .00 $40 .00 $35.00 $30 .00 $30 .00 $35.00 $45.00 $7 .00 $35 .00 $30 .00 $30 .00 N/A N/A N/A NIA $35.00 $25.00 $25 .00 $40.00 $110.00 N/A All TRRP deliverables & requirements provided@ no additional charge wl the exception of Full Tier I/Level IV QA/QC (add 10%/ Percent moisture determination & associated dry-weight corrected soil results are provided at no additional charge For additional or project specific pricing please contact Greg Grandits (Account Rep.)@ 713-271-4700 Accutest Laboratories Gulf Coast, Inc. 10165 Harwin , Su ite 150 Houston , TX 77036 phone : (713) 271-4700 fa x : (713) 271-4770 www .accutest.com Page 2 2.6 PROVIDER 'S COMPANY EXPERIENCE 2.6.1 Provider shall identify its company name , address , telephone number(s), and FAX number(s) for the local office as well as the headquarters . 2.6.2 Provider shall attach an up-to-date and concise copy of its current Statement of Qualifications. If subcontractors, or branch locations of Prime Contractor, are to be utilized for services to be provided , current Statements of Qualifications for those companies/locations must also be included in section 2.10. ~ 2.6.3 Provide listing of major equipment owned and operated by the Provider including analysis capability and age of the equipment. In short , a ready reference of in- house capabilities for analysis. 2.6.4 Document Provider's experience managing and performing laboratory analyses. 2.6 .5 Describe any web-based customer service system that may be available to view , download data (include exporting format capabilities), and manage City projects. INCLUDE A COPY OF THE QUALIFICATIONS FOLLOWING THIS PAGE BOUND WITHIN THE PROPOSAL PACKAGE 2-10 Company Organization Introduction to Accutest: Accutest Laboratories is a privately held, independent testing laboratory successfully delivering legally defensible data for over 47 years. Founded in 1956, Accutest provides a full range of environmental analytical services to industrial, engineering/consulting and government clients throughout the United States. Operating from integrated laboratories in New Jersey, Massachusetts, Florida and Texas, Accutest's resources include a staff of over 285, six million dollars' worth of laboratory instrumentation and more than 100,000 square feet oflaboratory space. Accutest is ranked as the sixth largest environmental laboratory in the United States. Our growth is attributed to our corporate philosophy of developing long-term business relationships through dedication to quality, client services , technology and strong, consistent management. In an industry where acquisitions and consolidations are commonplace, Accutest remains one of the most stable, qualified, accurate and performance-based environmental testing laboratories. Our mission is to be the highest-quality, performance-focused, cost-effective provider in the environmental laboratory industry. Accutest's analytical programs include organic and inorganic analyses of water, soil and air samples collected in support ofRCRA, ISRA, NPDES, CERCLA, CAA, CWA, SDWA, ACOE, NFESC and other regulatory or industrial programs. Accredited by NELAC , our stringent corporate QA program enables us to maintain multi-state certification and approval by major federal agencies, as well as maintain credentials for national corporate analytical programs. Together with computerized data management and extensive electronic communications, this allows Accutest to provide reliable and uniform analytical services to our clients on a national basis. Accutest facilities supporting "City of Ft. Worth Contract: Gulf Coast Accutest Laboratories Gulf Coast 10165 Harwin Drive Houston, Texas 77036 713-271-4700 (phone) 713-271-4770 (fax) 4 Southeast (Emergency backup only) Accutest Laboratories Southeast 4405 Vineland Road Orlando, Florida 32811 407-425-6700 (phone) 407-425-0707 (fax) Laboratory Contact Information Sales Contact: The overall Accutest Program contact for the "City of Fort Worth" for assisting with administration issues , communication coordination and overall issues related laboratory performance is : Greg Grandits Business Development Manager -Accutest Gulf Coast 10165 Harwin Drive, Suite 150 Houston, Texas 77036 713-271-4700 (office), 713-271-4770 (FAX) 281-808 -63 60 ( cell) Technical Points of Contact: The following individuals are the technical points of contact (Project Mangers) for day to day activities and coordination of analytical testing needs. These individuals may involve local QA officers or the Laboratory Director for technical discussions as necessary. Accutest Laboratories Gulf Coast Sylvia Garza Project Manager 10165 Harwin Drive, Suite 150 Houston, Texas 77036 713-271-4700 (office) 281-808-6360 (cell) syl viag @accutest.com Ron Martino Laboratory Director 10165 Harwin Drive, Suite 150 Houston, Texas 77036 713-271-4700 (office) 281-850-4087 (cell) ro nm @ accut e st.com 5 Understanding of Scope of Wo rk Accutest is pleased to present this proposal for analytical services to "City of Fort Worth" for support of the environmental work associated with project: DEM 07-04: LAB. Our full service Houston, Texas laboratory located on Harwin A venue will support all the testing outlined in this proposal as required. Our Orlando Florida Laboratory will serve as an Emergency back up only in case of catastophic disasters. Accutest has read thoroughly the scope of work as presented and can comply with all requested analysis and reporting requirements to support of Project : DEM 07-04:LAB project. Xenco Laboratories will be our M /WBE partner throughout the term of the contract if awarded. Sample Pick Up / Containers: Samples courier service can be provided free of Charge for sample pick up and delivery to our Houston Laboratory. If FedEx is elected to be used all cost will be included in pricing for return shipping of samples to laboratory. All bottles, coolers and sample containers are provided in unit cost. Laboratory and Courier services are available Monday through Friday 7 am -6pm. Weekend and Holiday services can be arranged with advance notice. If desired Accutest can supply and maintain an inventory of containers for sampling events on site and perform sample pick up on a pre-scheduled basis without the need for a pickup request. Additional Sampling Value added Services: • Accutest can provide pre-printed chains and labeled sample containers for all analytical events if desired. All sample containers can be organized by sampling location to assist in organization of field activities. DI water can be provided at No additional charge. • Accutest offers customers real time Internet access for retrieval of data results, sample log in confirmations, tracking analysis status, access to chains of custody's, historical data review, and electronic downloads. 3 Accutest Laboratories Experience Matrix: M ultipl e Sup erfund RIFS Activities for Large RIFS Utility Company Full TCLITAL analyses for 1. CLP Sup erfund sites in Puerto Rico, North Carolina and Georgia Florida . CLP like Deliverables and extensive electronic deliverables. RIFS Brownfield Redevelopment Project Highly visible RCRA Brownfield Site. Expedited analysis for priority pollutant 2. BROWN compounds , waste classification and general chemistry New Jersey parameters . LabLink electronically transferred data via auto e- FIELDS mail. NPDES P etroleum Refinery, Linden, NJ Analytical services m Major RCRA su pport of the Bayway Refinery . Analyzed groundwater and P etroleum 3. CER soil samp les for petroleum based contaminants including full Company CLP TCL/T AL. Full and reduced deliverables. Custom CLA electronic deliverables . Third party validation. Texas RCRA Texas Commission Environm ental Quality Analytica l TCEQ Field 4. NPDES Services Contract in support of Field Operations Divi sion. Operation s Superfund Programs include Superfund , UST , RCRA , and NPDES , Division utili z ing EPA 600 and 8000 Series Methods. Texas Augusta R efinery remedial investigation Analytical Services Large Contract with Shaw E&I and Williams Energy in support of Rem ediation 5. RIFS analysis for clean up and remediation of the former Augusta Former Augusta Refinery in Kansas. 3 project with monthly sampling events for 8270 , 8260, Metals , TPH. Using SW-846 methods to meet Refinery very low detection limits as per project objectives. Kansas TCEO Certification: Accutest Laboratories is NELAP certified by the State of Texas. Accutest NELAP Certification number is# Tl04704220-06TX Accutest is a TCEO Contract Laboratory: Accutest Laboratories is a TCEQ contract laboratory for the TCEQ field Operations division. Accutest has been awarded for the past 7 years a direct analytical contract with the TCEQ. Accutest routinely serves as the TCEQ quality laboratory for split sampling events when the TCEQ is involved with site investigations. Accutest serves multiple TCEQ regions on a routine basis and serves as the TCEQ's largest contract laboratory provider. 13 ACCUTEST LABORATORIES Statement of Qualifications And Experience 2007 2007 Statement of Qualifications and Experience 0 Corporate Headquarters Accutest Laboratories 2235 Route 130 Dayton , New Jersey 08810 (732) 329-0200 • New England Accutest Laboratories of New England 495 Technology Center West Marlborough, Massachusetts 01752 (508) 481-6200 • Southeast Accutest Laboratories Southeast 4405 Vineland Road Orlando , Florida 32811 (407) 425-6700 • Gulf Coast Accutest Laboratories Gulf Coast 10165 Harwin Drive Houston, Texas 77036 (713) 271-4 700 Proprietary Notice -Information contained herein is the property of and is proprietary to Accutest Laboratories and shall not be reproduced , disclosed , or used without the prior written permission of Accutest Laboratories . Section D Accutest Overview Introduction Project Management Client Services Table of Contents Laboratory Information Management System (LIMS) • Electronic Data Deliverables • LabLink® fJ Facilities/Resources Locations Instrumentation/Equipment BJ Analytical Capabilities Analytical Capabilities Deliverables Field Services Courier Services El Staff Organization and Responsibility Key Technical Staff lfl Quality Assurance QA Program Proficiency Test Scores Certifications m Project Experience Engineering Firms Industrial Projects DOD Projects 1a Miscellaneous Health and Safety Waste/Sample Disposal Insurance Small Business Classification Affirmative Action Dun & Bradstreet Rating Page 1 2 3 4 5 7 8 9 10 10 11 12 18 20 21 24 26 28 30 30 31 31 31 31 Introduction to Accutest "Accutest remains one of the most stable, independent environmental testing labs in the industry." Accutest Laboratories is a privately held, independent testing laboratory successfully delivering legally defensible data for over 50 years. Founded in 1956, Accutest provides a full range of environmental analytical services to industrial, engineering/consulting and government clients throughout the United States. Operating from coordinated laboratories in New Jersey , Massachusetts, Florida and Texas, Accutest's resources include a staff of over 335 , seven million dollars' worth of laboratory instrumentation/equipment and more than 110 ,000 square feet of laboratory space. Accutest is ranked as the 3rd largest environmental laboratory in the United States. Our growth is attributed to our corporate philosophy of developing long term business relationships through dedication to client services, technology and strong, consistent management. In an industry where acquisitions and consolidations are common place, Accutest remains one of the most stable, qualified , accurate and performance based environmental testing laboratories today. Our mission is to be the most cost, quality and performance-effective laboratory in the industry. Accutest 's analytical programs include organic and inorganic analyses of water, soil and air samples collected in support ofRCRA , ISRA, NPDES , CERCLA, CAA, CWA , SOWA , ACOE, NFESC , AFCEE and other regulatory or industrial programs. Our stringent corporate QA program is based on full NELAP accreditation. This enables us to hold multi-state certifications, approval by major federal agencies and maintain credentials for national corporate analytical programs . This, combined with LabLink, our web based data management service and extensive electronic deliverables, allows Accutest to provide reliable and uniform analytical services to our clients on a national basis. D 1 Project Management "We take great pride in the quality of services provided. This is best exemplified by the fact that more than 85°/o of Accutest's business is from repeat clients." The basis of our business philosophy is the relationship we build with our c li ents. Good communication develops trusted partnerships , which in turn leads to successful project management. Our primary goal is to create and maintain lo ya l, long-term relationships . We take g reat pride in the quality of services provided. This is best exemplified by the fact that 85% of Accutest 's business is from repeat clients. Our project managers are committed to delivering the full measure of our expertise, to ensure complete c li ent satisfaction with eac h and eve ry Accutest service: • subm itta l of technical information • analytical work plan assistance • coordination of field sampling • sample shipping/courier services • analyses/project status updates • LabLink electronic data service • final report delivery /int erpretation • electronic data deliverables (EDD's) • inv oici ng Accutest's client services group understands through exper ience that successfu l completion of every project requires up-front planning. This includes everything from certification requirements , regulatory-specific methodology and detection limits, matrix specific quality control, sample delivery criter ia and turnaround requirements to electronic data deliverables (EDD) and invoicing formats. The resulting product is a data package that is on -tim e, reliable and in the desired format. The efforts of our c li ent service group -project managers and technical sa les representatives - teamed with our field and ana lyt ica l personnel serve to make Accutest an extension of yo ur environmental staff. We are your partner. D 2 Client Services "Accutest is a performance- based laboratory continuously monitoring key indicators identified by our clients." From the very beginning , serving clients needs and a lw ays striv in g to find better ways to fulfill those needs , has been at the heart of Accutest Laboratories. Our philosophy is to enhance communications and teamwork , cultivating in a work environment dedicated to continuous process evaluation, redesign and improvement. Our employees have a sense of ownership which fosters their commitment to total customer satisfaction. Al l our clients are assigned to a project manager who becomes their dedicated representative and contact for all analytica l inquiries. The assigned project manager ensures that client expectations and program objectives are met by obtaining a thorough understanding of all relevant technical and contractua l requirements. Our highly experienced staff of quality assurance specialists , chemists , and project managers comb in e to form a unique resource that can be used to provide technical and regulatory guidance and provide ass istance developing innovative solutions to today 's complex array of environmenta l requirements. Accutest is a performance-based laboratory continuously monitoring key indicators identified by our clients as vital to their satisfact ion. The following are an example of indicators that are used as a measure of successfu l performance: • turnaround time of emergency /rush analytical reports • turnaround time of standard analyt ical reports • reissued reports • holding times • data challenges Using statistica l evaluations, we are able to measure and refine our performance to continuously exceed client expectations. D 3 "Accutest consistently provides the most accurate EDD's through totally automated data transfer." Laboratory Information Management System (LIMS) The LIMS is the most critical central tool in the operation of the laboratory. Accutest 's LIMS is one of the most powerful and sophisticated in the industry today . The LIMS at each Accutest location resides on an independent server sized to insure impressive performance for our internal user s and our on-line customers. The LIMS is based on a state of the art Oracle relational database that has been specifically designed to handle the complex issues faced by the commercial environmental laboratory. The Accutest LIMS automates virtually every phase of laboratory operations , including sample receipt/login , sample scheduling and tracking , data acqui sition , calculations , QA /QC , final reports , electronic deliverables , and invoicing . As a result , it allows Accutest to deliver the most accurate and consistent product in the industry. Electronic Data Deliverables One of the most significant trends in this industry is the increased dependence on Electronic Data Deliverables , or EDD 's. EDD 's that are produced or modified manually cannot be relied on for accuracy. Accutest consistently provides the most accurate EDD's through totally automated data transfer. At the front end, virtually all laboratory data is collected electronicall y into the LIMS without manual transcription and goes through multiple levels of approval. From this point , the LIMS database becomes the single source for all deliverables including data reports , QC reports, and EDD 's. Simply put , this means that the raw data matches the paper reports , and the reports match the EDD 's. LabLink® The LIMS database has allowed Accutest to develop LabLink , the most comprehensive on-line data service in the industry. Available via the Internet to all Accutest clients, LabLink provides real-time access to project status , current and historical data, on-line reports , electronic data deliverables , and billing information. You can even configure LabLink to send you reports via email automatically upon data completion. We will provide you with a secure account with all interactions encrypted to keep your data confidential. LabLink has set a new standard for e lectronic data management. D 4 F acili ties/Resources "Accutest's facilities have been designed from the ground up, specifically for environmental laboratory testing." Accutest 's facilities have been designed from the ground up, specifically for environmental laboratory testing. The installation is functionally designed both to promote efficient processing of a large volume of samples and provide a comfortable, safe working environment for laboratory staff. The facilities are equipped with centralized process gas distribution, water purification centers and separate, dedicated HY AC systems . These systems maintain critical positive/negative pressure relationships between internal laboratories, ensuring adequate ventilation and preventing atmospheric cross-contamination. • Accutest Laboratories (Corporate Headquarters) 2235 Route 130 Dayton , New Jersey 08810 50 ,000 ft 2 Phone: (732) 329-0200 Fax: (732) 329-3499 • Accutest Laboratories of New England 495 Technology Center West Marlborough , Massachusetts 01752 25,000 ft 2 Phone: (508) 481-6200 Fax: (508) 481-7753 • Accutest Laboratories Southeast 4405 Vineland Road, Suite C-15 Orlando, Florida 32811 24,000 ft 2 Phone: ( 407) 425-6700 Fax: ( 407) 425-0707 • Accutest Laboratories Gulf Coast 10165 Harwin Drive Houston , Texas 77009 13 ,000 ft 2 Phone: (713) 271-4700 Fax: (713) 271-4 770 5 D NJ Lab • MA La b D FL Lab D TX Lab 0) Regional Laboratories and Centers • 0 AZ NM Laboratory Sa les/Service Ce nt e r TX e Texas Gulf Coast Massachu se tts NJ DE MD DC MA RI CT New J e rsey Mid- Atlantic Florida Southeast II In strumentation "A major factor when evaluating a laboratory is the age, model and condition of its equipment." Acc utes t ma int a in s a ut omate d, co mpu te ri ze d ana lyti ca l in strum ent ati on to supp ort large co mpl ex invest igat ions as we ll as ro ut in e ana lyses of stand ard ana lyt ica l para mete rs. O ur co mmi tme nt to our c lie nts is re fl ected by o ur investme nt in fac il it ies , eq ui pment and tec hn o logy. Acc utest's pro du cti o n ca pa bili ty , ca pac ity and redund ancy of in st rum e nt at ion ensur es the re li a bili ty and pe rfo rma nce nee ded to success full y de live r maj or ana lyti ca l proj ects . In strum ents are dedi cate d to s pec ific mat ri ces and ana lyses to preve nt cross co nta m inatio n. A majo r factor whe n eva lu at in g a la borato ry is t he age, mode l a nd co nditi o n of its equip me nt. Acc ut es t ma in ta in s a hi gh propo rtion of ad va nce d late mode l in strum ent ation . Major Instrumentation Summary Analytical NJ MA FL TX Accutest Instrument Laboratory Laboratory Laboratory Laboratory Total GC/MS VOA 33 11 9 4 57 GC/MS SVOA 9 3 4 2 18 GCVOA 12 6 8 2 28 GC SVOA 12 7 13 4 36 HPLC 1 2 4 --7 ICP/ICPMS 3/1 2 2 1 9 Analytical Capabilities "In 2006, Accutest logged in more than 54,000 jobs, processed over 350,000 samples and reported over 1,000,000 tests." Accutest 's staff has extensive expertise in the use of ana lytical methods approved by federal and state environmental regulatory agencies. The foundation of our company is the production and presentation of accurate analytical data. In 2006 Accutest logged in more than 54 ,000 jobs, processed over 350 ,000 samp les and reported over 1,000 ,000 tests. Al l of these tests were performed under strict compliance with project-specific data quality objectives. The most recent versions of the following methodology documents are routinely utilized by Accutest: • EPA Federa l Register 40 CFR Part 136 • EPA Test Methods for Eva luatin g Solid Waste, SW-846 • EPA Methods for Chemica l Ana lysis of Water and Wastes • EPA Methods for the determination of Toxic Organic Compounds in Air , TO Methods • EPA Methods for the Determination of Organic Compounds in Drinking Water • EPA Methods for the Determination of Metals in Enviro nm enta l Samples • Standard Methods for the Examination of Water and Wastewater • ASTM -American Society for Testing and Materials • NIOSH Manual for Analytical Methods Acc ut est 's ana lytica l expertise includes organ ic and in organic analysis of water , soi l and air samples co ll ected in support of the following programs: • ISRA -Indu strial Site Remediation Act • RCRA -Resource Conservation Recovery Act • NPDES -National Pollution Discharge Elimination System • CAA - C lean Air Act • CERCLA -Compre hens ive Environmental Response Compensation Liability Act • CW A - C lean Water Act • SDW A -Safe Drinking Water Act • ACOE -Army Corp of Engineers • NFESC -Naval Facilities Engineering Service Center • AFCEE -Air Force Central Env ironmental Excellence 9 Analytical Capabilities "The foundation of our company is the production and presentation of accurate analytical data." T he types of projects and studies performed by Accutest includ e: • Site Investigations • Remedial Investigation s and Feasibility St udi es • Remedial Action • Groundwater Monitoring • Underground Storage Tanks • Air Monitoring • Permitting and Compliance Monitoring • Treatment System Monitoring • Hazardous Waste Id entification /C lass ifi cat io n Deliverables Accutest's final reports are fully supported by QA /QC deliverables designed to meet the requirements of the regulatory program that the data wi ll be utili zed for. Our reports are designed for ease of results interpretation as we ll as efficient va lid ation of the supported data. In addition to hard copy, Accutest presently provides e lectronic data deliverables (EDD's) for over 95% of o ur projects. T he fo ll owing formats are routinely produced by Accutest: Hard Copy • Ful l Deliverables (Leve l 4) • Reduced Deliverables (Leve l 2 & 3) • Standard Commercia l Format (Leve l I) E lectronic • LabLink® -Accutest's Proprietary On-Line Data Management Service • eHard Copy -Full y Navigable, Interactive, PDF Report • Commercia l Database Imp ort Formats (i.e. EQUTS, Enfos, GIS /Key) • Client Specific Database Import Formats • Custom Spreadsheet Reports • Regulatory Required EDD Formats 10 Field Services "Accutest's field services department offers OSHA- trained sampling technicians to support analytical projects." Accutest 's field services department offers OSHA-trained sampling technicians to support analytical projects. Accutest has the capacity to fu ll y equip and mobilize teams for level C and D sampling . Our technicians have extensive experience in the sampling of groundwater, surface water , soi l, hazardous waste and air. Our sampling teams have been successfully audited by State and Federal regu latory agencies. All field parameters are monitored (pH , specific conductance , temperature , dissolved oxygen) to ensure representative groundwater samples. The following field sampling procedures are utilized by Accutest. • Equipment Decontamination • Teflon /SS Bailers • Submersib le Well Pumps • Peristaltic Pumps • 24 Hour Composite Samplers • Wheaton Grab Samplers • Bacon Bomb Samp lers • Open Tube Samplers • Soil Augers/Trowels • Summa Canisters /Ted lar Bags • Personal Air Samplers/Tubes Courier Services In addition to field services , Accutest maintains a fleet of couriers that handle sample pickup and container delivery within a I 00 mile radius of our laboratories. All couriers are employees of Accutest , with experience in handling environmenta l samp les and associated paperwork. For samples that will be shipped , our samp le management department wi ll provide properly packaged coolers containing pre-labeled sample bottles, preservatives, sea ls, chain of custody documentation and temperature blanks. Fie ld quality control samples such as trip and field blanks will also be provided. Overnight shipping will be coordinated by Accutest. 11 Accutest Laboratories Corporate Organizational Chart Renee Capizzano Accounting Manager Reza Tand Laboratory Director New England Regional Laboratory Harry Behzad i Laboratory Director Southeast Regional Laboratory Ronald Martino Laboratory Director Gulf Coast Regional Laboratory Olivia Lawless Human Resources Manager ncent J. Pugliese President, CEO Matthew Cordova Client Services Director David Speis Jamie Yakes Health & Safety Manager Brian Davis IT Systems Manager II 12 Key Technical Staff William Sherding Vice President, Laboratory Operations Years with Firm: 25 Total Years Ex perience: 25 Degree : BS , Natural Resources Experience: Mr. Sherding is responsible for day to day laboratory operations at Accutest's Corporate Headquarters in Dayton , NJ. He has supervisory responsibility for a ll technical personnel. This includes responsibility for all operational department managers, who report directly to Mr. Sherding regarding production , capacity, and technical issues. He initiates all equipment purchases and executes facility design to accommodate growth in targeted business sectors. Mr. Sherding led the design effort for the expansions of the New Jersey , Massachusetts, Florida, and Houston facilities. Mr. Sherding's tenure at Accutest has included "hands on" experience for the majority of the testing programs used by the organization. This includes method development, laboratory implementation , and sample analysis. He also provides technical support to all Accutest faci liti es on method development, equipment troubleshooting , and production efficiency. Mr. Sherding's method implementation credits include analytical program s for organic compounds by GC and GC/MS techniques using EPA 500 , 600 , 8000, and CLP method s . He has also designed and implemented an air toxics program for the analysis of ambient air using EPA Methods T0-3/EPA18 and T0-14/15. He has researched , designed , developed , and implemented methodology for the analysis of dissolved gases to monitor the metabolites of natural attenuation. David N. Speis Director, Corporate Quality Assurance Years with Firm: 9 Total Years Experience: 38 Degree: BS , Science Education Experience: Mr. Speis is Accutest's Director of Corporate Quality Assurance. He is responsible for developing the corporate quality assurance program and implementing the program into each of Accutest's laboratory facilities. Mr. Speis began his career in environmental chemistry in 1969. His experience in environmental chemistry includes e leven (11) years with USEPA Region II as a bench chemist conducting the analys is of organic pollutants by GC/MS. He has extensive management experience in commercial environmental laboratories including technical operations, quality assurance, business development, and facility general management. Mr. Speis is the Vice Cha irm an of the Board of Directors of the Institute for National Environmental Laboratory Accreditation (INELA) and the Secretary of the New Jersey Environmental Laboratory Advisory Committee. He served on the Editorial Advisory Board of Environmental Testing and Analysis and on the board of directors of the International Association of E nvironmental Testing Laboratories (IAETL). He has published sixteen (16) articles on various topics in environmental chemistry and bu s iness management of commercial laboratory operat ions . II 13 Andrew Dexter Vice President, Information Systems Years with Firm : 13 Total Years Experience: 3 I Experience: As rs Director, Mr. Dexter has developed an overall TS strategy for Accutest and has taken the lead role in implementing a new state-of-the-art LIMS system at all Accutest Laboratories. He has over 20 years of experience in systems and laboratory automation as well as 14 years of environmental laboratory experience . Before joining Accutest, Mr. Dexter was one of seven founding members of Automated Compliance Systems, where he played a key roll in developing the UMS software now implemented at Accutest. He was the sole designer/developer of Seedpak2 , an Oracle-based instrument interfacing package that was later licensed to Perkin-Elmer for use in its SQL-LIMS product. Mr. Dexter was the sole designer/developer of AQUARIUS , a software package for automated GC/MS data acquisition. This package was subsequently licensed to Hewlett Packard and sold several thousand copies worldwide. It is Mr. Dexter 's mission to take Accutest to the next level of automation using the latest indu stry standard relational database software. This will provide Accutest with the utmost in efficient and accurate data handling and will give Accutest clients the most flexible and open access to their data in the industry today. Jamie J. Yakes Corporate Health and Safety Manager Years with Firm : 6 Total Years Experience: 8 Certified: 40 Hr. Hazwoper; Degree: BS , Biochemistry Experience: Mr. Yakes is the Corporate Health and Safety Manager for Accutest Laboratories . His primary responsibilities are to ensure Accutest provides a safe and healthy environment for its employees, visitors and clients, while ensuring public protection and the preservation of the company 's a s sets and property. To accomplish this task, Mr. Yakes creates and maintains up-to- date s afety programs pertinent to Accutest's functions , as well as develops and administers company-wide training programs regarding health and safety for its employees. Through both scheduled and unscheduled facility audits and inspections, Mr. Yakes ensures the facility and its employees perform in a manner consistent, not only with federal , state and local regulations, but al s o with Accutest Laboratories commitment to safety. Prior to Mr. Yakes ' position of Corporate Health and Safety Manager he served as Inorganic Supervisor for Accutest Headquarters in New Jersey. As Inorganic Supervisor Mr. Yakes gained extensive experience in clas s ical/w et chemistry preparation and analysis , instrumental analysis including TOC by IR , ion chromatography , and automated colorimetric analyses , TCLP extractions , and microbiology . He worked in areas of management, scheduling, and training as well as in instrument and an alytical t roubl eshootin g . Mr. Yakes was al s o respon s ible for data review for regular a nd CLP work and wo rked closel y w ith th e client s ervice s department in providing information and answering qu estion s fo r c li e nt s . II 14 Reza Tand Laboratory Director, New England Division Years with Firm: 19 Total Years Experience: 22 Degree: BS , Chemistry Experience: Mr. Tand is currently Director of the New England Division Laboratory. The division specializes in the analysis of organics and inorganics in water, soil and air matrices with special programs for waste classification (TCLP) and priority turnarounds. Mr. Tand was formally Manager of the Organics Laboratories at Accutest Headquarters in New Jersey. Previously, Mr. Tand served 3 years as GC /MS supervisor, generating EPA/CLP data for a major environmenta l production laboratory. He was also responsible for 2,3,7,8 TCDD analysis, instrument trouble shoot in g and data validation. Mr. Tand's duties include the coordination with the NJ laboratories on major environmenta l projects and overseeing all projects in the New England market. Harry Behzadi Laboratory Director, Southeast Division Years with Firm: 13 Total Years Experience: 24 Degree: Ph.D., Analytica l Chemistry Experience: Dr. Behzadi is currently Director of the Southeast Division Laboratory . He has extensive experience in trace organics and inorganic analyses of environmental samples. He has been respon s ible for laboratory management , analytical method development, professional training and QA /QC in both the environmental and pharmaceutical industries. Dr. Behzadi has extensive experience in the operation , maintenance and trouble shooting of the following instrumentation; GC /MS , GC , HPLC , ICP , AA , IR , GPC and UV/VJS. Previously , Dr. Behzadi has served as an environmental laboratory organics manager and a pharmaceutical laboratory manager. Ronald Martino Laboratory Director, Gulf Coast Division Years with Firm: 6 Total Years Experience: 20 Degree: BS , Chemistry Experience: Mr. Martino is responsible for day to day laboratory operations at Accutest 's Gulf Coast laboratory in Houston , TX. Accutest Gulf Coast specializes in the analysis of organics and inorganics in water , soi l and sediment matrices. He has supervisory responsibility for all personnel. This includes responsibility for all departments. Mr. Martino's ana lytical experience includes a ll environmental analysis performed at Accutest Gulf Coast. Mr. Martino initiates all equipment purchases , develops and implements new methodology , oversees all production efficiency , and approves all data in compl iance with Accutest's QA/QC gu id elines. Previously , Mr. Martino has 12 years experience as an organic analyst and supervisor as well as 3 years ex perience as a project manager. II 15 II Wen-Wen Chi Organics Manager Years with Firm: 18 Total Years Experience: 27 Degree: BS , Chemical Engineering Experience: As the Mana ge r of the Organics Laboratory, Ms. Chi has extensive experience in Priority Pollutant Analysis utilizing GC -GC /MS Technology, EPA 500 /600 Series Methodology, SW846 , CLP work for EPA , Appendix IX and Dioxin Analysis. Ms. Chi also has a great deal of expe rience in special project assignments (EPA, SAS), new equipment/methodology evaluations , start-up laboratory plannin g, technical consultation with clients, and development of application programs to standardize, simplify and automate laboratory operations. Nancy Cole lnorganics Manager Years with Firm: 18 Total Years Experience: 23 Degree: MS , lnorganics Chemistry Experience: Ms. Cole is currently the I norganics Manager for Accutest Laboratories. The 1 norganics division include s metals digestion and analysis including ICP, ICP/MS and GF AAS , classical /wet chemistry preparation and analysis, instrumental analysis including TOC by TR , ion chromatography, and automated colorimetric analyses, TCLP extractions, and microbiology . Ms . Cole has exte nsive experience in EPA, SW846, CLP, Standard Methods, NIOSH , and ASTM methodologies. She has attended training seminars on a variety of technical and managerial issues. Ms. Cole is responsible for overseeing all work in the metals and general chemistry areas. She works in areas of management , scheduling, and training as well as in instrument and analytical troubleshooting and method s development. She is also involved in data review for regular and CLP work and works closely with the client services department in providing information and answering questions for clients. John Hamilton Technical Supervisor, New England Division Years with Firm: 19 Total Years Experience: 24 Degree: BS , Chemistry Experience: Mr. Hamilton is currently the Technical Supervisor at Accutest Laboratories of New England . Previous positions include Chief Chemist and Senior Chemist. Mr. Hamilton has extensive experience in analytical chemistry including GC, GC /MS , HPLC , ICP and AA with a wide variety of matrices and has coordinated and evaluated multi-department projects involving Superfund/CLP , U.S. Army Toxic and Hazardous Materials Agency, various state/federal environmental agencies and special projects for major corporations and engineering/contractor clients. He has developed , refined and utilized al l major forms of Chromatography and Gel Filtration /Permeation and Chromogenic Paired Ion . Detection systems have included Flame detection systems Gas /Liquid, Gas /Solids, Liquid /Liquid , Liquid /So lid , Ion Exchange, Ion Exclusion, Ionization , Electron Capture , Flame Photometric , Radiometric , Fluorescence UVNTS, Photoionization , Electrochemical and Conductimetric . 16 Matthew Cordova Director, Client Services Years with Firm: I 0 Total Years Ex perience: 26 Degree: BS , Marine Biology Experience: As the Client Services Manager, Mr. Cordova is respon s ible for the overall implementation of the client services and project management activities within the laboratory. He also mana ges the sample log in process, to ensure that project specifications are accurately entered into the LIM system and communicated to the laboratory . Mr. Cordova is also responsible for developing detailed weekly forecasting reports of upcoming work which are then used for strategic planning. Working in conjunction with the production managers , Mr. Cordova ensures that the Client Services Department meets project commitments and data quality objectives. Mr. Cordova has extensive experience in the environmental testing field. He has 6 years of bench level inorganic chemistry experience, and has extensive knowledge of atomic s pectroscopy . Since 1987 , Mr. Cordova has served in a variety of laboratory management positions ; thi s has provided him with experience in field sampling, quality assurance, laboratory audits, project management, regulatory comp li ance, lab safety, computers and all technical areas common to environmental laboratories . Mr. Cordova has a thorough knowledge of environmental methods found in SW846, EPA-MCA WW, Standard Methods, 40 CFR, and the Contract Laboratory Program (CLP). His experience as a Lab Operations Manager a ll ows him to provide total project management for Accutest clients. Ronald Van Blarcom Manager, Sample Management Years with Firm: 20 Total Years Ex perience: 24 Experience: Mr. Van Blarcom oversees the Sample Management Department providing sa mpling kits for shipping and local courier services. He is also responsible for the processing, storage, tracking and final disposal of samp les submitted to the laboratory. Mr. Yan Blarcom has been instrumental in developing one of the largest sample management service operations on the East Coast. This group directly interfaces with clients providing advice and service for their sa mpling needs. The Sample Management group also interfaces with other work groups at Accutest in our continuing strive for quality. Mr. Van Blarcom is also in charge of the bottle glassware department and help s to oversee the building maintenance as well. II 17 Harold Meissner Manager, Field Operations Years with Firm: 21 Total Years Experience: 21 Degree: BS Biology /Chemistry Experience: Mr. Meissner's Field Operations Group , with support from the Sample Management Group , provides field sampling, testing/analysis and instrumentation screening se rvices to a wide range of clients in support of their environmental operations. The Group has extensive experience with a wide variety of environmental regulatory agency sampling procedures including USEPA, USACOE and NIOSH protocols . The group is standardized on NJDEP and NYDEC field sampling protocols . The group, headed by Mr. Meissner , currently fields a fully-equipped team experienced in sampling a wide variety of matrices including water, wastewater, stormwater , so il , air, solids and sludge. Mr. Meissner and all sampling personnel are fully OSHA certified. II 18 Quality Assurance Th e Accutes t QA Prog ram "Our Quality Assurance program is designed to ensure that Accutest delivers legally- defensible data of the highest quality on a consistent basis." At Acc ute st, we co ntin ua ll y build q ua li ty in to the pro du ct de li vere d to o ur c li ents as a des ign spec ificat ion . T hi s is acco m plished by incorporati ng the e le me nts of our Q ua lity Syste m in to every laborato ry process as an intrin sic co m po nent of o ur day to day operati o ns. O ur a pp roac h reflects o ur de di ca ti on to a qu a lit y sys tem that meets nat io na l a nd inte rn ationa l sta nd ard s . T hi s is ac hi eved thro ugh a Corporate Qu a lity Assurance Program th at esta bli shes t he fra mewo rk fo r th e qu a li ty syste ms o pera ted and ma int a in ed at eac h Acc utes t fac ility. O ur Po li cy reflec ts o ur kn ow led ge of t he reg ul ato ry ana lyti ca l process and t he ro le o ur pro du ct plays in safeg ua rdin g hum a n hea lt h an d th e enviro nm ent as deta il ed in th e fo ll ow in g: P olicy State ment: T he manageme nt and staff of Acc utest La borato ri es share th e res pons ibili ty for pro du ct q ua li ty. Acco rdin g ly, Acc utest's qu a li ty sys tem is des ig ned to ass ure th at all processes and pro ce dur es , whi ch are co mpo nents of env iro nm enta l data pro du cti o n, mee t es t abli shed indu str y requir eme nts , a re adequ ate ly doc um ent ed fro m a proce du ra l and data tra cea bili ty pe rspect ive , and are co ns iste nt ly exec ute d by the staff. It a lso ass ures t hat ana lyt ica l data of know n q uali ty , mee tin g the q ua li ty obj ect ives of t he ana lyt ica l met hod in use and th e data use r's re qu irement s, are co ns iste ntl y pro du ced in th e laboratory . T hi s ass ura nce e na bl es th e data use r to make ra ti ona l, co nfid ent , cost -effect ive dec isio ns on t he assess me nt and reso lu t io n of env iro nm enta l iss ues. T he laborato ry Q ua li ty System a lso prov id es th e manage ment staff w ith data qu a li ty and operat io nal fee db ack data . T h is enabl es t hem to determin e if th e la borato ry has ac hi eve d th e establis hed q ua li ty and o peratio na l sta nd ard s, whic h are di ctate d by th e c li ent or esta bli shed by reg ul ati o n. T he in fo rm at io n prov ided to manage ment , thro ug h the Q ua li ty Syste m, is used to assess operat ional perfor mance fro m a qua I ity pers pec ti ve and to perfor m co rr ect ive act io n as necessary. 19 The Quality Assurance Standard We understand the importance of operating a quality program which meets the requirements for laboratory operations established by the international community . Every Accutest facility has implemented a quality system that follows ISO Guide 17025 , General Requirements for the Competence of Calibration and Testing Laboratories. The structure of TSO Guide 17025 has been adopted by the National Environmental Laboratory Accreditation Program (NELAP), the voluntary national accreditation program originally established by the USEPA . NELAP has established a uniform national standard for environmental laboratories that places a strong emphasis on quality systems. The quality system at each Accutest facility has been designed to meet NELAP Standards. Accutest was among the first laboratories to submit applications to the approved state accrediting authorities for recognition as a NELAP Accredited laboratory. All Accutest Facilities are NELAP Accredited. Quality Assurance At The Corporate Level Our Corporate Quality Assurance Program establishes the quality framework for each individual Accutest facility. The Corporate Quality Assurance Director determines corporate policies and defines the quality responsibilities at the facility level. He is responsible for monitoring the quality system at each facility and providing feedback to the management staff. The reporting relationship between Corporate Quality Assurance and the Quality Assurance Officers at the facilities reflects a dotted line responsibility. This type of relationship enables the Corporate Program to be implemented locally while enhancing day to day operational efficiency at each facility. Quality Assurance At the Facility Level Accutest 's philosophy enables each facility to implement quality policy using their unique operating style. This approach provides them with the autonomy they need to meet the requirements of their local regulatory jurisdictions while conducting business using the procedures that enable them to most efficiently meet their operational objectives. The Quality Assurance Program at each facility incorporates all the elements of TSO Guide 17025 and NELAP. The operations management staff is responsible for implementing the program elements and operating the quality system. The Quality Assurance Officer monitors the program, provides feedback to local and corporate management , and assists with corrective action and training if needed . 20 WP/WS Proficiency Test Scores Non-Potable Water (WP) Potable Water (WS) Solid & Hazardous Wastes (SHW) ,- - 100 98 ; 96 e a, 94 Q. 92 90 NJ Lab MA Lab FL Lab 99.6% 99.3% 99.0% 96.9% 97.3% 100% 99.2% 99.4% 99.3% Lab Network PT Scores ...__ _____. -T TX Lab 99.0% Na 97.1% 1 Non-Potable Water Potable Water Solid & Hazardous Wastes PT Test Category Accutest participates in the following regulatory proficiency test programs: • Water Pollution Study (NELAP fields of testing) • Water Supp ly Study (NELAP fields of testing) • RCRA Water PT Samples • RCRA Soil PT Samples • independent Single Blind PT Samp les • Independent Double Blind PT Samples Net Avg 98.9% 97.2% 99.2% Accutest also participates in numerous national corporate proficiency te st programs/audits sponsored by our client s, utilizing independent , third party consulting firms. 21 Certifications/ Accreditations Agency Laboratorv Facilitv Laboratorv ID# NELAP New Jersey (AA: New Jersey) NJ00141 (Primary Accredit in g Authority) Florida (AA: Florida) FL00946 Texas (AA: Texas) Tl 04 704220-06TX Massachusetts (AA: Florida) MAOOl36 Alabama Florida 41500 Arkansas Florida 03-072-0 Texas 04-024-1 Cali fornia (NELAP) New Jersey 01152CA Flor id a 04226CA Connecticut New Jersey PH-0585 Massachusetts PH-0109 Delaware New Jersey DNREC HSCA Program Florida (NELAP) New Jersey E87482 Massachusetts E87579 Florida E83510 Texas E87628 Georgia Florida Illin ois (N ELAP) New Jersey 200045 Massachusetts 001061 [ndiana New Jersey C-NJ-03 Iowa Florida IA366 Kansas (NELAP) New Jersey E-10356 Florida E-10327 Texas E-10366 Kentucky New Jersey 90131 Florida 0065 Louisiana (NELAP) New Jersey 04106 Florida 38582 Texas 04004 Maine Massachusetts MA136 Maryland New Jersey 167 Massachusetts New Jersey M-NJ141 Massachusetts M-MA136 Florida M-FL946 Missis s ippi Florida Monta na New Jersey Massachusetts New Hampshire (NELAP) Massachusetts 250204 New Jersey (NELAP) New Jersey 12129 Massachusetts MA926 Florida FL002 22 Agency Laboratory Facility Laboratory ID# New York (DOH) (NELAP) Massachusetts 11791 New Jersey 10983 North Carolina Florida 573 Ohio Voluntary Action Program New Jersey CL0056 Oklahoma Texas 9103 Florida 9959 Pennsy lvania (NELAP) New Jersey 68-408 Rhode Island New Jersey 00176 Massachusetts 00071 South Carolina New Jersey 94009001 Florida 96038001 Tennessee New Jersey 02863 Texas (NELAP) New Jersey Tl 0704234-06-TX Texas TI 04 704220-06-TX Utah Gulf Coast 7132714700 Virginia New Jersey 00004 West Virginia New Jersey 329 Wisconsin Florida 399063370 New Jersey United States Army Corp Massachusetts HTR W Center of Of Engineers (USA COE) Florida Expertise Texas Naval Facilities Engineering Florida Service Center Massachusetts New Jersey S-53041 US Dept. of Agriculture Massachusetts S-56483 (Foreign Soils Permit) Florida S-56027 Texas S -61939 Note: Accutest routinely analyzes non-potable water, soil , and air samples in states not listed above. Many states only maintain a drinking water certification program. 23 • D D ,,· Accutest State Certifications WA OR WY co AZ NM AK HI Certified Acce pted (DW On ly, NA fo r NP Water , Soi l, Ai r) Not Cert ifi ed (Accut est can acq uir e cert in 30-60 days) ND SD • Laboratory 0 Sa les/Serv ice Center DE MD DC MA RI CT Experience (E ngi neeri ng Firms) Project Type Project Description Engineering Firm Location Multiple UST/Remediation/Treatment Projects in a I 2 state area. Analysis for complete range of analytical parameters . NPDES Coordinated s a mple management planning to process over 2,000 1. RCRA samples per month. Installed and trained client personnel on New Jersey ISRA proprietary LabLink® system for data access and project management. Extensive e lectronic deliverables for data management and integration. Multiple Remediation/Monitoring Projects Multiple RJ /FS, ISRNECRA , UST, RCRA projects throughout New Jersey and 2. R I/FS New York . TC L/TAL, priority po II utan ts, appendix IX New Jersey ISRA parameters utilizing EPA 500, 600, 8000 and SW-846.methods. Extensive electronic deliverables for data management and integration . Site Investigation/Remedial Investigation for Major Airline RIFS Large on-going Site Investigation/Remedial Investigation In 3. S I support of on-going construction activities. Full TCL/TAL New York analysis utilizing SW 846 methodology and deliverables . Expedited TAT, custom EDD , 3•<l party validation. Multiple RIFS Activities for 25 Federal Aviation Administration Sites . Data reported according to USEPA and 4. RIFS NJ Site Remediation Laboratory Deliverable formats. Full Connecticut NPD ES TCL/TAL analysis with custom reporting limits. Highly visible and re g ulated site requirin g legally defensible data. Massachusetts Turnpike Authority, Central Artery Big Dig 5. Concentrated effort to process 3000 post-excavation samples for Massachusetts RCRA a full s uite of analys is. 48-72 hour TAT. LabLink used to electronically transfer the d ata for immediate validation and use. Remedial Investigation at Former Chemical Manufacturing Site. Analysis of soil and water included method development 6. RIFS for GC/MS SIM analysis to reach extremely low detection limits Delaware re quired for site-specific compounds. Data provided in custom electronic format. Vapor Intrusion Study at Multiple Sites. Analysis by Method T0-15 for indoor air a nd soi l gas. Lab provided certified 7. RCRA Summa Canisters and analyzed for a custom compound I ist. New York Proj e ct required rush turnaround, full data deliverables and electronic data deliverables. Kentucky Natural Resources and Environmental Protection Cabinet Underground Storage Tanks (UST) Program for over 8. RCRA 300 s ites in Eastern Kentucky . Analyzed groundwater and soil Kentucky UST s amples for BTEX , PAHs, Metals and RCRA Characteristics utilizing SW-846 methods. Analyzed over I 000 samples in a 4 month period, a ll of which required expedited turnaround. 25 Experience (Engineering Firms) Project Type Project Description Engineering Firm Location RIFS Multiple Remediation/Monitoring Projects Multiple Rl/FS , RCRA UST, RCRA projects throu g hout New Jersey and New York. 9. NPDES TCL/TAL, priority pollutant parameters utilizing EPA 500, 600 , New Jersey BROWN 8000 and SW-846. Ex tensive electronic deliverables for data FIELDS management and integration. Remediation/Monitoring Project Soil remediation and 10. RIFS groundwater monitoring for a major aerospace company. SW-846 Pennsylvania RCRA methods meeting PA ACT 2 requirements. Full deliverables and EQUIS EDD. Multiple Superfund RIFS Activities for large Utility Company 11. RIFS Full TC L/TAL analyses for Superfund sites in Puerto Rico, North Georgia CLP Carolina and Florida. Full deliverables and extensive electronic deliverables. Large RIFS under both EPA and NYSDEC Oversite Highly 12. RIFS visible s ite requiring daily sampling for volatile organics over a New York NYS ASP three month period . Seven-day turnaround , NYS ASP protoco I. LabLink delivered all data via auto e-mail. RIFS Brownfield Redevelopment Project Highly visible Brownfield 13. RCRA Site. Expedited analysi s for priority pollutant compounds, waste New Jersey BROWN clas sification and general chemistry parameters. LabLink FIELDS electronically transferred data via auto e-mail. Site Inv estigation/Remediation Soil and groundwater RIFS investi gation for F011une 50 Manufacturing Company. Full 14. ISRA TCL/TAL analyses with emphasis on hexavalent chromium New Jersey anal ys es . Project included treatability and leaching studies . Custom client EDD. 26 Project Type 1. 2. 3. 4. 5. 6. NPDES RCRA RCRA NPDES RCRA RCRA ISRA NPDES RIFS RCRA RCRA NPDES Experience (Industrial Projects) Project Description Corporate Contract Covering 3 Regions/] 2 States Analytical services for east coast petroleum sites (>500) involving UST/remediation and treatment projects. Extensive management of multi-state regulations, methodologies and deliverables. Sample m a nagement coordination of samples, supplies and transpo11ation to multiple consulting/engineering firms. Instrumental 111 maintaining full compliance with regulatory permits. Rated as one of the top labs in the laboratory program based on qua11erly performance activity reports. Petroleum Refinery, St. Croix US Virgin Islands Large, on- going sampling and analysis program requiring Full Appendix IX and Appendix Ill analyses as pa11 of a RCRA Facility Investigation (R.Fl) and RCRA permitted land and wastewater treatment unit monitoring. The collection of Accurate, Valid, and Representative data was of the utmost importance in order to determine the chemical and physical nature of the groundwater and to demonstrate than no migration of hazardous constituents was occurring from the treatment units. Due to the large numbers of samples being taken during each sampling event, customized, preprinted chains of custody and sample bottle labels were supplied to the client in order to minimize time spent in the field. As many as I 0-20 coolers filled with sample containers were prepared and shipped within 24 hours notice to accommodate emergency response sampling at the facility. Petroleum Refinery, linden, NJ Analytical services in support of the Bayway Refinery . Analyzed groundwater and soil samples for petroleum based contaminants including full TCL/TAL. Full and reduced deliverables. Custom electronic deliverables . Third pa11Y validation. Electric & Gas Company Extensive contract to support the Materials Management Group. Analytical services for MGP sites and facilities . Contract also includes emergency response and field sampling . Analysis of soil and water for Full TCLITAL with emphasis on Hexavalent Chromium analysis. Special method modification and development to meet client needs. Custom electronic deliverables. Custom Waste Analysis to Support Pharmaceutical Manufacturing Facility, as well as Routine NPDES Monitoring Custom analysis and reporting limits to expedite disposal of solvent waste. Data delivered in 24, 48 and 72 hours . Extensive project management and custom electronic deliverables. LabLink critical tool for access to rush data . Engineering Firm Location Major Petroleum Company Texas Major Petroleum Company New Jersey Major Petroleum Company Texas Utilities Company New Jersey Major Aerospace & Defense Contractor New Jersey Major Pharmaceutical Manufacturer New Jersey 27 Experience (Industria l Projects) Project Type Project Description Engineering Firm Location Blanket Analytical Contract for Large Aerospace RI/FS Manufacturer Contact includ es Corporate R e m edi ati o n and Large 7. RCRA Facili ty Env ironm e nta l M a nage m e nt. Full TCL/T AL, Appendi x Industrial IX a nd RC RA a na lys is . Ex te ns ive d evelo pme nt o f e lectroni c Manufa cturer d e livera bl e fo r integrati o n into cli e nt d ata base . Fi e ld sampling N ew Y o rk se rv ices s uppl ie d upon requ es t. RIFS Multiple RI FS/RCRA s ites throughout the mid-west. An a lys es Utilities 8. RCRA o f soil a nd g round wate r for full TC L/TAL. Sta te -s pe cifi c Company m ethod s utili zed as need ed . C ustom e lectroni c d at a d e li verables . Indi a na RCRA Texas N atural Resource Conservation Commission An a ly tica l TN RCC Field 9. NPDES Se rv ic es C o ntrac t In s uppo1t of Fi e ld Operation s Di v is ion . Operations UST Prog ram s include UST , RCRA , and NPD ES , utili z in g E PA 600 Division a nd 8000 S e ri es M etho d s. Texas Exten s iv e Sampling and Analys is Contract for /02 Major RIFS Groundwater Wells fo r reg ul atory compli a nce. Full TC L/T A L Pharmaceutical 10. RECRA a nal ys is of wate r a nd so il s ampl es durin g RIFS ac ti v ities. Company Hi g hl y v is ibl e s it e re quiring 3rd party va lidation . Custom e lect ro ni c d e li ve rabl es. N e w Jersey RIFS Superfund Site in West Palm Beach Ex clu s ive la bo ratory Large 11. RCRA co nt rac t to s uppo rt R l/FS activi ty. A na lyzed o ver 1800 sampl es Aerospace NPDES fo r full s uite of a na lys is. Exte ns iv e PCB studi es. E PA Manufacturer CLP M ethod o lo gy, full d e li ve rabl es. Florid a N PDES Groundwater Monitoring S a mpling a nd ana lys is o f 70+ g round wate r moni to rin g we lls for regul atory compliance . Chemical 12. NPDES A na lyzed fo r priori ty polluta nts a nd general ch e mi stry param e te rs Manufacturer RI/FS utili z in g E PA 600 sen es m e thods . Vol atil e o rgani cs w e re a na lyzed by E PA m ethod 52 4.2. Automate d compute ri ze d state New Je rsey fo rm s we re generate d for s ubmitta l to NJD E P N PDES Groundwater Monitoring Sa mplin g and a na lys is o f 6 2 g roundwat e r mo ni to rin g we ll s for regul a tory compli a nce. Petroleum 13. NPDES A na lyzed fo r pri o rity pollutants a nd g en e ral c he mi stry Company pa ramete rs utili z in g E PA 600 se ri es m e thods . A utom at e d New Jersey compute ri zed state form s gene rated for submittal to NJDE P . American Petroleum Institute Study A ir a n a lys is to d e te rmin e vapor recove r unit pe rform a nce fo r 19 HA P/N on-H A P American c ompo und s utili z in g E PA M ethods 18 , T0-3 a nd T0-14 w ith Petroleum 14. CAAA s umm a c ani s te rs. Study was c a rried out on be ha lf o f th e AP! in Institute conjun c tion w ith Shell Oil Comp a ny and Mobil Oil Company Was hin gt o n, e ncompass in g do ze ns of petrol e um t e rmin a ls th ro ug ho ut th e Un ite d States . Pa rt ic ip a nt s c omprise d o f m ajor o il c ompa ni es DC w ithin th e AP! net wo rk . 28 Experience (DOD Projects) Project Type Proj ect Description Engineering Firm Location Department of the Airforce, Airforce Center for Environmental Excellence Multiple RIFS , SI and Groundwater Monitoring Engineering Programs at Cape Canaveral . 600 samples analy z ed on an 1. DOD expedite d bas is for TCL Volatiles and EPA Method 8310. Firm Provid e d re duced CLP deliverables package and an E RPIMS Florida EDD. Department of the Navy, Southern Division Navy Clean Contract 1600 samples analyzed according to NFESC protocol. Engineering 2 . Anal y ses included Full TCL/TAL and EPA Method 8330. Firm DOD Provid e d le vel II I d e ! iverab les and a custom electronic deliverable . Sites include NAS Cec il Field , NAS Jax , NAS Key Pennsylvania West, NTC Orlando, NAS Pensacola, and Eglin AFB. Department of the US Navy, Northern Division Navy Clean Contract 500 samples analyzed according to NFESC protocol. Engineering 3. DOD Full TC L/TAL , EPH/V PH , and Low Level VOA, SVOA and Firm PCB anal ys is. Provid e d level I and II deliverables and a custom Pennsy lvania electronic deliverable . Sites include Earl AFB , NSB New London , NWIRP Bedford , NAS South Weymouth. Department of the Navy, Atlantic Division Navy Clean Contract RIFS activities at Camp Lejuene, USN Cherry Point, Engineering 4. DOD and Yorktown Naval Weapons Station. Data electronical ly Firm tran s ferred via LabLink to expedite the validation of 250 Georgia samples. Department of the Army Corp. of Engineers, Savannah District Multiple RIFS activities on Air Force Base s in Florida and Puerto Engineering 5. DOD Rico . 60 samples analyzed for full TCL!f AL analysis according Firm to USACOE protocol. Third patty validators accessing and Tennessee tran s ferring fi les via LabLink. Department of the Army, Natick R&D laboratories Analytical Engineering 6. DOD to suppo1t Fi e ld Site Investigat ions, Treatability Studies and Firm Groundwa ter Monitoring. Analyses included full TCL+, Mercury. Mas sachusetts Department of the Navy, Southern Division Navy BRAC Engineering Contract Expedited 300 samp les for Full TCL/TAL. 7. DOD Electronically tran s ferred custom deliverable via LabLink to Firm expedite validation . Level II hard copy de liverable requirements. Georgia Regulatory Compliance Sampling and Analysis throughout Naval Air Station. Sampled groundwater monitoring wells , Nava/Air 8. wastewater grab and 24-hour composites, soil and waste drum Station DOD samples . Analyzed for priority pollutants , waste classification and gen e ral chemistry parameters utilizing EPA 600 and SW -Massachusetts 846 8000 series methods. 29 Experience (DOD Projects) Project T y pe Project Description Engineering Firm Location US A rmy Corps of Eng in eers Fo rt W in gate, New M e x ico, s ite Eng ineering 9. in ve stigatio n : Ex ped ited 150 sampl e s for Full T C L/TA L plu s Firm DOD Ex pl os ives. F ull leve l IV ha rd copy p lu s Electron icall y transferred c ustom de li verabl e to ex pe d ite d ata valid ati o n . Texas us A rmy Corp s of Eng ineers Fo 1t H a mil ton, NY s ite Eng ineering 10 . DOD in ves t igat io n . F ull a nd re du ced NY State AS P de li verabl es . Firm A na lys is ofTC L , TAL param eters. New Yo rk Department of th e A rmy, Chicago District T reatabili ty Study for Eng in ee ring 11. DOD t he Ind iana Harbo r Confi ned D is posal Faci li ty. A na lysis inc lud e d Firm Full TCL/TAL us in g SW846 M etho d o logy. M isso uri US A rmy Corps of En g in eers In a pe ri o d of t hree m o nt hs, several hund re d sa mpl es we re a na lyzed fo r TCL/TAL param eters, Engineering c hemi ca l wa rfare degradati o n by pro ducts, exp losives an d general 12 . DOD chem istry param ete rs. T he sampl e m atri ces in c lud e d so il , water, Firm fis h worm s a nd vegetat io n. T hird party valid ati o n and extens ive Ma ry land data de li vera bl es were re qui red fo r thi s p rn ject. US A rmy Corps of En g in eers, Philadelphia District. Ind e finit e Arm y Corps of de li very contract fo r several la rge scale in vestigatio n and 13 . DOD re med iat io n projects wi thin th e d istr ict. Provide fu ll d at a Engineers de li verab le packages, SE DD E DD and A DR E DD . Phil ade lphi a 30 Miscellaneous Health and Safety Accutest operates a formal health and safety program that complies with the requirements of the Occupational Health and Safety Administration. Accutest's goal is to provide a safe and healthy working environment for its employees and clients while protecting the public and preserving the Company 's assets and property. The Company complies with all applicable government regulations pertaining to the safety and health in the laboratory and the workplace . The objective of the Accutest Health and Safety Program is to promote safe work practices that minimize the occurrence of injuries and illness to the staff through proper health and safety training, correct laboratory technique application and the use of engineering controls. The program consists of key policies and practices that are essential to safe laboratory operation. All employees receive training on the program elements. Job specific training is conducted to assure safe practices for specified tasks. All employees are required to participate in the program , receive initial and annual training, and comply with the program requirements. Waste/Sample Disposal Laboratory waste (i.e., chlorinated and non-chlorinated solvents, GC-GC/MS extract vials) are properly manifested , transported and disposed of following all EPA and state regulations . All hazardous laboratory samples are properly manifested, transported and disposed of following all EPA and State regulations. 31 Insurance Profess ional Liability (E&O) General Liability Excess Liability (Umbrel la) Employer's Liability / Workers Comp. Auto Liability Small Business Classification $2,000,000.00 $1,000,000.00 I $2,000,000.00 aggr. $5,000,000.00 $1,000,000.00 $1,000,000.00 Accutest is classified as a small business (<500 employees) as defined by the Federal Government NAICS 562910 Environmental Remediation Services procurement guidelines. Affirmative Action Accutest is an Equal Employment Opportunity (EEO) emp lo yer. Accutest maintains a current Affirmative Action certificate (#4693) filed with the State of New Jersey Dun & Bradstreet DUNS: 01-154-8195 Financial Rating: 4A 1 This is the highest possible financial rating for a company our size. 32 Accutest Laboratories Environmental Analytical Capabilities >, "C --C: (/) (/) Cl) ns ns ns (/) 0 Cl) ... O') Cl) Capabilities (.) .£: -, C: -w ~ :::s 3: :::s 0 3: (!) Cl) Cl) Cl) z z • • • • • • • • • • • 8 Page 90 of 91 Revision Date: June 26 , 2006 Revis ion II Accutest Laboratories Equipment List Organic Instrumentation Instrument Manufacture & Description Serial Number Purchase GC/MS Hewlett-Packard 5970MSDlfekmar P&T/4552 01 AS/5890 2923A 12433 HPGC 1990 GC/MS Hewlett-Packard 5971 MSD/ Ol / 4552 01 AS/5890HPGC 3234A03983 1993 GC/MS Hewlett-Packard 5890 GC/HP5971 MSD/7673HP AS 3223A43695 1993 GC/MS Hewlett-Packard 5972MSD/HP5890 GC/HP7673AS 3501A02354 1999 GC/MS Agilent Technologies 6890N MSD/ 4552 01 AS/01 P&T US10251065 2003 4560 GC/MS Agilent Technologies 6890N MSD/ 4552 01 AS/01 P&T US40646501 2004 4560 GC Hewlett-Packard 5890GC/Ol 4552AS /014560 P&T/01 3203A41760 1999 PID ,PID GC Hewlett-Packard 5890GC/OI PID/FID/014560 P&T/4551A 3235A 44696 AS 1999 GC Hewlett-Packard 5890GC/F1D/7673A AS/7673A Controller 2750A 15605 1988 GC Hewlett-Packard GC/Dual ECD/7673A AS/7673A Controller GC Hewlett-Packard 6890 GC/Dual FID Agilent 6890/ 01 G1513A AS GC Hewlett-Packard GC/Dual ECO/ 7673 AS/7673 Controller Metals Instrumentation Instrument Manufacture & Description ICP CV T JA Enviro Trace 61 E Simultaneous Leeman Labs Inc., Hydra AA Automated Mercury Analysis System #1 Wet Chemistry Instrumentation Instrument Manufacture & Description Auto Anal. Alpkem -RFA2 Auto Anal. Technicon AAII Wet Chemistry Instrumentation: (cont.) Instrument TOCAnal. TOXAnal. Manufactu re & Description Shimadzu TOC-VCSN Mitsubishi TOX-10E 2843A20813 1989 US00002475 2001 2643A11566 1987 Serial Number Purchase 268490 3013 1994 2003 Serial Number Purchase 86007 001050 1989 1986 Serial Number Purchase H51204235074 2005 75C01202 1992 IR Spec Miran 1 Foxboro DO Meter YSl-508 UWIS Spec Milton Roy 20-D PH Meter Orion 230A PH Meter Orion 710A+ PH Meter Orion 520A Purchase UWIS Spec Milton Roy Spectronic 501 Chlorine Meter Hach DR 100 Colorimeter 41100 Page 91 of 91 Revision Date : June 26 , 2006 Revision II MIE5454K055 93C03605 3DU8192042 005013 070160 005401 3604197010 5022 1992 1991 1989 1992 2003 1994 1995 1982 Accutest LabLinksM As a standard part of our analytical data services, Accutest offers LabLink, a complete on- line data service with power and ease of use that is unprecedented in our industry. From the minute your samples are received at Accutest, LabLink gives you up-to-the-minute access to project information right from your PC via our secure website. The Most Comprehensive On-Line Service in the Industry Accutest's LabLink service will save you time , effort and money. We have made a long term commitment to provide the most comprehensive on-line service in the industry. Co nsider the features that are already available in LabLink today: • Automated Sample Receipt Confirmation: Allows you to confirm that your samples have arrived at the lab safely and have been logged in properly . This ensures the correct te sts, samples ID 's, TA T's, etc. Your chain of custody arrives with the log-in report for review. • Complete Project Status Information: From the minute your sa mples are received at Accutest, you have comp lete access to job, sample, and test information. In addition, status information is available in rea l time, allowing you to follow the progress of your sa mple s. • On-line Chain of Custody Documents: As part of sample login, chains of custody documents are scanned into PDF files that are available on-line to LabLink users with a single click. • Immediate Access to Test Results: LabLink provides complete access to test results the minute they are approved by the laboratory (no more waiting for verbal results or faxes). The LabLink data query provides powerful options (like hits only) to get the answers you need as quickly as pos si ble. You can also compare your results to a variety of State and Federal regulatory limits. • Access to Quality Control Data: Method blank, MS/MSD, blank spike and surrogates are available on -lin e. You can also review chromatograms, spectra and other raw data . • Historical Data Query: With LabLink, it is just as easy to view historical data. Powerful query options and sort criteria can be specified and executed in seconds to look for trends. • e-Hardcopy Reports available via auto-email or on-line: Finished data may be generated in e-Hardcopy format complete with signed cover page , chain of custody and comprehensive QC reports . LabLink allows the user to enable Auto-Email on projects of interest, such that an e-Hardcopy report will be sent automatically on completion of a job. Accutest LabLinksM • Billing / Invoice Information: LabLink even allows access to preliminary billing information . This allows you to check quote prices before you have an invoice in your hands. In addition , hi sto rical billing information is maintained , allowing up-to-the-minute project financi a l summaries. Fina l invoices may even be downloaded on demand in PDF format. • Electronic Deliverables on Demand: Electronic data deliverables (EDD's) may be generated on demand through LabLink. This capabi li ty is unprecedented in the industry. How to Get On-Line? Getting started with LabLink couldn 't be easier. A ll you need is access to the Internet. We will set you up with a secure LabLink account and you'l l be on-line. Best of all, access to Lab Link is provided at no additional charge simply for doin g business with Accutest. Lablink'" 2 .7 PROVIDER'S PERSONNEL QUALIFICATIONS AND EXPERIENCE 2. 7 .1 Provider should complete a matrix including the following information detailing the providers relevant personnel , their qualifications , and years of experience. • Position Title and Job function as associated with this contract, (Laboratory Managers, Technical Managers, QAQC Managers/Supervisors, Project Managers, Chemists, Lab Techs, Customer Service Representatives, Etc.) • Name • Certifications/Licenses • Total Years Experience • Years of Experience with Provider If a single individual fulfills more than one position then provide the relevant years of experience for that position . 2.7.2 Provider should submit a brief resume (one page maximum , 1 Opt type minimum) of each professional person who will be assigned to this contract. Identify key persons by name and title and describe the primary work assigned as associated with this contract. INCLUDE A COPY OF THE ABOVE DOCUMENTATION FOLLOWING THIS PAGE BOUND WITHIN THE PROPOSAL PACKAGE 2-11 2.8 ORGANIZATIONAL CHART Provider shall include an organization chart depicting contact arrangement from the City to the Provider, from the Provider's representative to other areas w ithin the Provider and from the Provider to any subcontractors. INCLUDE A COPY OF THE ORGANIZATION CHART FOLLOWING THIS PAGE BOUND WITHIN THE PROPOSAL 2-12 Employee Name Job Title Benedicta Bigtacion Analyst Lien Nguyen Analyst Nidia Saspa Analyst Luis Racelis Technician Sheila Cheng Analyst Rochelle Child Analyst Tim Smith Analyst Zandra Holbrook Analyst Jennifer Hoang Analyst Lyida Jasso Analyst Felix Oses Analyst Richard Rodriguez Team Leader Charles Hardesty Team Leader Jim Low Technician Melissa Contreras Technician Ena Fields Technician Tamara Snowden-Welch QA Officer Ron Martino Laboratory Director Alisha Rodriguez Supervisor Dan Borak Driver Cassie Escotto Technician Accutest Laboratories -Gulf Coast Technical Staff Biographies Department Degree Degree Year General Chemistry BS 1976 General Chemistry BS 1989 Metals Analysis BS 1976 Metals Prep BS 1967 Semivolatile Organics MS 1977 Semivolatile Organics BS 2003 Sem ivolatile Organics BS 2006 Volatile Organics BS 2000 Volatile Organics BS 1991 Volatile Organics HS DIPLOMA 1989 Volatile Organics AAS 1997 Organic Supervisor BS 1987 Organic Prep BS 1987 Organic Prep PhD 1973 Organic Prep HS DIPLOMA 2000 Organic Prep/Glassware HS DIPLOMA 1989 Quality Assurance BS 2005 Laboratory Management BS 1989 Sample Management HS DIPLOMA 1997 Sample Management HS DIPLOMA 1992 Sample Management HS DIPLOMA 2005 Major Chemistry Chemistry Chemistry Chemical Engineering Chemistry Chemistry Chemistry Biology Biology Electrical Engineering Agriculture Maritime Administration Chemistry Chemistry Chemistry Professional Experience {Yrs) Hire Date 1 2007 26 1994 13 2005 6 2001 19 2001 2 2004 9 2006 1 2005 15 1992 17 2004 6 2004 12 2004 5 2004 30 2004 3 2006 1 2005 5 2006 20 2000 6 2005 3 2005 >1 2006 RONALD S. MARTINO Laboratory Director Accutest Laboratories Gulf Coast, Inc. Houston, Texas Mr. Martino is responsible for day to day laboratory operations at Accutest's Gulf Coast laboratory in Houston, TX. Accutest Gulf Coast specializes in the analyses or organics and inorganics in water, soil and sediment matrices. He has supervisory responsibility for all personnel. This includes responsibility for all departments. Mr . Martino's analytical experience includes all environmental analyses performed at Accutest Gulf Coast. Mr. Martino initiates all equipment purchases, develops and implements new methodology, oversees all production efficiency, and approves all data in compliance with Accutest's QA/QC guidelines . Previously, Mr. Martino has 12 years experience as an organic analysts and supervisor as well as three years experience as a project manager . EDUCATION MS, Environmental Management, University of San Francisco Pending BS, Chemistry, Cal Poly San Luis Obispo CONTINUING EDUCATION • OSHA HAZWOPER 40-hour Certified, February 2000 PROFESSIONAL EXPERIENCE Severn Trent Laboratories -St. Louis, Project Manager, 1999 -2001 • Oversee the project specifications and intricacies. Communicate the clients analytical and turn around time needs to the laboratory and the laboratory capabilities to the client. • Manage DOE, DOD and commercial client projects through the US and South America. • Report and data package review of final product. • Review and comment all RFP and contracts before laboratory acceptance. • First contact for all call in clients. Gather project information and specifications, . then create price quotations . Also, follow up with the quote for acceptance or rejection. Document losses to CSM for trending and/or market fluctuations . • Participate in all forecasting of client revenue, respond to RFP with pricing and laboratory qualifications, and advise operations on forecasted revenue to determine what departments will be impacted for both instrumentation and personnel expectations. Rev. 08/09/06 RONALD S. MARTINO Laboratory Director Accutest Laboratories Gulf Coast, Inc. Houston, Texas GC/MS Supervisor • Oversee the operations of the GC/MS department. • Performed all managerial responsibilities associated with the operations of an analytical department within the environmental laboratory including hiring, training and reviewing all associates, budget adherence and trouble shooting of instruments . • Analysis of volatile and semivolatile organics using the various GC/MS methodologies. • Second review of GC/MS and GC data. ACZ Laboratories, Organic Supervisor, 1994-1998 • Oversee the operations of the extraction and analysis for all organic analysis. This included the setting up of instrumentation, training of associates, data review and adherence to all QA/QC procedures. • Analysis of volatile and semivolatile organics through GC/MS, pesticides and PCBs and fuels through GC, Explosives and Polynuclear Aromatics by HPLC while following RCRA, CERCLA and drinking water protocols. • Performed all managerial responsibilities associated with the operations of a analytical department within an environmental laboratory including hiring, training, reviewing all associates, budgeting, trouble shooting instruments, etc. • Principal Achievements: Automation of reports, increase production from 400K in 1994 to 688K in 1996 with 5 associates, and 90% or better scores on all WP and WS studies. GTEL , Environmental Laboratories, Inc ., Semivolatile Manager, 1993-1994 • Over see the operations of the extraction and analytical laboratory for the semi and non-volatile organic analysis. This included the setting up of instrumentation, training of associates, data review, and adherence to all QA/QC procedures. • Analysis of volatile and semivolatile organics through GC/MS; pesticides and PCBs and fuels through GC while following RCRA, CERCLA, and drinking water protocols. • Performed all managerial responsibilities associated with the operations of an analytical department within an environmental laboratory including hiring, firing, training and reviewing associates, budgeting, trouble shooting instruments, etc. • Principal Achievements: Increased production from 785K in 1993 to 1.2 million in 1994 with 9 associates . Certified the semivolatile department for DOD and DOE work and successfully changed the sample make up from UST work to CERCLA and RCRA work. Rev. 08/09/06 1 RONALD S. MARTINO Laboratory Director Accutest Laboratories Gulf Coast, Inc . Houston, Texas Assistant Laboratory Director, 1992-1993 • Operations manager at GTEL. This included purchasing of equipment, budget review and adherence, projection of capacity and work load, client inquiries and presentations, quality assurance programs, and the hiring and performance reviews of all 50 associates. • Wrote and reviewed all QAPPs, including the sampling plan, to insure that the laboratory met the needs ·of the clients . • Oversaw the certification of GTEL for DOD contracts from the Department of the Navy and USACE. GTEL Concord and GTEL Torrance, GC/MS Supervisor, 1989-1992 • Oversee the analysis of all GC/MS organic analysis. This included the setting up of instrumentation, training of associates, data review, and adherence to all QA/QC procedures . • Performed all supervisor responsibilities for both GC/MS departments for both the Concord and Torrance facilities. TMA Norcal , Chemist, 1987-1989 • Extraction and analysis of all types of organic analysis within the CERCLA and RCRA protocols. • Analysis included: Pesticides and PCBs, semi-volatile and volatile GC/MS, fuels through the California LUFT manual. Rev. 08/09/06 TAMARA WELCH Quality Assurance Officer Accutest Laboratories Gulf Coast, Inc. Houston, Texas Mrs. Welch has recently joined Accutest, and is currently Accutest Laboratories Gulf Coast Quality Assurance Officer. She is responsible for the facility's adherence to Accutest's corporate quality assurance program. She generates summary sheets and various reports for clients on a regular basis in addition to generating EPA reports as required for certain projects . EDUCATION B.S. Science, Grambling State University PROFESSIONAL EXPERIENCE Severn Trent Laboratory -Houston, TX 2001-2006 Safety and Quality Assurance Assistant • Assist the Employee Health and Safety Coordinator with responsibility for administering the EH&S program that provides a safe, healthy working environment for all employees and the environment. Monitors all areas for unsafe conditions, acts, and potential hazards. Enforces environmental, health, and safety policies and procedures. Maintains regulatory compliance with local, state, and federal laws . Make safety and health recommendations to laboratory management in conjunction with the facility safety committee . • Assist the Quality Assurance Manager during audits and client visits, maintains reference data, and performs spot audits internally at the request of the QA Manager. Performs customer service requests for Project Management staff, supplies Standard Operating Procedures (SOP), certification information, and method information. Requests, compiles, and enters Method Detection Limit study information for each test method in the laboratory. Works with the laboratory to maintain SOP's. Data Package Technician •:• Use data provided by various analytical groups, prepares complete and accurate client report packages in accordance with contract compliance, Severn Trent Laboratories Quality Assurance practices, Standard Operating Procedures, and client requirements . Asst. Supervisor of Sample Administration Rev. 08/09/06 •!• Responsibilities include providing assistance with planning, directing, and coordinating activities in the department. Strong, dynamic interfacing with co- workers and clients. Able to interact with all levels of management. Rev. 08/09/06 PENG-SHIA WEI CHENG Organic Mass Spec. Analyst III Accutest Laboratories Gulf Coast, Inc. Houston, Texas Ms. Cheng has been with Accutest Laboratories Gulf Coast, Inc. since 2001. As OrganicMass Spec . Analyst III, she effectively manages the daily operations and sample analyses in the GC and GC/MS Semi-Volatile areas. Ms. Cheng also coordinates with the organic extractions department to efficiently schedule analyses in a joint effort to meet and exceed all turnaround requests . She currently performs the analyses of various sample matrices for Semi-Volatiles by SW-846 method 8270C and EPA methods 625 as well as Total Petroleum Hydrocarbons by TX-1005. Also analyze DRO water and soil samples by EPA method 8015 . Ms Cheng also coordinates method implementation, performs data review and generates organic data packages in addition to training new and current personnel. EDUCATION M .S. Chemistry, University of Texas at El Paso, May 1977. B.S . Chemistry, Chung-Yuan College of Science & Engineering, July 1973 PROFESSIONAL EXPERIENCE Southern Petroleum Laboratories -Houston, Texas, Senior GC/MS Chemist 1999- 2001 • Performed the analysis of samples of various matrices including water, soil and hazardous waste semi-volatile organic compounds following EPA CLP protocols, SW-846 methodology and the method 625 and 8270. • Implemented the procedures for providing rapid turnaround analytical services with a 24 to 48 hour turnaround time. • Proficient in the operation of the following GC/MS instruments: HP-5971, 5972 and 5973 (HP UNIX Stations). Recra LabNet -Houston, Texas , GC/MS Supervisor (12/1996 -10/1998) • Supervised the daily operations and sample analysis activities in the GC/MS department including sample scheduling, personnel evaluation and training, new analytical procedures implementations, SOP preparation, data review and data package production. Quality Control/Data Review Chemist (5/1994 -12/1996) • Responsible for reviewing GC/MS data packages to ensure QA/QC compliance with the client/project requirements, including those generated under the EPA Special Rev. 08/09/06 Analytical Service (SAS) program. Rev . 08/09/06 1 , J • Other duties included the training of new analysts, routine instrument maintenance and mass spectral interpretation . Senior GC/MS Chemist (9/1987 -4/1994) • Performed the analysis of samples of various matrices including water, soil and hazardous waste volatile and semi-volatile organic compounds following EPA CLP protocols , SW -846 methodology and the method 624, 625, 8240, 8260, 8270 , 524 .2 and 1625 . • Implemented the procedures for providing rapid turnaround time analytical services with a 24 to _48 hour turnaround time. • Proficient in the operation of the following GC/MS instruments : HP-5972, (HP Chem Station), Finnigan 4000, 4020, 4510, 4530, 5100 and INCOS 500. Rev . 08/09/06 JENNIFER N. HOANG GC/GCMS Analyst Accutest Laboratories Gulf Coast , Inc. Houston, Texas Ms. Hoang 's primary responsibility is analyzing water/soil samples using EPA/SW- 846 Methods 8260B/624/8015B/8021B and maintaining all instrument GC & GC/MS in VOA group . EDUCATION University of Houston -Central Campus, Houston , TX , 1991 Bachelor of Science in Biology with Chemistry Minor CONTINUING EDUCATION Restekduction Intro to Capillary Chromatography PROFESSIONAL EXPERIENCE Maxim Technologies , Inc., Houston, TX, 1992 -Present -GC Analyst Jennife r joined Maxim Technologies, Inc . in April, 1992 . Her current responsibilities include the operations and maintenance of Gas Chromatographic equipment employed in the analysis of various environmental samples from the petroleum and agricultural industries for compounds such as PCBs, pesticides, herbicides, and trace level petroleum products in water, soil and air samples . Prior to her transfer to the GC department, Jennifer was a wet chemistry analyst. She was responsible for all solid analysis, such as total dissolved solids , total suspended solids, total solids, etc . She was al so responsible for analyzing total & extractable organic halogens using a total organic halogen analyzer and total organic carbon using a total organic carbon instrument. Jennifer was also proficient in other wet chemistry analysis, such as fluoride, alkalinity, surfactants, BOD/COD , etc. Halliburton NUS Environmental, 1991 -1992 Analyst II -Coordinated quality control, analytical procedures, documentation , scheduling , instrument calibration/operations and personnel training in a team setting for laboratory analysis of environmental samples . Conducted laboratory procedures s uch as total organic halogen s (TOX), biochemical oxygen demand (BOD), total organic carbon (TOC), chemical oxygen demand (COD), cyanide analysis, etc . resulting in compliance with client specifications and industry/government standards. Also provided formal , informal , and cross training for fellow employees in analytical testing procedures resulting in flexible teamwork, improved productivity . Rev. 08/09/06 LIEN T. NGUYEN Environmental Analyst Accutest Laboratories Gulf Coast, Inc. Houston, Texas Lien Nguyen has been with Accutest Laboratories over 9 years and works in the wet chemistry lab. Her duties are maintenance of ovens and instruments, maintaining current logbooks and calibrating scales. Her duties also include analysis for Ammonia, TKN, Total Phosphorous, Orthophosphate, Nitrate, Nitrite, Sulfate, COD, TOC, Cyanide, Phenol , Reactive Cyanide, Reactive Sulfide and Sulfide. Besides her responsibility tests, Lien has experience to perform all tests in the wet chemistry area. She also assists in the metals prep area when needed. EDUCATION University of Houston, Clear Lake, TX, May 1989 B.S . Degree in Analytical Chemistry Associate of Art -Applied Science in Chemical Technology, Texas Sate Technical Institute, Waco, Texas, September 1978 -March 1980 CONTINUING EDUCATION Laboratory Certification Microbiology of Drinking water -Texas Department of Health -Austin, Texas Laboratory calculation, Record keeping and Quality Control, -Texas Natural Resource Conservation Commission. PROFESSIONAL EXPERIENCE Maxim Technologies , Inc. Houston, TX, April 1994 -Present Environmental Analyst -Perform analytical testing of water, wastewater & solid waste, using both wet chemistry & instrumental techniques. AnalytiKEM Laboratory, Houston, Texas, July 1989 -August 1993 General Chemistry Analyst -Perform analytical testing, calibrate and maintain instruments, prepare solutions and standards and calculate results and quality control data, all of which is reviewed by the Quality Assurance/Quality Control officer for approval and also developing and validating analytical methods . Hughes Tool Company, Houston, Texas, August 1981 -April 1984 Chemistry Lab Technician -Use of various equipment and methods m wastewater treatment , copper plating and tool materials analysis . Arco Chemical Company, Channelview, Texas, March 1980 -August 1981 Chemistry Lab Technician -Performed various techniques of analytical chemistry in petro-chemical environmental: calibration, gas and liquid chromatography, use of Rev. 08/09/06 atomic absorption and general wet chemistry. Rev . 08/09/06 ALEJANDRA FRANCO Client Services Accutest Laboratories Gulf Coast, Inc. Houston, Texas Ms . Franco (Luna) has been with Accutest Laboratories for over 2 years and her duties include the following : assist Project Managers, help out in Sample Receiving when needed, Receptionist and other clerical duties. EDUCATION High School Diploma, Alief-Elsik, Houston, Texas 1990-1994 Houston Community College 1995-1996, 2002 PROFESSIONAL EXPERIENCE Accutest Laboratories Gulf Coast, Houston, Texas, 2001-present Client Services . Duties include project manager assistant, receptionist and clerical duties . Severn Trent Laboratories , Houston, Texas, 1996-2001 Project Manager Assistant. Primary responsibilities included project management assistance with heavy client contact. My duties included producing analytical reports, data validation, and management of subcontracting samples coming to and from the laboratory, data entry and general clerical duties. Rev. 08/09/06 Wet Chemistry Technician Accutest Laboratories Gulf Coast , Inc . Houston , Texas Shaguanda N. Cade Shaquanda "Nikki" Cade responsibility at Accutest Laboratories is analysis in the wet chemistry lab . Her duties are maintenance of ovens and refrigerator temperature, preparation of chemicals and standards, maintaining current logbooks and calibrating scales . Her duties also include analysis for gravemetric: Sulfate , TSS , TDS, TS and Percent Solids . Linear Regression: Hexavalent Chromium, Ortho Phosphorous and Silica . Titration : Alkalinity and Chloride . Miscellaneous : BOD, CBOD, Specific Conductance, Hardness, Calcium, Fluoride-distilled Fluoride and pH measurements . EDUCATION Wiley College, B.S . Biology PROFESSIONAL EXPERIENCE Kelly Scientific Services, Houston, Texas, January 2005 -April 2005 • Lab Technician -Analysis of gasoline and diesel fuels . Rev . 08/09/06 Glassw are Accu test Laboratories Gulf Coast , Inc . Houston , Texas ENA FIELDS Ms . Fields has recently joined Accutest Laboratories and her duties include the following: maintaining clean glassware for extractions , wet chemistry and metals department. She also helps out in Sample Receiving when needed and also assists the lab technicians in the extraction department. EDUCATION Willowridge High School, Houston, TX 1989 PROFESSIONAL EXPERIENCE Accutest Laboratories, Houston, Texas, Glassware & Lab Technician, present Rev. 08/09/06 LUIS E. RACELIS Metals Prep Technician Accutest Laboratories Gulf Coast, Inc . Hous ton, Texas Mr. Racelis is responsible for metals prep, scheduling, and preparation. Mr. Racelis is experienced in various metal preparation procedures : SW-846 3000, 7000 Series, and EPA 200 Series . He also assists in TCLP & SPLP extractions. Mr. Racelis's primary responsibility is analyzing water/soil samples using EPA/SW- 846 Methods 8021B and maintaining the GC in VOA group . 03/04 -05/04. Work Performed 2001-2004 : Extraction for water and soil BNA, DRO, Pesticides, PCB's, TPH -1005 and Herbicides by liquid. Liquid seperatory extraction and by sonicator . EDUCATION B. S . Chemical Engineering National University, Manila, Philippines 1967 CAD/CAM classes Houston Community College, Houston, Texas PROFESSIONAL EXPERIENCE Severn Trent Laboratories, Houston, Texas, 9/00 -9/01 Extraction Department -Organic extraction of soil and water National Engineering Service, Houston, Texas, 3/99 - 1 f/99 Designer (Foster Wheeler) Shaw Fabricator Inc., Houston, Texas, 9/98 -3/99 Piping Designer Raytheon Engineers and Constructors, Lynhurst, New Jersey, 9/90 -6/98 Designer Wynn Consultants, Friendswood, Texas, 3/99 -11/99 Piping Designer Rev. 08/09/06 CHARLES L. HARDESTY, JR. Senior Extraction Lab Analyst Accutest Laboratories Gulf Coast, Inc . Houston , Texas Mr. Hardesty recently joined Accutest Laboratory . He is responsible for efficiently extracting and preparing all samples received for organic analyses including Semivolatile Organic Compounds (SVOCs), Total Petroleum Hydrocarbons (TPH), Herbicides, Pesticides and PCBs, with strict adherence to holding time. He is also responsible for preparation of TCLP, ZHE and SPLP samples. EDUCATION Texas A&M University -College Station , Texas, 1987 Bachelor of Science Maritime Administration U.S . Merchant Marine Academy , 1979-1982 PROFESSIONAL EXPERIENCE Pace Analytical Laboratory-Houston, Texas Organic Extraction Supervisor -Managed workload and assignments for TCLP, Texas 1005 , DRO, Pesticides, PCBs, Herbicides, and 8270 extractions and concentrations. Responsibl e for ensuring deadlines and holding times were met. Responsible for ordering supplies . He was the laboratory Safety Officer . Maritime Areas of Expertise Performed all vessel cargo operations including: cargo plan layout, loading, di scharging, securing vessel documentation, supervision of long shore gangs, equipment management, and warehousing. Cargo Handling Experience Heavy lifts , containers, steel products, paper/woodpulp products, oil well supplies, reefer and general car gos . Rev. 08/09/06 ALISHA RODRIGUEZ Sample Manager Accutest Laboratories Gulf Coast, Inc. Houston, Texas Ms. Rodriguez has recently joined Accutest, and is currently responsible for sample control. Her duties include, but are not limited to, checking in of samples, preparing bottle kits , custody records, logging in samples into the LIMS system, and overseeing sample disposal. She also does some field sampling. EDUCATION H.S . Diploma -Klein Forest University of Houston-Downtown -1997-1999 PROFESSIONAL EXPERIENCE Severn Trent Laboratories -Houston, Texas, 2000-2005 Assistant Supervisor, Sample Login Dept. Oversee 3 sample technicians. Responsible for receiving and importing EPA and TNRCC testing parameters and holding times into laboratoy system and tracking up to 500 soil and water samples a day. JC Bradford and Company-Houston, Texas 1999 Sales Assistant-oriented, organized and maintained accounts for over 8 investment brokers utilizing Excel and Microsoft Word. Answered a lO+phone line system for about 30 employees. Marcom Advertising-Houston, Texas 1999 Office Clerk/Receptionist-organized daily client advertising schedules between a multiple of radio stations and commercial clientele utilizing Excel spreadsheets and Microsoft Word. Rev. 08/09/06 GCMS Volatiles Analyst Accutest Laboratories Gulf Coast, Inc . Houston, Texas 418.1, 413.2 , 8310, and 8100. LYDIA JASSO Duties included -assign and monitor sample throughput in extractions, coordinate samples with project managers, prepare standards and solutions, prepare SOPs, assisted in method development . Aqua Process Inc., Houston, Texas, 1988-1989 Lab Assistant: Performed various tests in the laboratory and assisted Chemists with research projects. Duties included -analyzed oil samples using the IR and AA instruments, performed titrations and pH tests, assisted in research. Rev. 08/09/06 '-- GC Semi-VolatileAnalyst Accu test Laboratories Gulf Coast, Inc . Houston, Texas FELIX OSES, JR. Feli x is the GC Semi volatile chemist for Accutest Labs . His duties include, but are not limited to, all ECD analyses. This includes test methods for Pesticides , PCB's and Herbicides . He is responsible for analyzing and reporting results in an accurate and efficient manner to fulfill client/laboratory deadlines. Instrument maintenance and upkeep are included in Mr. Oses ' responsibilities . In order to ensure the fulfillment of deadlines , he also communicates daily with the organic extractions department about sample prep and analysis . EDUCATION San Jacinto College , Pasadena, TX Associate in Electrical Technology, 1997 H.S . Diploma -Life Christian Academy, 1992 PROFESSIONAL EXPERIENCE Pace Analytical Services, Inc., Houston, Texas , 2000 -2004 Lead Analyst III GCSV Department: Analyzed soil, water and wastewater samples referencing EPA methods 8080/8081, 8082 , 8150/8151 , and 8011 GC Sem i-Volatiles -Analyzed soil, water and wastewater samples for Alcohol's, DRO and TPH (TX1005 and TX1006) referencing EPA methods 8015, TXI005 and TXI006. Duties included-preparation of calibration standards and samples, analysis of samples, processing and reporting samples . Organic Extraction Supervisor -performed supervisory duties in the absence of the supervisor, extracted oil, wipes, soil and water samples using methods 3510, 3520, 3550 , 8310, 8330, 9071 , 418 .1, TCLP/SPLP , TCEQ1005/I006. Duties included -assign and monitor sample throughput in extractions, manage emplo yees, order supplies as needed . Inorgan ic Experience : familiar with Mercury Analysis, TOC , Solids, and OG analyses among others . Rev. 08/09/06 Field Services Experience: prepared sample kits and performed sampling duties . Assisted in sample pickups . Rev. 08/09/06 Client Services Representative Accutest Laboratories Gulf Coast, Inc . Houston , Texas SYLVIA GARZA Ms . Garza has primary responsibility for client services/ project management. She communicates directly with clients to insure accuracy of requested analysis and sample information needed for correct reporting of results. She advises technicians of project scopes through LIMS (a sample management database) and verbally coordinates urgent deadline capacities . She also fields inquiries regarding price quotations, method citation, holding and turn-around times, sampling containers, sample preservatives, and report status . Ms . Garza has assisted sample control. Her duties include, but are not limited to, logging in samples into the LIMS system, checking in of samples , preparing bottle kits, custody records . EDUCATION Hours at Galveston Community College, Galveston, TX Science Emphasis PROFESSIONAL EXPERIENCE Pace Analytical Services, Inc., Clear Lake, Texas , 2001 -2004 Data Specialis t: Her duties included, logging in samples, checking in of samples, invoicing , subcontracting, generating and reviewing reports . SPL, Inc., Houston, Texas, 1997 -2001 Data Management and Reporting: Her duties included, generating and reviewing reports , monitoring sample data throughput , subcontracting samples and writing narratives. Pace Analytical Services, Inc., Clear Lake, Texas, 1995-1997 Reporting: Her duties included, entering data into the system, creating spreadsheets, providing EDDs and reports to clients N.U.S/Pace Analytical Services, Inc., Clear Lake, Texas, 1992-1995 Organic/Metals Prep Lab Technician: Her duties included, performed extractions for a variety of semi-volatile soil and waters, pesticides, PCBs, and PNAs . She also performed metals digestions. Rev. 08/09/06 Custodian Sample Technician Accutest Laboratories Gulf Coast, Inc. Houston , Texas J. Dan Borak Mr. Barak assists in sample control. His duties include , but are not limited to, logging in samples into the LIMS system, checking in of samples, preparing bottle kits, custody records. Rev . 08/09/06 JIMY. LOW Extraction Lab Technician Accutest Laboratories Gulf Coast, Inc. Houston , Texas Mr. Low is currently working part time in the Extraction Laboratory . He is responsible for efficiently extracting and preparing all samples received for organic analyses including Semivolatile Organic Compounds (SVOCs), Total Petroleum Hydrocarbons (TPH), Herbicides, Pesticides and PCBs, with strict adherence to holding time. EDUCATION University of North Dakota -1973 Ph.D . in Chemistry University of Missouri -1970 M.S. in Chemistry Indiana University -1967 B .S . in Chemistry PROFESSIONAL EXPERIENCE The Southern Petroleum Laboratories., Houston, Texas, 1999-2004 Organic Extraction Supervisor Supervised 11 technicians, improved moral, reduced turnover , improved on time analysis , developed and improved methods. The M.W. Kellogg Company ., Houston, Texas, 1995-1998 Principal Chemist Supervised Residuum Oil Supercritical Extraction (ROSE) Pilot Plant evaluations for clients . Managed research and development projects in support of the Kellogg's ROSE deasphalting process. Kerr-McGee Corporation., Oklahoma City, Oklahoma, 1988-1995 Senior Project Chemist Responsible for developing new processes and chemical products which included new synthetic routes for fuel additives , preparing MTBE and octane improver. Phillips Petroleum Company., Bartlesville, OK, 1977-1988 Senior Research Chemist Conducted research in hydrotreating catalyst screening at pilot plant scale, in heavy oil upgrading by using homogeneous catalyst and synfuels . SRI International., Menlo Park, California, 1976-1977 Research Chemist Evaluated homogeneous acid catalyst-super acids for coal liquefaction resulted in Rev . 08/09/06 further funding from the Department of Energy. Rev. 08/09/06 ROCHELLE CHILD GC Semi-Volatile Analyst Accutest Laboratories Gulf Coast, Inc . Houston, Texas Rochelle is the GC Semivolatile TPH analyst for Accutest Labs. Her duties include, but are not limited to,TX1005 and TX1006 preparation and analysis. She is responsible for analyzing and reporting results in an accurate and efficient manner to fulfill client/laboratory deadlines. Instrument maintenance and upkeep are included in Ms. Child's responsibilities. In order to ensure the fulfillment of deadlines , she also communicates daily with the organic extractions department about sample prep . EDUCATION University of London, King's College London Bachelor of Science, 2003 EMPLOYMENT The British Medical Association., 2003-2004 Assistant Assisted the Senior Group Member of the Information and Management technology department , assisted with invoicing and negotiations, aided in purchasing department and updating the website. Grosvenor., 2002-2003 Data input. Wilkinson Hardware Stores Ltd., 2000-2002 Customer Sales Advisor Responsible for organizing displays , assisting customers, training staff, and some supervisory duties. Euphony Consultant Enterprise., Aug. 1999 -Dec. 1999 Rec eptionist Responsible for organizing meeting rooms and scheduling appointments and meetings. Rev. 08/09/06 RICHARD RODRIGUEZ Organics Technical Director Accutest Laboratories Gulf Coast, Inc. Houston, Texas Richard is the GC/MS Volatile analyst for Accutest Labs. His duties include, but are not limited to, preparation and analysis. He is responsible for analyzing and reporting results in an accurate and efficient manner to fulfill client/laboratory deadlines. Instrument maintenance and upkeep are included in Mr. Rodriguez's responsibilities. EDUCATION B.S. Agriculture, Texas State University, 1987 Technical Training, Perkin Elmer, 1993 Masters in Environmental, Texas A&M -Corpus Christi, 1994 Technical Training, Varian Inc ., 1999 EMPLOYMENT ESN-South Mobile Laboratories, 1995-2004 Laboratory Manager Responsibilities include general management of all the mobile laboratories and fixed based lab, project scheduling, performing maintenance of all instrumentation, developing of QA/QC plan, S0Ps, MDLs, and gas chromatography method development. Performing analysis of VOC's by GC, GC/MS (8021B, 8260B), TPH(TX-1005 and US EPA 8015), SVOC's (8270C), pesticides and PCB's (8081, 8082). Other responsibilities involve traveling with the mobile laboratory to perform on-site analysis, creating marketing strategies and maintaining customer relations. Core Service, Inc., 1991-1995 Lab Technician Testing of various types of environmental parameters: BOD, TPH, Metals, BTEX, VOC's, pesticides and method developments. Assumed responsibility for the design and installation of the new laboratory and writing of the Standard Operation Procedures. Union fishing S.A. in Casama, Peru., 1987-1991 General Manager Responsible for the management of two farms and two offices and also accountable for the selling produce. Traveled extensively in South America, Europe, and United States Rev. 08/09/06 for the purchase of new equipment and locating potential customers for our exports . Rev. 08/09/06 Agnes Vicknair Senior Project Manager Accutest Laboratories Gulf Coast, Inc. Houston, Texas Ms . Vicknair has primary responsibility for client services / project management. She communicates directly with clients to insure accuracy of requested analysis and sample information needed for correct reporting of results. She advises technicians of project scopes through LIMS (a sample management database) and verbally coordinates urgent deadline capacities. She also fields inquiries regarding price quotations, method citation, holding and turn-around times, sampling containers, sample preservatives, and report status. Ms. Vicknair also assists in sample control. EDUCATION Associate Degree -Natrural Science, 1981 PROFESSIONAL EXPERIENCE Severn Trent Laboratory, Houston, Texas, 1997-2005 Project Manager: Coordinate and manage customers' projects through all phases of laboratory operations . Maintain communications with clients and Account Executives and serve as a liaison between clients and laboratory operations. Monitor compliance with industry regulations, contractual agreements, program management processes and program specifications. Severn Trent Laboratory, Houston, Texas, 19995-1997 Laboratory Supervisor: Managed a team of professional scientists, analysts, and support staff. Rev. 08/09/06 UACCU ,: QA Officer Tamera Welch 713-271-4700 ext. 104 Ld.bor::1lor1e '.:: City of Fort Worth Environmental Management Department Accutes t Laboratories Gulf Coast, Inc . 10165 Harwin, Suite 150 Houston , TX 77036 Phone : (713) 271-4700 Fax: (713) 271-4770 www.accutest.com Xenco Labs, Inc S11h-C 'ontract Lah 91!!1 (jACCUTEST. Revision Date : March 2007 Revision I Accutest Laboratories Organization Chart David Speis Director, Corporate Quality Assurance • Tamara Welch Quality Assurance Officer I Alisha Rodriguez Cassie Escotto J . Dan Borak ~::,mnlP. M::,n::,nP.mP.nt I Sheila Cheng Tim Smith Rochelle Child Felix Oses Semi-Vala ile Oraanics Ena Fileds Charles Hardesty Jim Low Melissa Contreras nrn::anir Pr,:an Richard Rodriguez Technical Director, Organics Vincent J. Pugliese President, CEO Ron Martino Laboratory Director Gulf Coast Laboratory I Ron Martino Technical Director, lnorganics I Greg Grandits Business Development Manaaer I Allie Franco Administrative Assistant Lien Nguyen -Wet Chem ]· Nidia Saspa -Metals 11 .. I Luis Racelis -Metals prep Eden Bigtacion -Wet Chem Jennifer Hoang Zandra Holbrook Lydia Jasso Volatile Organics I Sylvia Garza Project Manager Agnes Vicknair Sr. Project Manager 2 .9 PROVIDER 'S LICENSES & CERTIFICATES 2 .9.1 Provider shall include a copy of all certifications and/or licenses including required NELAC accreditation documentation. 2 .9 .2 Provider shall procure all permits and licenses , pay all charges , costs , and fees , and give all notices necessary and incident to the due and lawful prosecution of the work. The undersigned acknowledges the requirements of this section , and intends to comply with same in the execution of this project. PROVIDER: //Cc</Te$" T L.fi/Jo~rl7or!/Ef BY : CfiECiJlt,Y T. GtfAt-lO ;-rf Company Name (print or type name of signatory) /o/C § /../Al?. W I N LJA. ,;v,TE 1.fo ~ r Address (Signature) ;.1ovfTu/.J r ,>c 77o'J6 ~t/S//J,1:J"f /YE//, /J?/lfll/16£~ City, State , Zip Title (print or type) 2-13 9 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY ·,,,,.-:;-~- ":,,,lu:.__,.,-4 NELAP-Recognized Laboratory Accreditation is hereby awarded to Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive, Suite 150 Houston, TX 77036-1622 in accordance with, Texas Water Code Chapter 5, SubclUlpter R, Title 30 Texas Administrative Code Chapter 25, and the Nationa/Environmenta,/ Laboratory Accreditation Program. The laboratory's scope of accreditation includes th~ fields of accreditation that accompany this certificate. Continued accreditation depends upon successful ongoing participation in the program. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Certificate Number: T 104 704220-07-TX Effective Date: March 28, 2007 Executive Director Expiration Date: March 31, 2008 Texas Commission on Environmental Quality TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation (/.,.,., Accutest Laboratories Gulf Coast , Inc. 10165 Harwin Drive Suite 150 Houston , Texas 77036-1622 .........:.----"""- Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date: March 31, 2008 These fields of accred itation supercede all previous fields . The Texas Commission on Environmental Q uality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Fields of Accreditation Matrix: Solid and Chemical Materials Category/Method: Metals/EPA 60108 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Aluminum Antimony Arsenic Bar ium Beryllium Boron Cadm ium Ca lcium Chromium r~· Copper on Lead thium Magnesium anganese Molybdenum ickel Potassium Selenium Silver ~ilica Strontium Sodium Thallium T in Titanium Vanadium Zinc Category/Method: Metals/EPA 7470 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Mercury Category/Method: Metals/EPA 7471A Analytes: Code: CAS No .: Analytes: Code: CAS No.: Mercury Category/Method: Waste Characteristics/EPA 1010 Analytes: Code: CAS No.: Analytes: Code: CAS No .: lgnitability Category/Method: Waste Characteristics/EPA 9040 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Corrosiv ity Page 1 of 18 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Issue Date: March 28, 2007 Expiration Date: March 31, 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: So/Id and Chemical Materials Category/Method: General Chemistry/EPA 340.2 Analytes: Code: CAS No.: Fluoride Category/Method: General Chemistry/EPA 350. 1 Analytes: Code: CAS No.: Ammonia (as N) Category/Method: General Chemistry/EPA 353.2 Analytes: Code: CAS No.: Nitrate (as N) Nitrite (as N) Category/Method: General Chemistry/EPA 365.2 Analytes: Code: CAS No.: Orthophosphate (as P) Category/Method: General Chemistry/EPA 1664 Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Category/Method: General Chemistry/EPA 7196 Analytes: Code: CAS No.: Chromium VI Category/Method: General Chemistry/EPA 9012 Analytes: Code: CAS No.: Cyanide, Amenable Category/Method: General Chemistry/EPA 9035 Analytes: Code: CAS No.: Sulfate Category/Method: General Chemistry/EPA 9040 Analytes: Code: CAS No.: pH Analytes: Analytes: , Analytes: Nitrate-Nitrite (as N) Analytes: Analytes: Analytes: Analytes: Cyanide, Total Analytes: Analytes: Page 2of 18 Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMEN'JAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation ~(./ .,. 11 ... Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date : March 31, 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Solid and Chemical Materials Category/Method: General Chemistry/EPA 9045C Analytes: Code: CAS No.: pH Category/Method: General Chemistry/EPA 9050 Analytes: Code: CAS No.: Specific Conductance (Conductivity) Category/Method: General Chemistry/EPA 9060 Analytes: Code: CAS No.: Organic Carbon , Total (TOC) Category/Method: General Chemistry/EPA 9066 Analytes: Code: CAS No.: Phenols Category/Method: General Chemistry/EPA 9095 Analytes: Code: CAS No.: Paint Filter Liquids Test Category/Method: General Chemistry/SM 25108 Analytes : Code: CAS No.: Specific Conductance (Conductivity) Category/Method: voes by GC!MSIEPA 82608 Analytes: Code: CAS No.: 1 , 1, 1,2-Tetrachloroethane 1 , 1,2,2-Tetrachloroethane 1 , 1-Dichloroethane 1, 1-0ichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichloroethane 1,3,5-Trimethyibenzene 1,3-Dichloropropane 1,4-Dioxane 2,2-Dichloropropane Analytes: Code: Analytes: Code: Analytes: Code: Analytes: Code : Analytes: Code: Analytes: Code: Analytes: Code: 1, 1, 1-T richloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2-Dibromo-3-chloropropane (DBCP) 1,2-Dichlorobenzene 1,2-0ichloropropane 1,3-Dichlorobenzene 1,4-0ichlorobenzene 1-Chlorohexane 2-Butanone (MEK) Page 3of 18 CAS No.: CAS No.: CAS No.: CAS No.: CAS No.: CAS No.: CAS No.: ... ·-··-· -----·-... ··-·. -··--... ---·······---·-------···-------·------~----------· ···--·-·. ·---·· ··- TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation ~ (/ . ,-H Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date: March 31 , 2008 These fields of accreditation supercede all previous fields. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Solid and Chemical Materials Category/Method: voes by GC!MS!EPA 82608 (Conti.) Analytes: Code: CAS No.: Analytes: 2-Chloroethyl vinyl ether 2-Chlorotoluene 2-Hexanone (MBK) 2-Nitropropane 4-Chlorotoluene 4-lsopropyltoluene 4-Methyl-2-pentanone (MIBK) Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform 8romomethane Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroform cis-1,2-Dichloroethene Dibromochloromethane Dichlorodifluoromethane Hexachlorobutadiene lsopropylbenzene Methylene chloride n-Butyt benzene sec-Butytbenzene tert-Butyl alcohol T etrachloroethene trans-1,2-Dichloroethene trans-1,4-Dichloro-2-butene Trichlorofluoromethane Vinyl chloride Xylenes, meta, para Category/Method: SVOCs by GC/MSIEPA 8270C Analytes: Code: CAS No.: 1,2,4,5-Tetrachlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 2,3,4,6-Tetrachlorophenol 2,4,6-Trichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene Chloroethane Chloromethane tis-1 , 3-Dichloropropene Oibromomethane Ethyl benzene lodomethane Methyl tert-butyl ether (MTBE) Naphthalene n-Propylbenzene Styrene iert-Butylbenzene Toluene trans-1 ,3-Dichloropropene Trichloroethane Vinyl acetate Xylene, ortho Xylenes, Total Analytes: 1,2,4-Trichlorobenzene ~ ,2-Diphenylhydrazine 1,4-Dichlorobenzene 2,4,5-T richlorophenol 2,4-Dichlorophenol 2,4-Dinitrophenol 2,6-Dinitrotoluene Page 4 of 18 Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENtAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date : March 31, 2008 These fields of accreditation supercede all previous fields. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current acaeditation status for particular methods and analyses. Matrix: Solid and Chemical Materials Category/Method: SVOCs by GC/MSIEPA 8270C (Conti.) Analytes: Code: 2-Chloronaphthalene 2-Methyt-4 ,6-dinitrophenol 2-Methytphenol 2-Nitrophenol 3,3'-Dichlorobenzidine 3-Nitroaniline 4-Bromophenyt phenyt ether 4-Chloroaniline 4-Methytphenol 4-Nitrophenol Acenaphthene Acetophenone Anthracene Benzidine Benzo(b)fluoranthene Benzo(k)fluoranthene Benzyt alcohol Bis(2-chlorethoxy)methane Bis (2-chloroisopropyt)ether Carbazole Dibenz( a,h)anthracene Dibenzofuran Dimethyl phthalate Di-n-octyl phthalate Fluoranthene Hexachlorobenzene Hexachlorocyclopentadiene lndeno( 1,2,3-c,d)pyrene Naphthalene N-Nitrosodiethytamine N-Nitrosodi-n-butytamine N-Nitrosodiphenytamine Pentachlorophenol Phenol Pyridine CAS No.: Analytes: Code: 2-Chlorophenol 2-Methytnaphthalene 2-Nitroaniline 2-Picoline 3-Methyf phenol 4 ,4'-Methylenebis(2-chloroaniline) 4-Chloro-3-methyf phenol 4-Chlorophenyt phenyt ether 4-Nitroaniline Y, 12-Dimethylbenz(a) anthracene Acenaphthyfene Aniline Benz( a )anthracene Benzo( a )pyrene Benzo(g,h,i)perylene Benzoic acid Benzyt butyt phthalate Bis (2-chloroethyt)ether Bis(2-ethyf hexyl)phthalate Chrysene Oibenz(a,j)acridine Diethyl phthalate Di-n-butyl phthalate Piphenytaminie Fluorene Hexachlorobutadiene Hexachloroethane lsophorone Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-propylamine Pentachlorobenzene Phenanthrene Pyrene Page 5 of 18 CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation , '~ (/ .. ,. 11 Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston , Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date : March 28, 2007 Expiration Date : March 31 , 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: Organics by GCnCEQ 1005 Analytes: Code: CAS No.: Total Petroleum Hydrocarbons Category/Method: Organics by GCIEPA 80158 Analytes: Code: CAS No.: Diesel Range Organics (ORO) Ethanol Methanol Category/Method: Organics by GCIEPA 80218 Analytes: Code: CAS No.: Benzene Methyl tert-butyl ether (MTBE) Xylene , ortho Xylenes, Total Category/Method: Organics by GC/EPA 8081A Analytes: Code: CAS No.: 4,4'-DDD 4,4'-DDT Aldr in Chlordane , alpha Chlordane, technical d-BHC Dieldrin Endosulfan II Endrin Endrin ketone Heptachlor Hexachlorobenzene Mirex Analytes: Code: Analytes: Code: Gasoline Range Organics (GRO) lsopropyl alcohol Analytes: ~thylbenzene Toluene Xylenes, meta, para Analytes: 4 ,4 '-DDE a-BHC b-BHC Chlordane, gamma Chlorothalonil Dicofol (Kelthane) Endosulfan I Endosulfan sulfate Endrin aldehyde g-BHC (Lindane) Heptachlor epoxide Methoxychlor Toxaphene Code: Code: Page6of 18 CAS No.: CAS No.: CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation (/.,. 11 --..:..-~ Accutest Laboratories Gulf Coast, Inc . 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number : T104704220-07.TX Issue Date : March 28 , 2007 Expiration Date : March 31 , 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: Organics by GCIEPA 8082 Analytes: Code: CAS No.: PCB-1016 PCB-1232 PCB-1248 PCB-1260 Category/Method: Organics by GC/EPA 8151A Analytes: Code: CAS No.: 2,4,5-T 2,4-D 4-Nitrophenol Dicamba Dinoseb MCPP Picloram Matrix: Non-Potable Water Category/Method: Metals/EPA 200. 7 Analytes: Code: CAS No.: Aluminum Arsenic Beryllium Cadmium Chromium Copper Lead Manganese Nickel Selenium Silver Strontium Tin Vanadium Analytes: PCB-1221 PCB-1242 PCB-1254 PCBs, Total Analytes: i,4,5-TP (Silvex) ?.4-DB IDalapon lbichloroprop (Weedone) MCPA l?entachlorophenol Analytes: Antimony Barium Boron Calcium Cobalt Ir on Magnesium Molybdenum Potassium Silica, Dissolved Sodium Thallium Titanium Zinc Page 7 of 18 Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QVALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date : March 28 , 2007 Expiration Date: March 31, 2008 These fields of accreditation supercede all previous fields. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: Metals/EPA 245. 1 Analytes: Code: CAS No.: Mercury Category/Method: Metals/EPA 60108 Analytes: Code: CAS No.: Aluminum Arsenic Beryllium Cadmium Chromium Copper Lead Magnesium Molybdenum Potassium Silica, dissolved Sodium Thallium Titanium Zinc Category/Method: Metals/EPA 7470A Analytes: Code: CAS No.: Mercury Category/Method: Metals/EPA 7471 Analytes: Code: CAS No.: Mercury Category/Method: General Chemistry/EPA 120.1 Analytes: Code: CAS No.: Specific Conductance Category/Method: General Chemistry/EPA 130.2 Analytes: Code: CAS No .: Hardness, Total Analytes: Analytes: Antimony Barium Boron Calcium Cobalt Iron Lithium Manganese Nickel Selenium Silver Strontium Tin Vanadium Analytes: Analytes: Analytes: Analytes : Page 8 of 18 Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No .: Code: CAS No.: Code: CAS No.: TEXAS COM~SSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation ~ (./ . . 1' H ,,, ' Accutest Laboratories Gulf Coast, Inc . 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T 104 704220-07-TX Issue Date : March 28, 2007 Expiration Date : March 31, 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 150.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: pH Category/Method: Genera/ Chemistry/EPA 160.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Residue, Filterab le (TDS) Category/Method: General Chemistry/EPA 160.2 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Residue , Nonfilterable (TSS) Category/Method: General Chemistry/EPA 160.3 Analytes : Code: CAS No.: Analytes: Code: CAS No.: Residue, Total Category/Method: General Chemistry/EPA 160.4 Analytes: Code: CAS No.: Analytes: Code: CAS No .: Residue, Volatile Category/Method: General Chemistry/EPA 215.2 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Calcium Category/Method: Genera/ Chemistry/EPA 310.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Alkalinity Category/Method: General Chemistry/EPA 325.3 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Chloride Category/Method: General Chemistry/EPA 330.5 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Chlorine, Total Residual Page 9 of 18 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date : March 31 , 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status fo r particular methods and analyses . Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 335.3 Analytes: Code: CAS No .: Cyanide , Total Category/Method: General Chemistry/EPA 340.2 Analytes: Code: CAS No.: Fluoride Category/Method: General Chemistry/EPA 350.1 Analytes: Code: CAS No.: Ammonia (as N) Category/Method: General Chemistry/EPA 351.2 Analytes: Code: CAS No.: Nitrogen, Total Kjeldahl (TKN) (as N) Category/Method: General Chemistry/EPA 353.2 Analytes: Code: CAS No.: Nitrate (as N) Nitrite (as N) Category/Method: General Chemistry/EPA 365.2 Analytes: Code: CAS No.: Orthophosphate (as P) Category/Method: General Chemistry/EPA 376.1 Analytes: Code: CAS No.: Sulfide Category/Method: General Chemistry/EPA 377.1 Analytes: Code: CAS No.: Sulfite Category/Method: General Chemistry/EPA 405.1 Analytes: Code: CAS No.: Biochemical Oxygen Demand (BOD) Analytes: Analytes: 'Analytes: Analytes: Analytes: Nitrate-Nitrite (as N) Analytes: Phosphorus, Total Analytes: Analytes: Analytes: Page 10 of 18 Code: CAS No.: Code: CAS No .: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation \, v ,. 11 Accutest Laboratories Gulf Coast , Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07~Tx Issue Date : March 28, 2007 Expiration Date: March 31 , 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods ar.id analyses. Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 410.4 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Chemical Oxygen Demand (COD) Category/Method: General Chemistry/EPA 415.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Organic Carbon, Total (TOC) Category/Method: General Chemistry/EPA 420.2 Analytes: Code: CAS No.: · Analytes: Code: CAS No.: Phenols Category/Method: General Chemistry/EPA 1010 Analytes: Code: CAS No.: Analytes: Code: CAS No.: lgnitability Category/Method: General Chemistry/EPA 1664 Analytes: Code: CAS No.: Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Category/Method: General Chemistry/EPA 7196 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Chromium VI Category/Method: General Chemistry/EPA 9012 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Cyanide, Amenable Cyanide , Total Category/Method: General Chemistry/EPA 9035 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Sulfate Category/Method: General Chemistry/EPA 90408 Analytes: Code: CAS No.: Analytes: Code: CAS No.: pH Page 11 of 18 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Issue Date: March 28, 2007 Expiration Date: March 31, 2008 These fields of accreditation supercede all previous fields. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods arid analyses. Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 9060A Analytes: Code: CAS No.: Analytes: Code: CAS No.: Organic Carbon, Total (TOC) Category/Method: General Chemistry/SM 23208 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Alkalinity Category/Method: General Chemistry/SM 25108 Analytes: Code: CAS No.: · Analytes: Code: CAS No.: Specific Conductance (Conductivity) Category/Method: General Chemistry/SM 4500-FC Analytes: Code: CAS No.: Analytes: Code: CAS No.: Fluoride Category/Method: General Chemistry/SM 52108 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Biochemical Oxygen Demand (BOD) Category/Method: General Chemistry/SM 5220D Analytes: Code: CAS No.: Chemical Oxygen Demand (COD) Category/Method: voes by GCIMS/EPA 624 Analytes: Code: CAS No.: 1, 1, 1-Trichloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2-Dichlorobenzene 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Chloroethy1 vinyl ether Acrolein Benzene Bromoform Carbon Tetrachloride Chloroethane Carbonaceous Biochemical Oxygen Demand (CBOD) Analytes: Analytes: 1, 1,2,2-Tetrachloroethane 1 , 1-Dichloroethane 1 ,2-Dibromoethane (EDB) 1.,2-Dichloroethane 1,3-Dichlorobenzene 2-Butanone (MEK) Acetone Acrylonitrile Bromodichloromethane Brom om ethane Chlorobenzene Chloroform Code: CAS No.: Code: CAS No.: Page 12 o~ 18 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation :'f (/ '/" #1 C Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date: March 31, 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Non-Potable Water Category/Method: voes by GCIMSIEPA 624 (conti.) Analytes: Code: CAS No.: Chloromethane Dibromochloromethane Methylene chloride T etrachloroethene trans-1,2-Dichloroethene Trichloroethene Vinyl chloride Xylenes, meta, para Category/Method: VOCs by GCIMS/EPA 82608 Analytes: Code: CAS No.: 1, 1, 1,2-T etrachlorethane 1, 1 .2.2-T etrachlorethane 1, 1-Dichloroethane 1, 1-Dichloropropene 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-Dichlorobenzene 1,2-Dichloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Chlorohexane 2-Butanone (MEK) 2-Chlorotoluene 2-Nitropropane 4-lsopropyltoluene Acetone Acrylonitrile Bromobenzene Bromodichloromethane Bromomethane Carbon tetrachloride Chlorethane Chloromethane cis-1,3-Dichloropropene Analytes: ~is-1,3-Dichloropropene Ethyl benzene Methyl tert-butyl ether (MTBE) Toluene trans-1,3-Dichloropropene T richlorofluoromethane Xylene, ortho .Xylenes, Total Code: Analytes: Code: 1.1, 1-Trichloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2 ,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2-Dibromoethane (EDB) 1,2-Dichlorethane 1,3,5-Trimethylbenzene 1,3-Dichloropropane 1,4-Dioxane 1,2-Dichloropropane 2-Chlorethyl vinyl ether 2-Hexanone (MBK) 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acrolein Benzene Bromochloromethane Bromoform Carbon disulfide Chlorobenzene Chloroform dis-1,2-Dichlorethene Dibromochloromethane Page 13 of 18 CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation ~ v.,.. H Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date: March 31, 2008 These fields of accreditation supercede all previous fields. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Non-Potable Water Category/Method: voes by GCIMSIEPA 82608 (Conti.) Analytes: Code: CAS No.: Analytes: Code: Dibromochloropropane Dichlorodifluoromethane Hexachlorobutadiene lsopropylbenzene Methylene chloride n-Butylbenzene sec-Butyl benzene tert-Butyl alcohol T etrachloroethene trans-1 ,2-Dichlorethene trans-1 ,4-Dichloro-2-butene Trichlorofluoromethane Vinyl chloride Xylenes, meta, para Category/Method:SVOCs by GCIMSIEPA 625 IDibromomethane Ethyl benzene l~domethane Methyl tert-butyl ether (MTBE) Naphthalene f'.1-Propylbenzene Styrene tert-Butylbenzene Toluene trans-1 ,3-Dichloropropene Trichloroethene Vinyl acetate Xylene, ortho Xylenes, Total Analytes: Code: CAS No.: Analytes: 1,2,4-Trichlorobenzene 1,3-Dichlorobenzene 2,3,4 ,6-Tetrachlorophenol 2,4,6-Trichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2-Chloronaphthalene 2-Methyl-4,6-dinitrophenol 3,3'-Dichlorobenzidine 4-Chloro-3-methylphenol 4-Nitrophenol Acenaphthylene 1,2-Dichlorobenzene 1,2,4,5-Tetrachlorobenzene 1,4-Dichlorobenzene 2,4,5-T richlorophenol 2,4-Dichlorophenol 2,4-Dinitrophenol 2,6-Dinitrotoluene 2-Chlorophenol 2-Nitrophenol 4-Bromophenyl phenyl ether 4-Chlorophenyl phenyl ether Acenaphthene Anthracene Benzo(a )anthracene Benzo(b )fluoranthene Benzo(k)fluoranthene Bis(2-chloroethoxy)methane Bis(2-chloroisopropyl)ether Chrysene Benzidine Benzo(a)pyrene Benzo{g,h ,i)perylene Benzyl butyl phthalate Bis(2-chloroethyt)ether Bis(2-ethylhexyl) phthalate Oibenzo( a,h )anthracene Page 14 of 18 Code: CAS No.: CAS No.: TEXAS CO~SSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast , Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date: March 28, 2007 Expiration Date : March 31 , 2008 These fields of accreditation supercede all previous fields . The Texas Cotil'lmission on Environmental Quality urges customers to verify the laboratory's current acaeditation status for particular methods and analyses. Matrix: Non-Potable Water Category!Method:SVOCs by GC/MSIEPA 625 (Conti.) Analytes: Code: CAS No.: Analytes: Code: Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane lndeno(1,2,3-cd)pyrene lsophorone Naphthalene Nitro benzene N-Nitrosodiethylamine N-Nitrosodimethylam ine N-Nitrosodi-n-butylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Pentachlorbenzene Pentachlorophenol Phenanthrene Phenol IPyrene Pyridine Category/Method: SVOCs by GC!MS/EPA 8270C Analytes: Code: CAS No.: Analytes: Code: 1,2,4,5-Tetrachlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 2,3,4,6-Tetrachlorophenol 2,4,6-Trichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chlorophenol 2-Methylnaphthalene 2-Nitroaniline 2-Picoline 3-Methylphenol 4,4'-Methylenebis(2-chloroaniline) 4-Chloro-3-methyl phenol 4-Chlorophenyl phenyl ether 4-Nitroaniline 7, 12-Dimethylbenz(a)anthracene Acenaphththylene Aniline 1,2,4-Trichlorobenzene 1,2-Diphenylhydrazine 1,4-Dichlorobenzene i ,4,5-Trichlorophenol 2,4-Dichlorophenol 2,4-Dinitrophenol 2,6-Dichlorophenol 2-Chloronaphthalene 2-Methyl-4,6-dinitrophenol 2-Methylphenol 2-Nitrophenol 3, 3'-Dichlorobenzidine 3-Nitroaniline 4-Bromophenyl phenyl ether 4-Chloroaniline 4-Methylphenol 4-Nitrophenol Acenapthene Acetophenone Anthracene Page 15 of 18 CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation ~(/ ,. ,., Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T 104 704220-07-TX Issue Date: March 28, 2007 Expiration Date: March 31, 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: SVOCs by GCIMSIEPA 8270C (Conti.) Analytes: Code: CAS No.: Analytes: Code: Benz(a}anthracene Benzo(a}pyrene Benzo(g,h,i}perylene Benzoic acid Benzyt butyl phthalate Bis(2-chlorethyt}ether Bis(2-ethythexyl}phthalate Chrysene Dibenz( a,j}acridine Diethyl phthalate Di-n-butyl phthalate Diphenytamine Fluorene Hexachlorobutadiene Hexachloroethane lsophorone Nitrobenzene N-Nitrosodimethylam ine N-N itrosodi-n-propytam ine Pentachlorobenzene Phenanthrene Pyrene Category/Method: Organics by GCflCEQ 1005 Analytes: Code: CAS No.: Total Petroleum Hydrocarbons Category/Method: Organics by GC!EPA 602 Analytes: Code: CAS No.: Benzene Toluene Xytenes, meta, para Benzidine Benzo(b }fluoranthene Benzo(k)fluoranthene Benzyt alcohol Bis(2-chloroethoxy}methane Bis(2-chlorisopropyl}ether Carbazole IDibenz(a,h)anthracene Oibenzofuran Oimethyt phthalate IDi-n-octyl phthalate Fluoranth~ne Hexachlorobenzene IHexachlorocyclopentadiene 11ndeno(1 ,2,3-c,d}pyrene Napthalene !')1-Nitrosodiethytamine N-Nitrosodi-n-butylamine N-Nitrosodiphenylamine F>entachlorophenol Phenol Pyridine Analytes: Analytes: f=thytbenzene Xytene, ortho Xytenes, Total Page 16 of 18 Code: Code: CAS No.: CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Accutest Laboratories Gulf Coast, Inc. 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Issue Date : March 28, 2007 Expiration Date : March 31, 2008 These fields of accreditation supercede all previous fields . The Texas Comm ission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Non-Potable Water Category/Method: Organics by GC/EPA 608 Analytes: Code: CAS No.: 4,4'-DDD 4 ,4'-DDT Aldrin Chlordane , alpha Chlordane , Technical Dieldrin Endosulfan II Endrin g-BHC (Lindane) Heptachlor epoxide Category/Method: Organics by GC/EPA 608 (Conti.) Analytes: 4,4'-DDE a-BHC b-BHC Chlordane , gamma d-BHC IEndosulfan I Endosulfan sulfate Endrin aldehyde Heptachlor Methoxychlor Analytes: Code: CAS No.: ; Analytes: PCB-1016 IPCB-1221 PCB-1232 IPCB-1242 PCB-1248 !PCB-1254 PCB-1260 T oxaphene Category/Method: Organics by GCIEPA 80158 Code: Code: Analytes: Code: CAS No.: Analytes: Code: Diesel Range Organics (ORO) Ethanol Methanol Category/Method: Organics by GC/EPA 80218 Analytes: Code: CAS No.: Benzene Methyl tert-butyl ether (MTBE) Xylene, ortho Category/Method: Organics by GCIEPA 8081A Analytes: Code: CAS No.: 4,4'-DDD 4,4'-DDT Aldrin Chlordane, alpha Chlordane, Technical Gasoline Range Organics (GRO) lsopropyl alcohol Analytes: Ethyl benzene Toluene Xylenes , meta, para Analytes: 4,4'-DDE a-BHC l>-BHC Chlordane, gamma Chlorothalonil Code: Code : Page 17 of 18 CAS No.: CAS No.: CAS No.: CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation ~(/ ,. 11 Accutest Laboratories Gulf Coast, Inc . 10165 Harwin Drive Suite 150 Houston, Texas 77036-1622 Certificate Number: T104704220-07-TX Issue Date : March 28, 2007 Expiration Date : March 31 , 2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Non-Potable Water Category/Method: Organics by GCIEPA 8081A (contL) Analytes: Code: CAS No.: Analytes: d-BHC Qicofol (Kelthane) Dieldrin IEndosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde Endrin ketone g-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene Methoxychlor Mirex T oxaphene Category/Method: Organics by GCIEPA 8082 Analytes: Code: CAS No.: PCB-1016 PCB-1232 PCB-1248 PCB-1260 Category/Method: Organics by GC/EPA 8151A Analytes: Code: CAS No.: 2,4,5-T 2,4-D 4-Nitrophenol Dalapon Dichloroprop (Weedone) MCPA Pentachlorophenol Analytes: PCB-1221 PCB-1242 PCB -1254 PCBs , Total Analytes: 2,4,5-TP (Silvex) 2,4-DB Chloramben Dicamba Dinoseb MCPP Piclo ram Page 18 of 18 Code: CAS No.: Code: CAS No.: Code: CAS No.: t~ ~ About Us .:e,.i, ~ Lab Link MBE/DBE Wof"ld Wide Qua lity Performa nce Houston Indoor Air Qua lity fl) {1.J -.a 0 l- a; Tampa u ~ Dallas ;, Special Services Austin S: San Antonio o'O; ,\\..,.: . sv• Facilities ~ Q Labora t ory Staff Mobile Labs Statement of Qua[ificatirons XENCO Delivering Excellence in Service, Value and Quality since 1990 On -Time and Paperless MBE/SDBE TABLE OF CONTENTS 1. COMPANY PROFILE ............................................................................................. 3 2 . KEY PERSONNEL .................................................................................................. 6 2.1 LABORATORY STAFF .......................................................................................... 6 2.2 ADMINISTRATIVE STAFF .................................................................................... 7 3 . FACILITY LOCATIONS AND E QUIPMENT ......................................................... 9 3.1. LOCATlO SAND BUSI NESS HOURS .................................................................... 9 3.2. MAJOR EQUIPMENT LIST ................................................................................. 12 4. CERTIFICATIONS AND ACCREDITATI ONS .................................................... 14 4.1. CERTIFlCATIONSANDACCREDITATIONS ......................................................... 14 4.2. MfNO RITY BUSI NES S CERTIFICAT IONS ............................................................ 14 4.3 THIRD PARTY ACCREDITATIONS ...................................................................... 15 5 . QUALITY PERFORMANCE ................................................................................... 16 5.1. Q UAL ITY STATEMENT ..................................................................................... 16 5 .2. QA/QC PLAN AND TH E QUALITY SYSTEM ...................................................... 16 5.3 . LABORATORY I NFO RMATIO N MANAGEMENT SYSTEM (LIMS) ....................... 17 5.4 . P ERFORMANCE EVALUATION T EST ING ........................................................... 19 5.5. PRES ENT AND PASS LABORATORY AUDITS ..................................................... 20 5.5. POLICY ON SUBCONTRACTfNG ........................................................................ 20 6 . SAMPLE cu·sTODY ................................................................................................. 21 6.1. SAMPLE INTEG RITY ························································································· 2 1 6.2. CHAIN OF CUSTODY ························································································ 21 6.3. SAMPLE DISPOSAL ·························································································· 2 1 7 . COURIER SERVICES ............................................................................................... 22 7.1. GROUND SHIPM ENTS -SAMPLING KITS DELIVERY ........................................ 22 7.2 . AIR SHIPM EN TS ............................................................................................... 22 8. SPECIALTY SERVICES & ATTACHMENTS ..................................................... 23 8.1. EX PERT TESTIMONY ....................................................................................... 23 8.2. SOFTWARE DEV ELO PME NT ............................................................................. 23 8.3. MOBILE LABORATORY .................................................................................... 23 8.4. ASBESTOS ANALYSES ...................................................................................... 24 Attachments : Basic Certifications 2 1. COMPANY PROFILE Background Synopsis The Corporate Office opened in Houston in 1990 Dallas and San Antonio were opened in 1996 • Tampa and Miami were opened in 2001 • 2005 Certes Laboratories' assets were purchased by Xenco Laboratories " Hispanic and Minority Owned ..;. Designated Small Minority Business .;, Sales representatives throughout Latin America ~ Vast experience in most phases of Environmental Testing Analytical and Sampling Project Expertise ..;, Superfund Sites Across the Country ..;. US Anny Corp of Engineer Projects .;, Remedial Investigations ,... Salt Water, Wastewater and Drinking Water Analysis 4' Hazardous Waste Classification .., Risk Reduction Programs .;, UST and Dry Cleaner Investigations ... R&D and Fingerprinting ..;, Expert Testimonial Studies .;, Mo ld and Indoor Air Quality .., Mobile Laboratory Services Deliverables and Quality S:rstcm Programs ' Contract Laboratory Program, EPA-CLP ~ Anny Corp of Engineers , USA CE -MRD ~ State Specific Data Deliverables i.e. Texas TRRP Level II, III and IV Data Deliverables Compliance with Various State Clean-up Programs • AFCEE Data Deliverables ~ Customized Electronic Data Deliverables (EDDs) .;, Excel Data Tables Staff Qualifications 4-3 Ph. D. degreed Chemists ..., 3 Master's degreed Chemists ~ 1 Master's degreed Chemical Engineer 2 Bachelor's degreed Chemical Engineers ., 27 Bachelor's degreed Chemists 4 Bachelor's degreed Biologists .-i,, 1 Master's degreed Marine Biologist ~ 2 Bachelor's degreed Environmental Scientists 2 Bachelor's degreed Microbiologists ..., 2 Bachelor's degreed Programmers ~ 3 MBA degreed Supervisors ..., 8 years average related Experience/Employee I nstrumcnt Capabilities HP-Agilent GC /MS 71 (2), 72 (6) and 73 (2) for SVOC Analyses HP -Agilent GC /MS 71 (1), 72 (5) and 73 (4) for VOC Analyses ..., 3 Varian Saturn GC /MS 2000 for VOC Analyses ..., HP GCs: 11 PID-FID , 7 FID-FID, 3 ECD-ECD, and 1 NPD-FPD 4-3 ICP-MS for Metals Analyses, 1 ICP 5 HP HPLC 1100 Fl -D A ..., Dionex Ion Chromatographs • 3 IR, 2 TOX, 1 TOC, 5 UV-Visible Spectrophotometers Analytical Capabilities • EPA and CLP Methodologies • SW-846 Methodologies • ASTM Methodologies • State Specific UST Methodologies • Customized Methodologies • Semi-Volatiles & Volatiles Organics by GC and GC/MS • Metals -Wet Chemistry • Mold & Bacterial Analysis • Pesticides -PCBs -Herbicides • BTEX-MTBE • TPH (FL-PRO , TXl 005, DRO , GRO) • Hydrocarbon Speciation (TX 1006, Massachusetts) • Finger Printing -R&D Houston I 1381 Meadowglen, Suite L, Housto n TX 77082 Dallas 9701 Harry Hines Blvd., Suite D, Dallas, TX 75220 San Antonio 5332 Blackberry, San Antonio, TX 78238 Mid land /Odessa 12600 1-20 East , Mid land , TX 79765 Miami 5757 NW 15 8t h Street, Mi ami lakes, FL 33014 Tampa 3016 US Hwy 30 I No rth , Suite 900, Tampa, FL 33619 Atlanta 6017 Financial Drive, Norcross, GA 3007 1 Phone: 281 589 0692 214 902 0300 2105093334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 4 Fax: 281 589 0695 214 35 1 9139 2105093335 4325631713 305 823 8555 813 620 2033 770 449 5477 Project Management and Data Reporting 4' A Project Manager is assigned to your account ., Custom Reports with CAS numbers, MDL, MQL, SQL, PQL, etc . ., Get your Data on Excel Tables. Multiple Flagging Criteria Data Deliverables, including J Flagging ~ Complete Electronic PDF Reports with Signatures, via e-mail Levels I, II, III and IV Reports .., Data Query Tools to Customize your EDDs ., Controlled and Secured Web Access to your data, which includes: ., Check Job Status ~ Request Bottle Orders ,1. Download PDF Reports and Certifications ~ Get Cost Estimates or Down Load Quotes .., Methodology and Analytes Data B ank Our Qua]ity System and Vision " Satisfy the needs of our clients beyond their expectations Operate under one common Quality System Certifications to Suit your Needs ., Deliver a Full Scope of Analytical Services Leading Edge Technology, which links seamless our Network " Provide World Wide Services Real time Web access ~ Deliver Custom Data Packages on Time " Grow and Promote Quality Employees ., In essence we deliver: Service, Quality and Value ., Our ultimate goal is to deliver data On Time Every Time! Certification & Accreditations Certifications are subject to renewal, please use our Web site's Lab Link to obtain a PDF copy of the latest certification or contact your PM. ,.. NELAC Accredited (Houston , Miami and Tampa Laboratories) ., FL -LA -AR -KT-OK -TX -NM -CO -AL -GA-IL, others . MBE/DBE Certifications: SBA, TX, FL and numerous State and loc al entities . ., Registered as a Small Business on the SBA's ProNet. The Link can be found on our Web site. Hou s ton 11381 Meadowglen , Suite L, Houston TX 77082 Da ll as 9701 Ha rr y Hines B lvd ., Suite D, Dallas , TX 75220 San Antonio 5332 Bl ackberry, San Antonio , TX 78238 Mid land /Odessa 12600 1-20 East , Midland, TX 79765 Miami 5757 NW 158th Street, Miami la ke s, FL 33014 Tampa 3016 US Hwy 30 I North , Suite 900, Tampa, FL 33619 Atlanta 6017 Financial Drive , Norcross, GA 30071 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 5 Fax: 281 589 0695 214351 9139 2105093335 432 563 1713 305 823 8555 813 620 2033 770 449 5477 1. KEY PERSONNEL 2.1 LABO RA TORY STAFF President: Eduardo Builes, Ph.D. The President has the final responsibility for the overall performance of all the laboratory facilities. Makes sure that all systems, tools, and key personnel , as well as the proper working environment are in place to get a superior job done. Oversees finances, marketing, contracting, and pricing structures and sales activities Company wide. Laboratory Managers/Technical Directors: Houston: San Antonio: Dallas: Midland/Odessa: Tampa: Miami : Carlos Castro, Ph.D. Irene Vann, B.S . Danielle Winnings, B.S. Brent Barron, B.S . Joseph Harrington, B.S. Tom Helton Laboratory Manager Client Services Manager Operations Director Laboratory Manager Project Manager Laboratory Manager The Technical Director, Managing Director, Operations Director, and Laboratory Managers are responsible for the day-to-day performance of all operations. They are responsible for monitoring each Department with the continuous vigilance of the Department Managers. They monitor the strict adhered of tum-around -tim es and project specifications with the continuous support of the Project Managers. They serve as the right hand of the President to get his job done by monitoring the good performance of all tools, systems, personnel as well serving as a liaison to pursue sales opportunities and marketing activities. Quality Assurance/Quality Control Director Texas: Aster Tekle , B.S.; Florida: Monica Alexander, B.S. The QA/QC director articulates all QA policies for all the laboratories and continuously monitors laboratory performance for compliance to those policies . Se has the primary responsibility for data validation and compliance with all Corporate Quality Systems and training programs. She oversees health, safety, Hou ston 113 8 1 Meadowglen , Suite L, Houston TX 77082 Dallas 9701 Harry Hines Blvd., Suite D, Dall as, TX 75220 San Antonio 5332 Blackberry, San Antonio, TX 78238 Midland/Odessa 12600 1-20 East, Midland , TX 79765 Miami 5757 NW 15 8t h Street, Miami Jakes, FL 33014 Tampa 3016 US Hwy 30 I North , Suite 900, Tampa, FL 33619 Atlanta 6017 Financial Drive, Norcross , GA 30071 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 813 620 2000 770 449 8800 6 Fax: 281 589 0695 214351 9139 2105093335 4325631713 305 823 8555 8 13 620 2033 770 449 5477 training programs and assists in the contracting review process. She is responsible for reviewing and monitoring the compliance of all non-conformances. Audits all laboratories as required, oversees all external audits and ensures that all corrective actions are done in a timely manner and in accordance to methodologies and the quality systems. Serves as a technical resource to all clients and company personnel. Guards the Integrity and Ethical systems for the organization . Laboratory Department Supervisors : Houston VOCs -Volatiles GC & GC-MS Cynthia Elmore, B.A. SVOCs -Semi-Volatiles GC & GC-MS Renee Scruggs, B .S ./M .B.A. Wet -Chem -Metals and Wet-Chemistry Hassan Tahami, M.S. Dallas VOCs -Volatiles GC & GC-MS Jeff Bullard, B.S. SVOCs -Semi-Volatiles GC & GC-MS Jeff Bullard , B.S. Wet-Chem -Metals and Wet-Chemistry David Terry Mold Danielle Winnings, B.S. Midland/Odessa VOCs and SVOCs Celey Keene , B.S. Wet-Chem -Metals and Wet-Chemistry Celey Keene, B.S. Miami voes Vicky Cuartas, B .S. SVOCs Vicky Cuartas, B.S. Wet-Chem Eleonora Servera, B.S. Tampa voes Ed Campbell , B.S. The Department Supervisors monitor the work of analysts and technicians within his laboratory section and has primary responsibility for compliance to specific methodologies, protocols, QAPP, Xenco quality systems, data validation and sample handling protocols . 2.2 ADMINISTRATIVE STAFF IT Director: Jaime A. Builes, B.S. The IT director has the oversight of our LIMS system, among the responsibilities include: maintenance, upgrades and new developments. It is also a responsibility for the management of the archiving systems of all computers, servers and instrument data. Development of customized software for reporting , EDD generation and data management. Hou ston I 13 8 1 Meadowg len, Suite L, Houston TX 77082 Da llas 9 701 Harry Hines Blvd., Suite D, Dallas, TX 7 5220 Sa n Antonio 5332 Blackberry, San Antonio , TX 7823 8 Midl a nd /Od es sa 12600 1-20 East , Midland , TX 79765 Mi ami 5 757 NW 15 8th Street, Mi a mi lakes, FL 33014 Tampa 3 0 16 US Hwy 30 I North , Suite 900 , Tampa , FL 3 3619 Atl a nta 6017 Fin a nci a l Drive , Norcros s , GA 30071 Phone : 281 5 89 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 8 13 620 2 000 770 449 8 800 7 Fa x: 2 8 1 5 89 0695 214 351 9139 210 509 3335 432 563 1713 305 823 8555 8 13 6 20 2033 770 449 5477 fB Responsible for the Management of the web site and Lab Link our very own data browser, which allows clients to view real-time their data and retrieve older reports and invoices. Also, responsible for all IT systems : from Telephony to Data Systems , from Terminals to Servers, from Archiving to Reporting. Project Management/Technical Services: Paula Kirtley, B.S. Debbie Simmons Cori Goodman Monica Tobar Danielle Winnings, B.S . Brent Barron , B.S. Irene Vann Joseph Harrington, B.S . Tom Helton, B.S. Cindy Kegelman Steve Walton Nick Straccione Houston Houston Houston Dallas Dallas Midland/ Odessa San Antonio Tampa Miami West Palm West Palm New Jersey The Technical Service Coordinators and/or Project Managers provide technical support to clients and all sections of the laboratory . As Project Managers they are responsible for the oversight of all communications between the client and the Laboratory. They are responsible of all aspects of client services: from quotes to sampling kits, from sample login to report generation, from invoicing to all aspects of client satisfaction. Account Executives: Kelly Steinberg, B.S. Lourdes Simmons Nicholas Straccione Wes Tyler Kevin Femander Brad Luchini Nationwide Corpus Christi Philadelphia/New Jersey Florida Georgia Georgia The Account Executives are responsible for business development, sales, local area project management and client service coordination with project managers at the various XENCO Laboratory offices. They are responsible for quotes, proposal generation and technical support. All Laboratory Managers often play a role of Account Executives. Hou ston 11 38 1 Meadowg len , S uite L, Houston TX 77082 Da llas 970 1 Harry Hin es Blvd ., Sui te D, Da ll as, TX 75220 San A ntonio 5332 Blackbe rry , San Antonio, TX 78238 Midl and /Odessa 12 600 1-20 East, Midl and , TX 79765 Mi ami 5 7 57 W 15 8th Street, Miami lake s , FL 330 14 T a mpa 30 16 US Hwy 30 I North , S uit e 900, Tampa, FL 33619 At la nta 60 17 Fin a ncial Dri ve, Norcross, GA 30071 Phone : 2 8 1 589 0692 2149020300 2105093334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 8 Fa x : 28 1 589 0695 21435 1 9 13 9 2105093335 432563 1713 305 823 8555 8 13 620 2033 770 449 5477 9 3. FACILITY LOCATIONS AND EQUIPMENT 3.1. Locations and business hours Lo{·ations: Corporate Facility: Houston , Texas * Address: 11381 Meadowglen Lane , Suite L Houston , TX 77082 Office: 28 1-589 -0 692 Fax: 281 -589-0695 Sa les Co nt act: Kelly Ste inb erg Additiona l Faci liti es: Dallas , Texas Address : 9701 Harry Hines Blvd., Suite D Dallas , TX 75220 Office: 214-903 -0 300 Fax: 2 14-35 1-9 139 Sa les Contact: Kelly Stei nb erg Hou ston 11381 Meadowg len , Suite L, Houston TX 77082 Dallas 970 I Harry Hines Blvd., Suite D, Dallas, TX 75220 San Antonio 5332 Blackberry, San Anton io, TX 78238 Midl and /Odessa 12600 1-2 0 East , Midland , TX 79765 Miami 5757 NW 158th Street, Miami lakes, FL 330 14 T amp a 3016 US Hw y 30 I North , Suite 900, Tampa, FL 336 19 At lanta 60 17 Fin a nc ial Drive, Norcross, GA 3007 1 Phone: 281 589 0692 214 902 0300 2105093334 432 563 1800 305 823 8500 813 620 2000 770 449 8800 Fax : 281 589 0695 2143519139 2105093335 432 563 17 13 305 823 8555 813 620 2033 770 449-54 77 10 •"{: , t • ~ r:,,T, i i C Mid land/Odessa, Texas e Address: 12600 1-20 East Mid land, TX 79765 Office: 432-563-1800 Fax: 432-563-1713 Sales Contact: Ke ll y Steinberg e Miami , Florida Address: 5757 NW 158th Street Miami Lakes , FL 33014 Office: 305 -823 -8500 Fax: 305-823 -8555 Sales Contact: Wes Tyler e Atlanta, Georgia Address: 6017 Financial Drive Norcross , GA 30071 Office: 770 -449-8800 Fax: 770-449 -5477 Sales Contact: Kevin Fernander Service Centers: II San Antonio, Texas Address: 5332 Blackberry San Antonio, Texas Office: 210 -509 -3334 Fax: 210-509 -3335 Sales Contact: Lulu Simmons II Corpus Christi: Address: 11229 B lades St. Corpus Christi , Texas 78410 Office: 361-726-8870 Sales Contact: Lu lu Simmons II Marlton , NJ/Philade lphia, PA : Address: 24 Apple Way Marlton, New Jersey 08053 Office: 610-955 -5649 Sales Contact: Nick Straccione Houston 11 38 1 Meadowglen , Su it e L, Houston TX 77082 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 813 620 2000 770 449 8800 Da llas 970 I Harry Hine s Blvd., Suite D, Dallas, TX 75220 San Antonio 5332 Blackbe rry, Sa n An toni o, TX 78238 Midland/Odessa 12600 1-20 Ea st, Midland , TX 79765 Miami 5757 NW 158th St reet, Miami lakes , FL 33014 Tampa 30 16 US Hwy 30 1 North, S uite 900, Tampa, FL 33619 At lanta 60 17 Fin anci al Drive, Norcross, GA 30071 Fax: 281 589 0695 2143519139 2105093335 432 563 17 13 305 823 8555 8136202033 770 449-5477 11 Business Hours: Houston: M-F 8:00 -18:00 (Sample Drop-off, Any Time pre- arranged) Sat 9:00 -13 :00 Other Offices : M-F 8:00 -17:30 (Sample Drop-off, Any Time pre- arranged) Rush services available year round, 24 hrs a day, as needed. Tum-Around Times counts only working days M-F unless otherwise pre- arranged. Houston I 13 8 1 Meadowglen , Suite L, Hou sto n TX 77082 Dallas 9701 Ha rry Hine s Blvd., Suite D, Dall as, TX 75220 San Antonio 5332 Blackberry, San Antonio, TX 78238 Mid land/Odessa 12600 1-20 East, Mid land , TX 79765 Miami 5757 NW 15 8th Street, Miami lake s, FL 33014 Tampa 3016 US Hwy 30 I North, Suite 900, Tampa, FL 336 19 Atlanta 6017 Financi a l Drive, Norcross, GA 30071 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 813 620 2000 770 449 8800 Fax: 281 589 0695 214 351 9139 2105093335 4325631713 305 823 8555 8 13 620 2033 770 449-5477 12 3.2. Major Equipment Li st Analysis Type N Equipm~nt Description Quantity Metals , ICP-MS HP 4500 plus ICP /MS (2), HP 7500 ICP /MS (1), 3 Metals , GF P erkin Elmer 41 OOZL Graphite Furnace 1 Metals , GF Thermolyne Muffle Furnace 1 Metals , H g Perkin Elmer MHS-10 Cold Vapor AA Spectrophotometer 1 Metals , Hg Leeman Cold Vapor Mercury Analyzer 1 Meta ls , ICP Perkin Elmer Plasma 400 Emissions Spec . (S equ ential ICP) 1 Metals , ICP Cirus Axi al ICP 1 Metals , Dig Microwave Metals Digesters 3 Meta ls , Di g Block Di gestors 2 M etals , SVOCs TCLP Rotators (24 places total) 3 Mold Analysis Microscop es 3 Micro-Biology Quebec , D arkfield Colony Counter, Incubators 2 Semi-volatiles HP HPLC 1100 Diode-Array-Fluorescence Detectors 5 Semi-vol atiles HP GC-MS 5890 Series II / 5971AMass Spectrometer 2 Semi-volatiles HP GC-MS 5890 Series II / 5972Mass Spectrometer 5 Semi-volatiles HP GC-MS 6890 Series II / 5973AMass Spectrometer 2 Semi-vol atil e s HP 5890 Series II , GC /FID-FID 9 S emi-volatiles HP 5890 Seri e s II GC with 5970A-Upgraded Mass Specs. 3 Semi-vol atiles HP 6890-5890 Series II Plus , GC /ECD (Dual Detector) 5 Vol atil es HP GC-MS 5890 Series II / 5971AMass Spectrometer 1 Vol atil es HP GC-MS 5890 Series II / 5972Mass Spectrometer 5 Vol atil e s HP GC-MS 6890 Series II / 5973AMass Spectrometer 4 Volatiles HP 5890 Series II, GC /FID-ELCD 1 Vol atil e s HP 5890 Series II, GC /FID-PID with Arcon Auto Samplers 11 Vol atiles Millipore Zero Head Space Extractors 20 Organic Prep Sonicators , Drying Ov ens , Fume Hoods , 3D Sh akers , L-L E x tractors , GPC System W et Chemistry Bal ances , Ove ns , UV -Visible Spectrophotometers, Meters , Electrod e s , Walk-in Refri gerators , Freezers, etc. W et Chemistry Dionex Ion Chromatographs (Anions and Cations) 2 W et Ch emistry Symphony 50 Conductance Meter 1 W et Chemistry Hach COD R eactor 1 Wet Chemistr y Buck Sci entific HC404 1 W et Chemistry Coming and Fisher pH Meter 1 Ho usto n 11 38 1 Meadowg le n, S uite L, Housto n TX 77082 Da ll as 970 1 Harr y Hin es B lvd ., S uite D , Da ll as, T X 752 20 Sa n Antoni o 5332 B lack berry, San A nto ni o, TX 78238 M id land /Odes sa 12600 1-20 East , M idl and , TX 7976 5 Miami 5757 NW 15 8th S tree t, M iami lakes, F L 330 14 Ta m pa 30 16 US Hwy 30 I North , S uite 90 0, Tampa, F L 3 36 19 Atl anta 60 17 Fin ancial Dri ve , Norcross, GA 3007 1 Ph o ne: 28 1 589 0692 214 9020300 2 105093334 43 2 563 1800 305 823 8500 8 13 620 2000 77 0 44 9 8800 Fax : 28 1 589 069 5 2 143 51 9 139 2 10 509 3335 4 32563 17 13 305 823 855 5 8 13 620 2033 770 449 -5477 13 1~4 ,.._ , t • l· ~ "· •T• •• •) '.<+· Wet Chem istry Kontes Mini -Vap D ist ill ati on Apparatus 1 Wet Chemistry Symphony D isso lved Oxygen Meter 1 Wet C hemistry Fisher/Tag Pensky Martens C losed Cup Flash Tester 2 Wet Chemistry Mitsubishi TOX -10, Total Organic Halogen Analyzer 2 Wet Chemistry Nanopure Type I water fi ltrati on system 1 Wet Chemistry O.I. Analytical, TOC Analyzer 3 Wet Chemistry Sequoia Turner Model 340 UV NIS Spectrophotometer 1 Wet Chemistry Spectronic 2 lD Visi ble Spectrophotometer Houston I 13 8 1 Meadowglen, Suite L, Houston TX 77082 Dallas 9701 Harry Hines Blvd ., Suite D, Da ll as, TX 75220 San Antonio 5332 Bl ac kbe rry, San Antonio, TX 78238 Midland/Odessa 12600 1-20 East, Mid land, TX 79765 Miami 5757 W 15 8th Street, Miami lak es, FL 33014 Tampa 30 16 US Hwy 301 North , Suite 900, Tampa, FL 33619 Atlanta 6017 Financial Drive, Norcross, GA 30071 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 1 Fax: 281 589 0695 214 351 9 139 210 509 3335 432 563 1713 305 823 8555 8 13 620 2033 770 449-5477 14 4. CERTIFIC A TlON S AND ACCREDITATIONS XENCO Laboratories is committed to obtain all certifications and accreditations required and pre-arranged for specific projects. Some Certifications are included in this SOQ . For further information you may contact your Account Executive, Local Lab Manager, or please request Info @xenco.com . 4.1. Certificati o n s and A ccreditations Warning: Certifications and Accreditations are always changing, if you have a project in a state where we do not have a laboratory please check with your XENCO representative on our current status . See Atta ch ed Certifications . Only the most frequ ently requested are enclosed. .., We operate und er ISO guidelines designed for Testing Laboratories and followed by A2LA and NELAC. US Army Corp of Engineers MRD Certifications via NELAP NELAP Accredite d at Houston, Tampa and Miami via the Texas Commission of Environmental Quality and the Department of Health of the State of Florida. NELAP Certification , at any participating State, currently 23 and growing. State of Louisiana. Department of Health and Environment of the State of Kansas. Water Resourc e s Board of the State of Oklahoma. "" AHIA Certi fie d fo r Mo ld A na lys is XENCO Laboratories also conforms with the requirements of the following states: Alabama, Georgia, Hawaii, Idaho, Indiana, Kentucky, Louisiana, Mississippi , Missouri , Montana, Nebraska, New Mexico , Texas, Vermont, Wyoming, etc. ,,. T he State of Texas drink in g water pro gram . ~ We are committed to pursue any certification that your projects may require . Plea se contact our QA/QC Director for further information. We are also associated with ver y reputable Laboratori es across the country whom we may use to better serve your needs and act as a QA resource. 4 .2 . M inority Bus in ess Ce rtific a tion s See Attach ed Certification s. Only th e mo s t frequ ently requ ested are enclosed. ~ We are committed to obtain any certification that you may need. SBA http://pro-net.s b a .gov POl 86628 . .., T exas HUB, Florida MBE Houston I 138 1 Mea do wg len, Suite L, Houston TX 7708 2 Da llas 970 1 Harr y Hin es Bl vd ., Suit e D, Da ll as, TX 75220 Sa n Anto nio 5332 Bl ack ber ry, Sa n Ant on io , TX 78238 Midl and /Odessa 12600 1-20 Eas t, Mid land , TX 7976 5 Mi ami 5757 NW 158 th Str ee t, Miami lakes , FL 330 14 Ta mp a 30 16 US Hwy 30 I No rth , Suit e 900, Tamp a, FL 336 19 Atl ant a 60 17 Fin ancial Dr ive, No rc ross , GA 30 07 1 Phon e: 28 1 589 0692 2 14 902 0300 21 0 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 88 00 Fax: 28 1 589 069 5 2 14 351 9 139 2 105093335 432 563 17 13 305 823 855 5 8 13 620 2033 770 44 9-5 477 15 ta Florida Counties : Miami-Dade, Hillsborough and Jacksonville Texas Cities: Houston, Austin, Dallas, and San Antonio DBE with NCTRCA, SCTRCA, DOT and Airport Authorities 4 .3 T hird p a rty A cc red i ta tion s The American Association for Laboratory Accreditation (A2LA) accredited XENCO Laboratories for technical competence in the field of enviromnental testing from 1992-1998 . The accreditation was not renewed as it was not requested by clients. If it is instrumenta l to your sales efforts let us know . XENCO is currently certified and accredited via NELAC at Houston, Tampa and Miami. Certifications enclosed. XENCO is also accredited by the ACIL for environmental laboratory analysis. Ho uston 11 38 1 M ead owg le n, S uit e L, Ho us ton T X 77082 Da ll as 970 1 Harr y Hin es Bl vd., S uite D, Da ll as, T X 7 5220 Sa n A nto ni o 5332 Bl ack be rry, San Anton io , T X 7 8238 Mi d land /Odessa 12600 1-20 East , Midl and , T X 7976 5 Mi ami 57 5 7 NW 158th Stree t, Mi ami lakes , F L 33 014 Tam pa 30 16 US Hwy 30 I No rth , S ui te 900, T amp a, FL 3 36 19 Atl anta 60 17 Fin anc ia l Dri ve , Norcross, G A 3 007 1 Phon e: 2 81 589 0 69 2 214 902 0300 21 0 5 09 33 34 432 563 1800 305 823 85 00 8 13 620 2000 770 44 9 8800 Fax: 28 1 589 0695 2 14 35 1 9 139 21 0509333 5 4 32 56 3 17 13 305 823 8555 8 13 620 2033 770 449 -5477 16 5. QUALITY PE RFORMANCE 5 .1. Quality S tatem e nt XENCO Laboratories meets the quality standards and adheres to the specifications and guidelines regarding sample handling, analytical methodologies, data reporting as required by our clients , or as promu lgated by applicable local, state, and /or federal regu lator y agencies. The XENCO Commitment states the philosophy and spirit of our mission: An alytical services of the highest quality consistent with our clients' needs . ~ Defensible and Dependable data . .., Reports on time, every time. Unique services and value for every client. Custom reports unm atched in the industry . .-, Wide rang e of analytical parameters . QN QC requirements fulfilled for every project. ..., Preventing errors instead of correcting errors. Comprehensive technical training. ~ Certified continuing education programs. 4" Nationwide accreditations and certifications to meet individual client needs . . . . All throu gh the concerted efforts of the h ighest quality Systems and best train ed professional staff. 5.2 . QA /Q C Plan and th e Q uality Sys tem XENCO Laboratories' Quality Assurance/Quality Control Manual: ~ States our policies and procedures for guaranteeing data of the highest quality . ....-Is modeled after the AFCEE QAPP . ~ Guarantees compl ete compliance with the TNRCC Superfund Program ~ Is dynamic , changing and adapting to new analytical trends and methodologies . ~ Is enforced throu gh a pro gram of regular internal audits . 4-Ensures that all significant matters of data quality and sample disposition are reported Houston 11 38 1 Mead owg le n, S uit e L, Ho usto n TX 77082 Da ll as 9701 Harry H ines Bl vd ., S uit e D, Da ll as , TX 7 5 220 San A nto ni o 5332 Bl ackb e rr y, San Antonio , TX 78 238 Mid land /Odessa 12600 1-20 Eas t, M idl and , TX 79765 Miami 5757 NW 158 th Street, M iami lakes, FL 3 30 14 Ta mp a 30 16 US Hwy 30 I North , S uit e 900 , Tampa, FL 336 19 Atl ant a 60 17 Fin anc ial Dri ve , Norcross , GA 3 007 1 Phon e : 2 8 1 589 0692 2 14 90 2 0 300 2105 093334 4 32 5 63 1800 305 823 8500 8 13 62 0 2000 770 44 9 8800 Fax: 28 1 5 89 0695 2 14 351 9 139 2 10 509 333 5 432 563 17 13 305 823 8555 8 13 620 2033 770 44 9 -5477 17 .., The QA/QC Manu a l and SOPs are available upon request. 5.3. La borato ry In fo rmation M anagement Sy s tem (LIM S) XENCO 's IMS department is currently implementing a s emi-paperless Laboratory Information Managem ent Sy stem , Enviro LIMS , developed in cooperation with XENCO Softw are. Enviro -LIMS offers the following capabilities : Totall y customi z able laboratory and QA r eports , both hardcopy and electronic. Automated ge neration of complex report data packages such as IRPIMS , CLP and various other lev el II , le vel III and level IV reports . Real time, onlin e data access via our Web site. -4' An el ectronic data v alidation system which allows our analysts to perform data reduction, reportin g and validation more accurately and precisel y w ithout transcription errors . .., Online dat a v alidation and "as ready" data re v iew capabilities by our clients .,, Online sample lo g-in for price discounts for interested clients . .., Bar coding and custom COC's ,.. Compreh ensive project management. .., Complete data m anagement. Full Audit Trail. Data importation and ex portation . El ectronic D ata Va lidations ... \Vhy ENVIRO lAMS: Customi z ed to optimi z e env ironmental lab operations and client satisfaction Virtually re ady to us e -very user friendly Built to operate on web servers , Lan Wan systems, mobile labs Operates on windows 95 -98 , NT, UNIX, Macs , almost any type of env ironm ent or operating system . .., Handles the most intricate details of your operations and industry n eeds Dramatically increas es efficiency, thus boosting employee morale , reducing personn e l, and increasing capacity and throughput ,.. Provid es a s erious competitive edge An yon e can afford it System specifications: Houston 1138 1 Mead owg le n, S uit e L, Ho usto n TX 77082 Da ll as 9 70 1 Ha rr y Hin es B lvd ., S ui te D , Da ll as , TX 75 22 0 San A nto n io 5332 B lackberry, San A nt o nio , TX 7823 8 Midl and/Odessa 12600 1-20 Eas t , M id land , T X 7976 5 M iami 5757 NW 158th Street, M iami lakes, FL 330 14 Tampa 30 16 US Hw y 30 I No rth , S uite 900 , Tamp a, FL 336 19 A t la nta 60 17 Fin anc ia l Dri ve , Norc ro ss , GA 3007 1 Ph o ne: 281 5 89 0692 2 14 902 0 300 2 105093334 43 2 563 1800 305 823 8 500 8 13 620 2000 770 44 9 8800 Fax : 28 1 5 89 069 5 21 435 1 9 139 2 105093335 4 32 5 63 17 13 305 823 8555 8 13 620 2033 770 449 -54 77 18 On Oracle , design for the next century User customizable Multi-level user access configuration .i,. Create new variables or modify existing fields. Change their color, fonts, labels , hints, help programs , and even the language for overseas operations Create or modify modules. Move or hide screens among modules or change their icons and user access rights. 4' Links to MS Office , accounting programs and many other applications. " Embed documentation where needed. Scan on-line, import or copy/paste SOPs, MS-DSS, guidance documents , contracts, forms, and raw data, etc. And take control of access, usage, versions, distribution , etc . Make them part of your database . + Embed critical photographs or video clips automatically, e.g. Coolers, samples, chromatographs, customers , employees, products , and training. Disk space is your only limitation . .., Expert off-line data navigator tool. Analyze your data and create reports as needed, e.g. Data validations, historical data review, work schedules, performance, capacity, revenues, inventory management, tracking, projections, technical information , methodologies, regulatory information, QNQC, human and physical resources, capabilities, control charting, electronic audits, audit trails, etc. Quotes management: " Link them to projects and master quotes ., One project may have many quotes .., Set your terms, conditions and SDGs " Establish delivery schedules for samples + Handles any type of billable service " Add fields of information, track status " Revenue projection and tracking tool Pro_jcct management: .i,. Manage contract requirements and multi-level of projects " Create project specifications including " Methods and Analytes .:, Reporting Limits and MDLs " QNQC Criteria " EDD Specifications Hou ston I 1381 Meadowg len, Suite L, Hou s ton TX 77082 Da llas 9701 H ar ry Hine s Blvd ., Su ite D , Dallas, TX 75220 San A nton io 5332 Bl ack berry, Sa n Anto nio , TX 78238 Midl a nd/Odessa 12600 1-20 East , Midland , TX 79 76 5 Miami 5757 NW 15 8th Street, Miami lakes , FL 3 30 14 T a mpa 3016 US Hwy 30 I North , Suite 900 , Tampa, FL 336 19 Atlanta 6017 Financial Dri ve , Norcross , GA 30071 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 Fa x : 28 1 589 0695 214 351 9139 2 10 509 3335 432 563 17 13 305 823 8 555 8 13 620 2033 770 449-5477 19 -., Used to create sampling kit labels and expedites sample login ., Links to jobs/work orders, kits , quotes ... Customize EDDs and data packages ., Track all project related addresses \Vork orders and sample login : ., Links to projects , kits and quotes .. Kit orders generated over the Internet and delivered via e-mail to the project managers. Bar-coded labels and pre-printed COCs Comprehensive work scheduling tools ., Track containers p er cooler and COC Take pictures or video clips of each container and or cooler as desired ,.. Define the analytical requirements per method including: sample preparations , MDLs, units , replicates, dilutions , etc. Create Non-confonnances associated to sampling and shipping. Data management and Reporting: .., Generate batches and sequences of various types: sample prep, analysis , MDL studies, calibrations, etc. 4 No manual data entry if a computer interface is available. 4 Electronic d ata validation and automatic dat a flagging ., Merge results of Dilutions into a single run . Fast Reporting w ith Automated EDDs, e.g. TRRP , AFCEE, CLP ... ., View your data or partial results over the Web ., Automate all reporting data packages ~ Electronic Data reporting with version control ., Ensures that EDDs and Report match. ' Many other tools and features ... Contacts and companies: ., Contacts m anagement link ed to your historical data .., Create relationships between contacts ., Tracks a ll phone numbers and addresses 5.4. Performance Evaluation Testing Houston 113 8 1 Meadowglen , Sui te L, Houston TX 77082 Da ll as 970 1 Harr y Hin es Blvd., Su ite D, Dallas, TX 75220 San Antonio 5332 Blackberry, San Antonio, TX 78238 Midland/Odessa 12600 1-20 East, Midland , TX 79765 Miami 5757 NW 158th Street, Mi ami lakes , FL 330 14 Tampa 30 16 US Hwy 30 I North , Suite 900, Ta mpa , FL 336 19 At lan ta 60 17 Fin anci a l Dri ve , Norcross, GA 30071 Phone: 281 589 0692 214 902 0300 2 10 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 Fax: 28 1 5 89 0695 2 14 351 9139 2105093335 432 563 1713 305 823 855 5 8 13 620 2033 770 449-5477 20 -.. Participation in Blind Performance Evaluation Studies, averaging on all parameters above 95%. Less than 5% of the Laboratories in the nation have such scores . .,, XENCO has always scored between 90-100% in every section. ' Third p arty PET Program and other round robin programs specified by our clients. 5.5. Present and Past Laboratory Audits • Clients or their designated representatives are granted access to audit as needed. Internal audits per our QNQC Manual. .,, The Laboratory Mangers and the QNQC Director enforce routine inspections and technical evaluations program. Independent, comprehensive audits and on-site assessments .,, The TCEQ frequently audits or Texas Laboratories The Department of Health Services of the State of California US Army Corp of Engineers MRD Certifications for a wide variety of parameters. Department of Health of the State of Florida. ~ We will pursue any certification that you may need if the volume grants the process . Other includes : A2LA, New York, Oklahoma and Louisiana 5.5. Policy on Subcontracting XENCO Laboratories will directly and effectively perform at our facilities all analyses, which are requested by our clients and are compatible with our present capabilities. No back-up laboratory will be used without the express approval of the client. Should the need arise, an independent laboratory will be subcontracted for the specific task of completing analytical work not currently performed at our facilities or in the case of temporary limitations in our capacity. Our client will be notified about the conditions for the subcontracted analyses and our standard operating procedure for the transfer of sample custody. XENCO Laboratories r equires subcontract laboratories to be accredited by the NELAC. We audit and carefully evaluate the results of EPA proficiency evaluation tests available from any subcontracting laboratory . Analytical reports submitted to XENCO by subcontracting Laboratories must include a QNQC data package , as specified by our SOP , for technical data validation. Houston I 138 1 Meadowglen , Suite L, Hou ston TX 77082 Dallas 9701 Harry Hines Blvd., Suite D, Dallas, TX 75220 Sa n Antonio 5332 B lackberry, San Anto nio, TX 78238 Midland/Odessa 12600 1-20 East , Midland , TX 79765 Miami 5757 NW 158th Street , Miami lakes, FL 33014 Tampa 3016 US Hwy 30 I North , Suite 900 , Tampa, FL 336 19 At lanta 60 17 Fin a nc ial Drive, No rcross , GA 3007 1 Phon e : 281 589 0692 2 14 902 0300 2 10 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 Fax: 28 1 589 0695 214 35 1 9 139 2105093335 432 563 1713 305 823 8555 813 620 2033 770 449-5477 21 6. SAMPLE CUSTODY 6.1. Sample Integrity XENCO Laboratories complies with the policies and procedures of the National Enforcement Investigation Center of the EPA and the AFCEE program for evidence and documentation of sample custody and integrity. Strict quality control is maintained, from sample receipt through final disposal according to the guidelines of our QA/QC Manual. 4' Samples are properly archived for at least seventy days from sample receipt, unless otherwise requested by the client. 6.2. Chain of Custody The Chain of Custody (COC) covers all steps from collection to proper sample disposal. XENCO's customized COC forms accurately record all significant details of the integrity and characteristics of all samples. In addition, a computer-generated listing of the sample analytical parameters is used to control sample transfer and facilitate sample tracking within the laboratory. Our new LIMS maintains electronic Custody of samples at all times and amounts of sample available at any stage of analysis throughout the life of the sample. Enviro LIMS has built in capabilities to store pictures of coolers , samples and sample extracts that could be of interest in litigation projects . Special project handling is available for projects under Litigation. Contact Brent Barron, your Local Laboratory Manger or your Project Manager for further details. 6.3. Sample Disposal Our LIMS is capable of tracking all samples for Cradle to Grave at all stages of flow throughout the Laboratory until properly disposed and accounted for. We routinely dispose samples and extracts at no cost to the client, unless some extenuating circumstances call for additional charges. Samples are hold for a minimum of 60 days fom1 sample receipt unless otherwise agreed in writing. Hou ston I 138 1 Meadowg le n, Suite L, Houston TX 77082 D a lla s 9701 Harry Hin es Blvd., Suite D, Dallas , TX 75220 San Antonio 5332 Bl ackberr y, San Antonio , TX 78 238 Midland/Odessa 12 600 l-20 East, Midland , TX 79765 Miami 5757 NW 15 8t h Street, Miami lak es, FL 33014 Tampa 3016 US Hw y 301 North , Suite 900 , Tampa, FL 33619 Atlanta 6017 Financial Drive, Norcross, GA 30071 Phone: 281 589 0692 21 49020300 210 509 3334 432 563 1800 305 823 85 00 813 620 2000 770 449 8800 Fax : 281 589 0695 214 351 9139 210 509 3335 432 563 1713 305 823 8555 8 13 620 2033 770 449-54 77 22 7. COURIER SERVICES Our ultimate goal is to provide simple and convenient services. We will adapt our systems to suit your needs. Our normal operating procedures are as follows: 7.1. Ground Shipments -Sampling Kits Delivery Free sample pick-up and delivery of sample containers ~ 8:00 a.m. to 5 :00 p.m., Monday through Friday -. Call your Local Laboratory to schedule a sample drop off after business hours. 4" Test kits requested shipped via regular UPS, unless otherwise requested. Additional charges may apply. All sampling kits can be prepared within hours and shipped or delivered the same day . .., We will serve your needs around the clock and around the year. Sample pick-up and delivery is free within 40 miles to the Laboratory unless otherwise pre- arranged . ., There will be $50 charge for pick-ups after hours or weekends . ,i;, All supplies typically returned to the Lab are free including regular bottles, COCs, Labels, packing materials. Some specialty containers will be billed to you at cost. ~ There will be a charge for specialty containers, i.e. Teddlar Bags , 5035 Sampling containers, Air Analysis Containers, etc . 7.2. Air Shipments Our ultimate goal is to be simple and convenient. Thus, we can adapt our systems to suit your needs. Typically, express airmail or rush air shipments will be the responsibility of the client .., However, XENCO Laboratories can manage air shipments through our accounts and will pass the invoice amount to the client. Or, Cost of inbound shipments can be incorporated in the unit cost per sample. Preferred carriers: within Texas Lone Star anywhere or FedEx. The bus system (Greyhound) is proving to be a viable, reliable and more economical alternative to air shipments for short distances , especially if direct routes are available. Houston I 1381 Meadowglen, Suite L, Houston TX 77082 Dallas 9701 Harry Hines Blvd., Suite D, Dallas , TX 75220 San Antonio 5332 Blackberry, San Antonio, TX 78238 Mid land/Odessa 12600 1-20 East, Midland, TX 79765 Miami 5757 NW 15 8th Street, Miami lakes , FL 33014 Tampa 30 16 US Hwy 301 No rth , Suite 900, Tampa, FL 33619 Atlanta 6017 Financia l Drive, Norcross, GA 30071 Phone : 281 589 0692 214 902 0300 210 509 3334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 Fax: 281 589 0695 214 351 9 139 2105093335 432 563 1713 305 823 8555 813 620 2033 770 449-5477 23 8. SPECIAL TY SERVICES 8.1. Expert Witness Testimony Our services go beyond the ordinary UST and Classical Chemistry testing Laboratories. Our vast and in-depth expertise in a myriad of analytical methodologies, compliance and regulatory programs coupled with individual lines of expertise in specialty parameters and fuel fingerprinting could be of much value to your next Litigation project. Our personnel have served as technical experts on both sides of the fence in numerous occasions in a multitude of projects including: Creosote Contaminated Sites Impacting Hundreds of Residents -.. Fuel Fingerprinting .-, Plume Delineation and Product Characterization -.. Contaminated Drinking Water Allergic Reactions Product Trace-ability and Aging Characterization ..,, Dredging Investigations ~ Research and Development Bio-Remediation Breakdown of products Research and Development. .. 8.2. Software Development XENCO Software, a sister company, has over 15 years of expertise in developing app lications in all phases of Accounting, Inventory Tracking, Time Management, Project Management, LIMS and many more Modules for a large variety of industries. We are continuously working on developing better systems to deliver electronic data and creating paper-less systems to deliver reports and all phases of communication. A Virtual Private Network, VPN, system has been implemented and it is cunently being fine-tuned to provide our clients and employees an Internet access to our LIMS. 8.3. Mobile Laboratories XENCO Laboratories is proud to offer On-Site Laboratory Services (OLS) on the Southeastern region of the USA. Our goals are to quickly set up a fleet of three Hou s ton 113 8 1 Meadowg len , Suite L, Hou s ton TX 77082 Da ll as 9701 Ha rr y Hine s Blvd ., Sui te D , Dallas, TX 75220 San Antonio 5332 Blackberry, Sa n Antonio, TX 7823 8 Midl and /Odessa 12600 1-20 East , Mid land , TX 79765 Mi a mi 5 757 NW 15 8th Street, Mi a mi Jak es, FL 33014 T a mpa 3016 US Hwy 30 I North , Suite 900, Tampa, FL 33619 Atlanta 6017 Financial Drive , Norcross, GA 30071 Phone: 281 589 0692 214 902 0300 2105093334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 Fax : 281 5 89 06 95 214 351 9 139 2105093335 4325631 7 13 305 823 8555 8 13 620 20 3 3 770 449-5477 24 Mobile Laboratories to serve the state of Florida and its surrounding areas . However, if a project is large enough, we will travel wherever it m ay be n eeded dependin g on yo ur specific need s. The first two la boratories are now read y . We are currently deve loping analytical methodologies and instrument configurations to deliver a much larger throughput of analysis per hour. Some of these m ethod s could result on the d e livery of as much as ten analyses per hour for several parameters . All instrume ntat ion is fully automated and completely inte grated within our netwo rk . Eve ry Mobile Laboratory is or will be NELAC Accredited for a specific set of paramete rs. Bi g Bertha or 101 is located in Miami and equipped to deli ver VOCs (826 0 , 624 and/or 8021) by GC-MS . But the vehicle is retrofitted to handle FL- PRO TPH, GRO , DRO , PAHs, and ICP . If your proj ect goes beyond GC -MS YOCs pl ease schedule it with ample time , at le ast 4 weeks. 8.4. Asbestos Ana lyses NVLAP Accredited for Polarized Light Microscopy (PLM) Texas Dept. of State Health Services Licensed for PLM. and PCM A w ide se lection of turnaround times is available , including same day. Pricing is ve ry competitive. • Bulk Materials by PLM (EPA 600/R -93/116 method) • Air Samples b y PCM (NIOSH 7400 method) Xenco's asbestos team has provided service to a broad range of clients , ranging from large municipal projects and major engineering firms do w n to indi v idual hom eowners. Xenco is the prime asbestos laboratory contractor for DFW Inte rnational A irport. Xenco is a lso one of very few , if not the only , MBE/DB E certified PLM as besto s labs in the DFW area. Our Asb estos team benefits from the leadership of Chris Munch, BS in Physics - University of Texas at Dall as. Mr. Munch has worked in the asbestos te sting indu stry s ince 1989 including positions at several different NVLAP accredited labs in th e Dall as are a. Ho uston I 138 1 Meadowg len , Sui te L, Hou ston TX 77082 Dallas 970 I Harry Hine s B lvd., Suite D, Da ll as, TX 75220 San A nto nio 5332 Blackberry, San Antonio, TX 78238 Mid land /Odessa 12600 1-20 East, Midland , TX 79765 Mi ami 5757 NW 15 8th Street, M iami lake s, FL 330 14 Tampa 30 16 US Hwy 30 1 North , S uit e 900 , Tampa, FL 336 19 Atlan ta 60 17 Financ ial Drive , No rcro ss , GA 3007 1 Phone: 28 1 589 0692 2 14 902 0300 2 105093334 432 563 1800 305 823 8500 8 13 620 2000 770 449 8800 Fax : 281 589 0695 2 1435 1 9 139 2 10 509 3335 432 563 17 13 305 823 8555 8 13 620 2033 770 449-5 477 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Accreditation is hereby awarded to XENCO Laboratories 11381 Meadowglen Lane, Suite L Houston, TX 77082-2647 in accordance with Texas Water Code Chapter 5, Subchapter R, Tide 30 Texas Administrative Code Chapter 25, and the National Environmental Laboratory Accreditation Program. T he laboratory's scope of accreditation includes the fields of accreditation that accompany this certificate. Continued accreditation depends upon successfu l o ngoing participation in the program. The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and ana lyses. Certificate Number : Effective Date : Expiration Date : T l047042 l 5-07-TX July 1, 2007 June 30, 2008 Executive Director Texas Commission on Environmental Quality TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Exp irat ion Date : June-30-2008 Th ese fi e ld s of accred itation supercede all previou s fie ld s. The Te xas Comm ission on Env ironmenta l Qual ity urges customers to ve rify the lab orato ry 's current ac creditation status fo r particular methods and analyses . Fields of Accreditation Matrix: Drinking Water Category/Method: Metals/EPA 200.8 Analytes: Code: CAS No.: Antimony Barium Cadmium Copper Mercury Selen ium Category/Method: General Chemistry/EPA 300.0 Analytes: Code: CAS No.: Fluoride Category/Method: General Chemistry/EPA 335.4 Analytes: Code : CAS No.: Cyan ide Analytes: Arsenic Beryllium Chrom ium Lead Nickel Thallium Analytes: Nitrate as N Analytes: Category/Method: Disinfection By-products/EPA 524 .2 Analytes: Code: CAS No.: Analytes: Trihalomethanes , Total Category/Method: voes by GCIMSIEPA 524 .2 Analytes: Code: CAS No.: 1, 1, 1-Trichloroethane 1, 1-Dichloroethylene 1,2-Dic hlorobenzene 1,2-Dich loropropane Benzene Chlorobenzene Dich loromethane (Methylene Chloride ) Styrene Toluene T rich loroethylene Xy lenes , meta , para Xylenes , Total Analytes: 1, 1,2-Trichloroethane 1,2,4-Trichlorobenzene 1,2-Dichloroethane 1,4-Dichlorobenzene Carbon tetrachloride c is-1 ,2-Dichloroethylene Ethylbenzene Tetrachloroethylene trans -1,2-Dichloroethylene V inyl Chloride Xylenes , ortho Page 1 of 22 Code: CAS No .: Code: CAS No.: Code: CAS No .: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accreditation supercede all previous fields . The Texas Commiss ion on Env ironmental Quality urges customers to verify the laboratory 's current accreditation status for particular methods and analyses . Matrix: Drinking Water Category/Method: Organics by GCIEPA 508 Analytes: Code: CAS No.: Chlordane, Technical Heptachlor Hexachlorobenzene Lindane (g-BHC) PCBs (screen as Aroclors) Category/Method: Organics by GCIEPA 515.1 Analytes: Code: CAS No.: 2,4 ,5-TP (Silvex) Dalapon Pentachlorophenol Category/Method: SVOCs by GC/MSIEPA 525.2 Analytes: Code: CAS No.: Benzo(a)pyrene Di(2-Ethylhexyl) phthalate Matrix: Solid and Chemical Materials Category/Method: Metals/EPA 6020A Analytes: Code: CAS No.: Aluminum Arsenic Beryllium Cadm ium Chromium Copper Lead Manganese Nickel Selen ium Sodium Thallium Titanium Zinc Analytes: Endrin Heptachlor epoxide (beta) Hexachlorocyclopentadiene Methoxychlor Toxaphene (total) Analytes: 2,4-0 (acid , salts and esters) Dinoseb Picloram Analytes: Di(2 -Ethylhexyl) adipate Analytes: Antimony Barium Boron Calcium Cobalt Iron Magnesium Molybdenum Potassium Silver Strontium Tin Vanadium Page 2 of 22 Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENT AL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Issue Date : July-01-2007 Expiration Date: June-30-2008 These fields of accred itation supercede all previous fields . The Texas Commission on Env ironmental Quality urges customers to verify the laboratory 's current accreditat ion status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: Metals/EPA 7190 Analytes: Code: CAS No.: Chromium VI Category/Method: Metals/EPA 7191 Analytes: Code: CAS No.: Chromium VI Category/Method: Waste Characteristics/EPA 1010 Analytes: Code: CAS No.: lgnitability Category/Method: General Chemistry/EPA 300.0 Analytes: Code: CAS No.: Bromide Fluoride Nitrate-Nitrite (as N) Orthophosphate (as P) Category/Method: General Chemistry/EPA 1664 Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Category/Method: General Chemistry/EPA 9014 Analytes: Code: CAS No.: Cyanide , Amenable Category/Method: General Chemistry/EPA 9020 Analytes: Code: CAS No.: Total Organic Halides (TOX) Category/Method: General Chemistry/EPA 9023 Analytes: Code: CAS No.: Extractable Organic Halides (EOX) Analytes: Analytes: Analytes: Analytes: Chloride Nitrate (as N) Nitrite (as N) Sulfate Code: Code: Code: Code: CAS No.: CAS No.: CAS No.: CAS No.: Analytes: Code: CAS No.: Silica Gel Treated n-Hexane Extractable Material (SGT· HEM) Analytes: Code: CAS No.: Cyanide , Total Analytes: Code: CAS No.: Analytes: Code: CAS No.: Page 3 of 22 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston, Texas 77082 Issue Date: July-01-2007 Expiration Date: June-30-2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Qual ity urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Solid and Chemical Materials Category/Method: General Chemistry/EPA 9040 Analytes: Code: CAS No.: pH Category/Method: General Chemistry/EPA 9045 Analytes: Code: GAS No.: pH Category/Method: General Chemistry/EPA 9050 Analytes: Code: CAS No.: Specific Conductance (Conductivity) Category/Method: General Chemistry/EPA 9056 Analytes: Code: CAS No.: Bromide Fluoride Nitrite (as N) Orthophosphate (as P) Category/Method: General Chemistry/EPA 9060 Analytes: Code: CAS No.: Organic Carbon, Total (TOC) Category/Method: General Chemistry/EPA 9065 Analytes: Code: CAS No.: Phenols Category/Method: General Chemistry/EPA 9070 Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Category/Method: General Chemistry/EPA 9071 Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Analytes: Analytes: Analytes: Analytes: Chloride Nitrate (as N) Nitrate-Nitrite (as N) Sulfate Analytes: Analytes: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Analytes: Code: CAS No.: Silica Gel Treated n-Hexane Extractable Material (SGT- HEM) Analytes: Code: CAS No.: Silica Gel Treated n-Hexane Extractable Material (SGT- HEM) Page 4 of 22 TEXAS COMMISSION ON ENVIRONMENT AL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 1138 1 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01 -2007 Expiration Date : June-30-2008 These fie lds of acc red itation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: voes by GC/MSIEPA 8260 Analytes: Code: CAS No.: 1, 1, 1,2-Tetrachloroethane 1, 1,2 ,2-Tetrachloroethane 1, 1-Dichloroethane 1, 1-Dichloropropene 1,2 ,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2-Dibromo-3-chloropropane (DBCP) 1,2-Dichlorobenzene 1,2-Dichloropropane 1,3-Dichloropropane 1-Chlorohexane 2 , 2-Dich loropropane 2-Chlorotoluene 2-Pentanone 4-Chlorotoluene Acetone Acetonitrile Benzene Bromobenzene Bromodichloromethane Carbon disulfide Chloroethane Chloromethane cis-1 ,2-Dichloroethene cis-1 ,4-D ichloro-2-butene Dibromomethane Ethyl methacrylate Hexachlorobutadiene Methyl tert-butyl ether (MTBE) Naphthalene Nitrobenzene Styrene Tetrachloroethene trans -1,2-Dichloroethene trans-1,4-D ichloro-2-butene Tri c hlorofluoromethane Analytes: Code: 1, 1, 1-Trichloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2,3-Trichloropropane 1,2 ,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichloroethane 1,3,5-Trimethylbenzene 1, 3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone (MEK) 2-Chloroethyl vinyl ether 2-Hexanone (MBK ) 4-lsopropyltoluene 4-Methyl-2-pentanone (MIBK) Acrolein Acrylon itrile Bromochloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroform cis-1 , 3-Dichloropropene Dibromoch loromethane Dichlorodifluoromethane Ethylbenzene I sopropylbenzene Methylene chloride n-Butylbenzene n-Propylbenzene sec-Butylbenzene tert-Butylbenzene Toluene trans-1 , 3-Dichloropropene Trichloroethene Page 5 of 22 CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recogoized Laboratory Fields of Accreditation ~(/ ''\"' r H O~\ Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accreditat ion supercede all prev ious fi e lds . The Texas Commission on Environmental Qual ity urges c usto mers to verify the labo rat ory 's current accreditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: voes by GCIMSIEPA 8260 (cont.) Analytes: Code: CAS No.: Vinyl chloride Xylenes , meta , para Xy lenes, Total Category/Method: SVOCs by GC/MS/EPA 8270C Analytes: Code: CAS No.: 1,2,4-Trichlorobenzene 1,2-Diphenylhydrazine 1,4-Dichlorobenzene 1-Chloronaphthalene 2,4 ,5-Trichlorophenol 2 . 4. 6-T richlorophenol 2 ,4-D ichlorophenol 2,4-Dinitrophenol 2-Chloronaphtha lene 2-Methylnaphthalene 2-Methylphenol 2-Nitrophenol 3. 3' -Dich lorobenz idine 3-Nitroaniline 4-Chloroaniline 4-Methylphenol 4-Nitroaniline Acenaphthene Acetophenone Anthracene Benzid ine Benzo(b )fluoranthene Benzo(k )fluoranthene Benzyl alcohol Bis(2 -chlorethoxy)methane Bis (2-chloroisopropyl)ether Bis (2-ethylhexyl )phthalate Chrysene Dibenzofuran Dimethyl phthalate Analytes: Vinyl acetate Xylene , ortho Analytes: 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,3-Dinitrobenzene 2 ,3 ,4 ,6-Tetrachlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene 2 , 6-Dinitrotoluene 2 ,6-Dichlorophenol 2-Chlorophenol 2-Methyl-4 ,6-dinitrophenol 2-Nitroaniline 2-Picoline 3-Methylphenol 4-Bromophenyl phenyl ether 4-Chloro-3-methylphenol 4-Chlorophenyl phenyl ether 4-Nitrophenol Acenaphthylene Aniline Azobenzene Benz( a )anthracene Benzo(a)pyrene Benzo(g ,h ,i)perylene Benzoic acid Benzyl butyl phthalate Bis (2-chloroethyl)ether Carbazole Dibenz(a , h)anthracene Diethyl phthalate Di-n-butyl phthalate Page 6 of 22 Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accreditation supercede all prev ious fields . The Tex as Commission on Environmental Quality urges customers to veri fy the laboratory's current accreditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: SVOCs by GCIMS/EPA 8270C (cont.) Analytes: Code: CAS No.: Analytes: Code: Oi-n-octyl phthalate Diphenylaminie Ethyl methanesulfonate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachloroethane Hexachlorocyclopentadiene Hexachloropropene lndeno(1 ,2,3-c,d)pyrene lsophorone Methapyrilene Methyl methanesulfonate Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitrosodiethylamine N-Nitrosod i-n-propylamine N-Nitrosodi-n-butylamine N-Nitrosomethylethylaminie N-Nitrosodiphenylamine N-Nitrosopiperidine N-Nitrosomorpholine N-Nitrosopyrrol idine Pentachloron itrobenzene Pentachlorobenzene Pentachlorophenol Phenanthrene Phenol Pyridine Pyrene Category/Method: Organics by GCITCEQ 1005 Analytes: Code: CAS No.: Analytes: Code: Total Petroleum Hydrocarbons Category/Method: Organics by GCIEPA 8015 Analytes: Code: CAS No.: Analytes: Code: Diesel Range Organics (ORO) Gasoline Range Organics (GRO) Category/Method: Organics by GCIEPA 8021 Analytes: Code: CAS No.: Analytes: Code: Benzene Methyl tert-butyl ether (MTBE) Xylenes , meta , para Xylenes , Total Ethyl benzene Toluene Xylene , ortho Page 7 of 22 CAS No.: CAS No.: CAS No.: CAS No .: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01 -2007 Expiration Date : June-30-2008 These fields of accreditation supercede all previous fields . The Te xas Comm ission on Environmental Quality urges customers to verify the laboratory's current acc reditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: Organics by GCIEPA 8081 B Analytes: Code: CAS No.: 4,4'-DDE 4,4 '-DDT Aldrin Chlordane, alpha Chlordane , technical ODD , Total DDT, Total Endosulfan I Endosulfan sulfate Endrin aldehyde g-BHC (Lindane) Heptachlor epoxide Hexachlorocyclopentadiene Toxaphene Category/Method: Organics by GC!EPA 80828 Analytes: Code: CAS No.: PCB-1016 PCB-1232 PCB-1248 PCB-1260 2-Chlorobiphenyll 2 ,2',3 ,5'-Tetrachlorobiphenyl 2 ,2',5 ,5 '-Tetrach lorobiphenyl 2 ,3',4,4'-Tetrachlorobiphenyl 2 ,2', 4 , 5 , 5'-Pentachlorobiphenyl 2 ,2',3 ,4 ,5 ,5 '-Hexachlorobiphenyl 2 ,2',3 ,5 ,5',6-Hexachlorobiphenyl 2 ,2 ',3 ,3',4 ,4',5-Heptachlorobiphenyl 2 ,2 ',3 ,4 ,4',5',6-Heptachlorobiphenyl 2 ,2 ',3 ,3',4,4',5 ,5',6-Nonachlorobiphenyl Analytes: 4,4'-DDD a-BHC b-BHC Chlordane , gamma d-BHC ODE , Total Dieldrin Endosulfan II Endrin Endrin ketone Heptachlor Hexachlorobenzene Methoxychlor Analytes: PCB-1221 PCB-1242 PCB-1254 PCBs , Total 2 ,3-Dichlorobiphenyl 2 ,2', 5-Trichlorobiphenyl 2,4' ,5-Trichlorobiphenyl 2 ,2', 3' ,4 , 5-Pentachlorobiphenyl 2 , 3 , 3' ,4', 6-Pentachlorobiphenyl Code: Code: 2 ,2' ,3,4,4' ,5'-Hexachlorobiphenyl 2 ,3 ,3',4 ,5,5'-Hexachlorobiphenyl 2 ,2',3 ,4,4',5 ,5'-Heptachlorobiphenyl 2 ,2',3 ,4 ',5 ,5',6-Heptachlorobiphenyl Page 8 of 22 CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accreditation supercede all previous fields . The Te xas Commission on Environmental Quality urges customers to ver ify the laboratory's current accreditation status for particular methods and analyses . Matrix: Solid and Chemical Materials Category/Method: Organics by GC!EPA 8151 Analytes: Code: CAS No.: 2,4 ,5-T 2,4-D Dalapon Dinoseb Picloram Category/Method: Organics by HPLCIEPA 8310 Analytes: Code: CAS No.: Acenaphthene Anthracene Benzo( a )pyrene Benzo(g , h,i)perylene Chrysene Fluoranthene lndeno(1,2 ,3-c ,d)pyrene Phenanthrene Matrix: Non-Potable Water Category/Method: Metals/EPA 200.8 Analytes: Code: CAS No.: Aluminum Arsenic Beryllium Cadmium Chromium Copper Lead Manganese Nickel Selenium Silver Strontium Tin Vanadium Analytes: 2,4,5-TP (Silvex) 2,4-DB Dicamba Pentachlorophenol Analytes: Acenaphthylene Benzo( a )anthracene Benzo( b )fluoranthene Benzo(k)fluoranthene Dibenzo(a,h)anthracene Fluorene Napthalene Pyrene Analytes: Antimony Barium Boron Calcium Cobalt Iron Magnesium Molybdenum Potassium Silica, Dissolved Sodium Thallium Titanium Zinc Page 9 of 22 Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date: July-01-2007 Expiration Date : June-30-2008 These fields of accreditation supercede all prev ious fields . The Texas Commissi on on Environmental Quality urges customers to verify the laboratory 's current accreditation status for part icular methods and analyses . Matrix: Non-Potable Water Category/Method: Metals/EPA 6020A Analytes: Code: CAS No.: Aluminum Arsenic Beryllium Cadmium Chromium Copper Lead Manganese Nickel Selenium Sodium Thallium Titanium Zinc Category/Method: Metals/EPA 7190 Analytes: Code: CAS No.: Chromium VI Category/Method: Metals/EPA 7191 Analytes: Code: CAS No.: Chromium VI Category/Method: General Chemistry/EPA 110.2 Analytes: Code: CAS No.: Color Category/Method: General Chemistry/EPA 120 .1 Analytes: Code: CAS No.: Specific Conductance Category/Method: General Chemistry/EPA 130.2 Analytes: Code: CAS No.: Hardness, Total Analytes: Antimony Barium Boron Calcium Cobalt Iron Magnesium Molybdenum Potassium Silver Strontium Tin Vanadium Analytes: Analytes: Analytes: Analytes: Analytes: Page 10 of 22 Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date: June-30-2008 These fields of accreditation supercede all prev ious fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory 's current accred itat ion status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 150.1 Analytes: Code: CAS No.: pH Category/Method: General Chemistry/EPA 160.1 Analytes: Code: CAS No.: Residue , Filterable (TDS) Category/Method: General Chemistry/EPA 160.2 Analytes: Code: CAS No.: Residue , Nonfilterable (TSS) Category/Method: General Chemistry/EPA 160.3 Analytes: Code: CAS No.: Residue, Total Category/Method: General Chemistry/EPA 160.4 Analytes: Code: CAS No.: Residue , Volatile Category/Method: General Chemistry/EPA 160.5 Analytes: Code: CAS No.: Residue, Settleable Category/Method: General Chemistry/EPA 180.1 Analytes: Code: CAS No.: Turbidity Category/Method: General Chemistry/EPA 300.0 Analytes: Code: CAS No.: Bromide Fluoride Nitrate-Nitrite (as N) Orthophosphate (as P) Category/Method: General Chemistry/EPA 305.1 Analytes: Code: CAS No.: Acidity Analytes: Analytes: Analytes: Analytes: Analytes: Analytes: Analytes: Analytes: Chloride Nitrate (as N) Nitrite (as N) Sulfate Analytes: Page 11 of 22 Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Issue Date: July-01-2007 Expiration Date : June-30-2008 These fields of accreditation supercede all prev ious fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 310.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Alkalinity Category/Method: General Chemistry/EPA 335.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Cyanide, Available (Amenable) Category/Method: General Chemistry/EPA 335.4 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Cyanide , Total Category/Method: General Chemistry/EPA 350.2 Analytes: Code : CAS No.: Analytes: Code: CAS No.: Ammonia (as N) Category/Method: General Chemistry/EPA 405.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Biochemical Oxygen Demand (BOD) Category/Method: General Chemistry/EPA 413.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Oil & Grease -Total Recoverable Category/Method: General Chemistry/EPA 415.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Organic Carbon, Total (TOC) Category/Method: General Chemistry/EPA 420.1 Analytes: Code: CAS No.: Analytes: Code: CAS No.: Phenols Category/Method: General Chemistry/EPA 1010 Analytes: Code: CAS No.: Analytes: Code: CAS No.: lgnitability Page 12 of 22 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 These fields of accreditation supercede all previous fields . The Texas Comm issio n on Env iro nmenta l Quality urges customers to verify th e laboratory 's current accreditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 1664 Analytes: Code: CAS No.: n-Hexane Extractable Material {HEM) Category/Method: General Chemistry/EPA 7196 Analytes: Code: CAS No.: Chromium VI Category/Method: General Chemistry/EPA 7199 Analytes: Code: CAS No.: Chromium VI Category/Method: General Chemistry/EPA 9014 Analytes: Code: CAS No.: Cyanide, Amenable Category/Method: General Chemistry/EPA 9020 Analytes: Code: CAS No.: Total Organic Halogens (TOX) Category/Method: General Chemistry/EPA 9034 Analytes: Code: CAS No.: Sulfide , Total Category/Method: General Chemistry/EPA 9040 Analytes: Code: CAS No.: pH Category/Method: General Chemistry/EPA 9050 Analytes: Code: CAS No.: Specific Conductance (Conductivity) Analytes: Code: CAS No.: Silica Gel Treated n-Hexane Extractable Material (SGT- HEM) Analytes: Code: CAS No.: Analytes: Code: CAS No.: Analytes: Code: CAS No.: Cyanide , Total Analytes: Code: CAS No.: Analytes: Code: CAS No.: Analytes: Code: CAS No.: Analytes: Code: CAS No.: Page 13 of 22 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June -3 0-2008 These fie lds of accred itation supercede all previous fields . The Texas Commission on Environmental Qual ity urges customers to verify the laboratory 's current accred itati on status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: General Chemistry/EPA 9056 Analytes: Code: CAS No.: Bromide Fluoride Nitrate-Nitrite (as N) Orthophosphate ( as P) Category/Method: General Chemistry/EPA 9060 Analytes: Code: CAS No.: Organic Carbon , Total (TOC) Category/Method: General Chemistry/EPA 9065 Analytes: Code: CAS No.: Phenols Category/Method: General Chemistry/EPA 9070 Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Category/Method: General Chemistry/EPA 9071 Analytes: Code: CAS No.: n-Hexane Extractable Material (HEM) Category/Method: General Chemistry/Hach 8000 Analytes: Code: CAS No.: Chemical Oxygen Demand (COD) Category/Method: voes by GC/MSIEPA 524.2 Analytes: Code: CAS No.: 1,2-Dichlorobenzene 2-P ropanone (Ac etone ) Benzene Chloroform Methyl tert-butyl ether (MTBE) Toluene Analytes: Chloride Nitrate (as N) Nitrite (as N) Sulfate Analytes: Analytes: Code: CAS No.: Code: CAS No.: Code: CAS No.: Analytes: Code: CAS No.: Silica Gel Treated n-Hexane Extractable Material (SGT-HEM) Analytes: Code: CAS No.: Silica Gel Treated n-Hexane Extractable Material (SGT-HEM) Analytes: Code: Analytes: Code: 1,2-Dichloroethane 4-Methyl-2-pentanone (MIBK) Chlorobenzene Methylene Chloride Tetrahydrofuran CAS No.: CAS No.: Page 14 of 22 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of acc reditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory's current accred itat ion status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: voes by GC/MSIEPA 624 Analytes: Code: CAS No.: 1, 1, 1-Trichloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2-Dichlorobenzene 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Chloroethyl vinyl ether Acrolein Benzene Bromoform Carbon Tetrachloride Chloroethane Chloromethane Dibromochloromethane Methylene chloride Tetrachloroethene trans-1 ,2-Dichloroethene Trichloroethene Vinyl chloride Xylenes , meta , para Category/Method: voes by GCIMS/EPA 8260 Analytes: Code: CAS No.: 1, 1, 1,2-Tetrachlorethane 1, 1,2 ,2-Tetrachlorethane 1, 1-Dich loroethane 1, 1-Dichloropropene 1,2 ,3-Trichlorobenzene 1,2 ,4 -Trichlorobenzene 1,2-Dibromoethane (EDS) 1,2 -D ichlorethane 1,3-Dichlorobenzene 1,4-D ichlorobenzene 1-Chlorohexane 2-Butanone (MEK ) 2-Chlorethyl vinyl ether Analytes: Code: 1, 1,2,2-Tetrachloroethane 1, 1-Dichloroethane 1,2-Dibromoethane (EDS ) 1,2-Dichloroethane 1,3-Dichlorobenzene 2-Butanone (MEK) Acetone Acrylonitrile Bromodichloromethane Bromomethane Chlorobenzene Chloroform cis-1, 3-Dich loropropene Ethylbenzene Methyl tert-butyl ether (MTBE) Toluene trans-1 ,3-Dichloropropene Trichlorofluoromethane Xylene, ortho Xylenes , Total Analytes: Code: 1, 1, 1-Trichloroethane 1, 1,2-Trichloroethane 1, 1-Dichloroethene 1,2 ,3-Trichloropropane 1,2 ,4-Trimethylbenzene 1,2-Dichlorobenzene 1,2-Dichloropropane 1, 3 , 5-T rimethylbenzene 1,3-Dichloropropane 1,4-Dioxane 2 ,2-Dichloropropane 2-Chlorotoluene 2-Hexanone (MBK) Page 15 of 22 CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accreditation supercede all previous fields . The Te xas Commission on Environmental Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: voes by GCIMSIEPA 8260 (cont.) Analytes: Code: CAS No.: 2-Pentanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetonitrile Acrylonitrile Bromobenzene Bromodichloromethane Bromomethane Carbon tetrachloride Chlorethane Chloromethane cis-1 ,3-D ichloropropene Dibromochloromethane Dibromomethane Ethyl methacrylate lodomethane Methyl tert-butyl ether (MTBE) Naphthalene Nitrobenzene Styrene tert-Butylbenzene Toluene trans-1 , 3-Dichloropropene Trichloroethene V inyl acetate Xylene , ortho Xylenes , Total Category/Method:SVOCs by GCIMSIEPA 625 Analytes: Code: CAS No.: 1,2 -Dichlorobenzene 1,2 ,4 , 5-T etrachlorobenzene 1,4-Dichlorobenzene 2 ,4 , 5-Trich lorophenol 2 , 4-Dichlorophenol 2,4-Dinitrophenol Analytes: 3-Chloropropionitrile 4-lsopropyltoluene Acetone Acrolein Benzene Bromochloromethane Bromoform Carbon disulfide Chlorobenzene Chloroform cis-1 ,2-Dichlorethene cis-1,4-Dichloro-2-butene Dibromofluoromethane Ethyl acetate Ethyl benzene lsopropylbenzene Methylene chloride n-Butylbenzene n-Propylbenzene sec-Butylbenzene Tetrachloroethene trans-1 ,2 -Dichlorethene trans-1,4-Dichloro-2-butene Trichlorofluoromethane Vinyl chloride Xylenes, meta, para Analytes: 1 ,2,4-Trichlorobenzene 1,3-Dichlorobenzene 2 ,3 ,4,6 -Tetrachlorophenol 2,4 ,6-Trichlorophenol 2,4-Dimethylphenol 2,4-Dinitrotoluene Page 16 of 22 Code: CAS No.: Code: CA$ No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston . Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accred it ation supercede all previous fields . The Te xas Commission on Environmenta l Quality urges customers to verify the laboratory's current accreditation status for particular methods and analyses. Matrix: Non-Potable Water Category/Method:SVOCs by GCIMS/EPA 625 (cont.) Analytes: Code: CAS No.: 2,6-Dinitrotoluene 2-Chlorophenol 2-N itrophenol 4-Bromophenyl phenyl ether 4-C h loro-3-methylphenol Acenaphthene Anthracene Benzo(a)anthracene Benzo(b )fluoranthene Benzo(k)fluoranthene Bis(2-chloroethoxy)methane Bis(2-chloro isopropyl)ether Chrysene Diethyl phthalate Di-n-butyl phthalate Fluoranthene Hexachlorobutadiene Hexachloroethane lsophorone Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-butylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Pyridine Category/Method: SVOCs by GCIMSIEPA 8270C Analytes: Code: CAS No.: 1,2 ,4-Trichlorobenzene 1,2-Dinitrobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2.4 ,5-Trichlorophenol 2 ,4 ,6-Trichlorophenol 2. 4-Dich lorophenol Analytes: 2-Chloronaphthalene 2-Methyl-4 ,6-dinitrophenol 3,3'-D ichlorobenzidine 4-Chlorophenyl phenyl ether 4-N itrophenol Acenaphthylene Benzidine Benzo(a)pyrene Benzo(g ,h ,i)perylene Benzyl butyl phthalate Bis(2-chloroethyl)ether Bis(2-ethylhexyl) phthalate Dibenzo(a,h)anthracene Dimethyl phthalate Di-n-octyl phthalate Fluorene Hexachlorobenzene Hexachlorocyclopentadiene ldeno(1 ,2,3-cd)pyrene Naphthalene N-Nitrosodiethylamine N-Nitrosodi-n-propylamine Pentachlorbenzene Phenanthrene Pyrene Analytes: 1,2-Dichlorobenzene 1,2-Diphenylhydrazine 1 ,3-Dinitrobenzene 1-Chloronaphthalene 2,3,4,6-Tetrachlorophenol 2 ,4-Dimethylphenol 2. 4-Dinitrotoluene Page 17 of 22 Code: CAS No.: Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Issue Date : July-01-2007 Expiration Date : June-30-2008 These fields of accred itati on supercede all previous fi elds . The Te xas Commission on Environmental Qual ity urges customers to verify the laboratory's current ac creditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method:SVOCs by GCIMSIEPA 8270C (cont.) Analytes: Code: CAS No.: Analytes: 2 ,4-Di n itrophenol 2 , 6-Dichlorophenol 2-Chloronaphthalene 2-Methylnaphthalene 2-Nitroaniline 2-Picoline 3-Methylphenol 4-Bromophenyl phenyl ether 4-Chloroan iline 4-Methylphenol 4-N itrophenol Acenaphththylene Aniline Benzidine Benzo(b )fluoranthene Benzo(k)fluoranthene Benzyl alcohol Bis(2-chloroethoxy)methane Bis(2-chlorisopropyl)ether Bis(2 -ethylhexyl)phthalate Chrysene Dibenzo(a,e)pyrene Diethyl phthalate Di -n-butyl phthalate Diphenylamine Fluoranthene Hexachlorobenzene Hexachlorcyclopentadiene Hexachlorpropene lsophorone Napthalene N-Nitrosodiethylamine N-Nitrosodi-n-butylamine N-Nitrosodiphenylamine N-N itrosomorpholine N-N itrosopyrrolidine 2, 6-Dinitrotoluene 2-Chlorophenol 2-Methyl-4 ,6-dinitrophenol 2-Methylphenol 2-Nitrophenol 3,3'-Dichlorobenzidine 3-Nitroaniline 4-Chloro-3-methylphenol 4-Chlorophenyl phenyl ether 4-Nitroaniline Acenapthene Acetophenone Anthracene Benz( a )anthracene Benzo(a)pyrene Benzo(g ,h,i)perylene Benzoic acid Benzyl butyl phthalate Bis(2-chlorethyl)ether Carbazole Dibenz(a ,h)anthracene Dibenzofuran Dimethyl phthalate Di-n-octyl phthalate Ethyl methanesulfonate Fluorene Hexachlorobutadiene Hexachloroethane lndeno(1 ,2,3-c,d)pyrene Methyl methanesulfonate Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosomethylethylamine N-Nitrosopiperdine Pentachlorobenzene Page 18 of 22 Code: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expi ration Date: June-30-2008 These fields of accreditation supercede all previous fields . The Texas Commissio n on Environmental Quality urges customers to verify the laboratory's current accreditat ion status for particular methods and analyses . Matrix: Non-Potable Water Category/Method:SVOCs by GCIMSIEPA 8270C (cont.) Analytes: Code: CA$ No.: Analytes: Code: CA$ No.: Pentachloronitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Category/Method: Organics by GCITCEQ 1005 Analytes: Code: CA$ No.: Analytes: Code: CA$ No.: Total Petroleum Hydrocarbons Category/Method: Organics by GCIEPA 602 Analytes: Code: CAS No.: Analytes: Code: CA$ No.: Xylene, ortho Xylenes , meta , para Xylenes , Total Category/Method: Organics by GCIEPA 608 Analytes: Code: CAS No.: Analytes: Code: CAS No.: 4 ,4'-DDD 4 ,4'-DDE 4,4'-DDT a-BHC Aldrin b-BHC Chlordane, alpha Chlordane , gamma Chlordane , Technical d-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate Endrin Endrin aldehyde g-BHC (Lindane) Heptachlor Heptachlor epo xide Methoxychlor PCB 1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Toxaphene Category/Method: Organics by GCIEPA 610 Analytes: Code: CAS No.: Analytes: Code: CA$ No .: Acenaphthene Acenaphthylene Anthracene Benzo( a )a nth racene Benzo (a )pyrene Benzo(b )fluoranthene Benzo(g ,h, i}perylene Benzo(k)fluoranthene Page 19 of 22 TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Field s of Accreditation Xenco Laborator ies 11381 Meadowglen Lane Houston , Texas 77082 Cert ificate Number: T104704215-07-TX Issue Date : July-01-2007 Ex piration Date : June-30-2008 The se field s of accre d itat ion s upercede all prev io us fields . Th e Texas Comm ission on Environmental Quality urges c ustom ers to ve rify the lab or atory 's c urre nt accred ita t ion status for pa rticular methods and anal yses . Matrix: Non-Potable Water Category/Method: Organics by GCIEPA 610 (cont.) Analytes: Code: CAS No.: Chrysene Fluoranthene ldeno (1 ,2 ,3-cd )pyrene Phenanthrene Category/Method: Organics by GC!EPA 615 Analytes: Code: CAS No.: 2,4 ,5-T 2 ,4-D Dalapon Dichlorop rop MCPA Category/Method: Organics by GCIEPA 8011 Analytes: Code: CAS No.: 1,2-Dibromo-3-chloropropane (DBCP ) Category/Method: Organics by GC!EPA 8015 Analytes: Code: CAS No.: Diesel Range Organics (ORO ) Category/Method: Organics by GC!EPA 8021 Analytes: Code: CAS No.: Methyl tert-buty l ether (MTBE ) Xylenes , meta , para Category/Method: Organics by GCIEPA 80818 Analytes: Code : CAS No.: 4,4 '-DDE a-BHC Aldr in Chlordane , alpha Chlordane , Techn ical Dieldrin Endosulfan II Endrin Analytes: Dibenzo( a , h )anthracene Fluorene Naphthalene Pyrene Analytes: 2,4 ,5-TP 2,4 -08 Dicamba Dinoseb MCPP Analytes: 1,2-Dibromoethane (EDB ) Code: Code: Code: Analytes: Code: Gasoline Range Organics (GRO ) Analytes: Xylene , ortho Xylenes , Tota l Analytes: 4 ,4'-DDD 4,4'-DDT b-BHC Chlordane , gamma d-BHC Endosulfan I Endosu lfan sulfate Endrin ketone Code: Code: Page 20 of 22 CAS No.: CAS No .: CAS No .: CAS No .: CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston, Texas 77082 Issue Date : July-01-2007 Expiration Date: June-30-2008 These fields of accreditation supercede all previous fields . The Texas Commission on Environmental Quality urges customers to verify the laboratory 's current accreditation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: Organics by GC/EPA 80818 (cont.) Analytes: Code: CAS No.: Analytes: Code: Endrin aldehyde g-BHC (Lindane) Heptachlor Heptachlor epoxide Hexachlorobenzene Hexachlorocyclopentadiene Methoxychlor Toxaphene Category/Method: Organics by GCIEPA 80828 Analytes: Code: CAS No.: Analytes: Code: PCB-1016 PCB-1232 PCB-1248 PCB-1260 2-Chlorobiphenyll 2 ,2', 5-Trichlorobiphenyl 2 ,2',3,5'-Tetrachlorobiphenyl 2,2',5 ,5'-Tetrach lorobiphenyl 2 ,2',4 ,5 ,5'-Pentachlorobiphenyl 2 ,2' ,3,4,4' ,5'-Hexachlorobiphenyl 2 ,2',3 ,5 ,5',6-Hexachlorobiphenyl Category/Method: Organics by GC!EPA 8151 Analytes: Code: CAS No.: 2,4 ,5-T 2,4-D Da lapon Dinoseb MCPP Picloram PCB-1221 PCB -1242 PCB-1254 PCBs, Total 2 , 3-Dichlorobiphenyl 2,4',5-Trichlorobiphenyl 2,3',4,4'-Tetrachlorobiphenyl 2 ,2', 3', 4 . 5-Pentachlorobiphenyl 2,3,3',4',6-Pentachlorobiphenyl 2 ,2',3 ,4 ,5,5'-Hexachlorobiphenyl 2 ,3 ,3',4 ,5 ,5'-Hexachlorobiphenyl Analytes: Code: 2,4 ,5-TP (Silvex) 2,4-DB Dicamba MCPA Pentachlorophenol Page 21 of 22 CAS No.: CAS No.: CAS No.: TEXAS COMMISSION ON ENVIRONMENTAL QUALITY NELAP-Recognized Laboratory Fields of Accreditation Xenco Laboratories 11381 Meadowglen Lane Houston , Texas 77082 Certificate Number: T104704215-07-TX Issue Date : July-01-2007 Expiration Date: June-30-2008 These fields of accreditation supercede all previous fie lds . The Texas Commission on Environmental Quality urges customers to ver ify the laboratory 's current accred itation status for particular methods and analyses . Matrix: Non-Potable Water Category/Method: Organics by HPLCIEPA 610 Analytes: Code: CAS No.: Acenaphthene Anthracene Benzo(a)pyrene Benzo(g ,h,i)perylene Chrysene Fluoranthene ldeno( 1, 2 , 3-cd) pyrene Phenanthrene Category/Method: Organics by HPLCIEPA 8310 Analytes: Code: CAS No.: Acenaphthene Anthracene Benzo(a)pyrene Benzo(g ,h ,i)perylene Chrysene Fluoranthene lndeno(1 ,2 ,3-c ,d)pyrene Phenanthrene Analytes: Acenaphthalene Benzo(a)anthracene Benzo(b )fluoranthene Benzo(k)fluoranthene Dibenzo(a , h )anthracene Fluorene Naphthalene Pyrene Analytes: Acenaphthylene Benzo( a )anthracene Benzo(b )fluoranthene Benzo(k)fluoranthene Dibenzo(a ,h)anthracene Fluorene Napthalene Pyrene Page 22 of 22 Code: CAS No.: Code: CAS No.: Table 02 Subcontractor's Subcontractor's Subcontractor's 1· Proposed Task Name Address Telephone No. ·························--·····--·--···--·-----· ......... -....... _...... ·······--·-·---·-··-···-.......... ·········---·-·-···· ········-···········-·······-·····---··-··-····-··--··-··---·-----····--·! IF NECESSARY, PROVIDE MORE SHEETS TO DESCRIBE ADDITIONAL SUBCONTRACTORS. INCLUDE A COPY OF THE SUBCONTRACTOR QUALIFICATIONS FOLLOWING THIS PAGE BOUND WITHIN THE PROPOSAL PACKAGE 2-15 2 .11 STATEMENT OF RESIDENCY The following information is required by the City of Fort Worth in order to comply with provisions of state law, TEXAS GOVERNMENT CODE § 2252 .001 , State or Political Subdivision Contracts for Construction , Supplies , Services ; Bids by Nonresident. Every Provider shall affirmatively state its principal place of business in its response to a Request for Proposal. Failure to provide the required information shall result in your proposal being declared non -responsive . Providers ' cooperation in this regard will avoid costly time delays in the award of the proposal by the City of Fort Worth . For this reason , each provider should complete and return , with its bid , the Statement of Residency Form. TEXAS GOVERNMENT CODE § 2252.001 defines a Texas "resident bidder" as a bidder whose principal place of business * is in the state of Texas , including a contractor whose ultimate parent company or majority owner has its principal place of business in the state of Texas. TEXAS GOVERNMENT CODE § 2252 .001 defines a "Nonresident bidder" as a bidder whose parent company or majority owner does not have its principal place of business * in the state of Texas . . LJccvTL1-':5 T L/l/.Jo~llTo/UEJ'" 0 ul..F Co/l>-r Bidder's complete company name : _/_7 ________________ _ State your business address in the space provided below if you are a Texas Resident bidder: /o/6'5 #/f~ W/N' ,tJAJ. f't/l i'e /SD /,loV570/\/, 7"X ? J<:J.J6' State your business address in the space provided below if you are a Nonresident bidder : *The State Purchasing and General Services Commission defines Principal Place of Business as follows : Principal Place of Business in Texas means , for any type of business entity recognized in the State of Texas , that the business entity • has at least one permanent office located within the State of Texas , from which business activities other than submitting bids to governmental agencies are conducted and from which the bid is submitted , and o has at least one employee who works in the Texas office Form prepared by : C/?EC cJI\Y ;r: 6/?/l/'J// 1T/'" Name ,16'1/f//V~~f' ,??Et/ /fJ;'?N /vo.e:!'e Title c; I 5/cJ;? Date 2-16 2.12 NONDISCRIMINATION All City contractors are required to comply with Chapter 17 , "Human Relations ," Article Ill , "Discrimination ," Division 3, "Employment Practices ," of the Code of the City of Fort Worth, prohibiting discrimination in employment practices . Proposer agrees that Proposer, its employees , officers, agents , contractors or subcontractors , have fully complied with all provisions of such Ordinance , and that no employee , participant , applicant , contractor or subcontractor has been discriminated against according to the terms of such Ordinance by Proposer, its employees , officers , agents , contractor or subcontractors herein. PROVIDER: /-}eel/TE-fl j_A/1<1/(flTO~ /ES" Company Name /o/C5 fJlflfW)~ tJ~. f///UI.Fv Address //tJt.JSTON, 7;x 770:JG City , State , Zip (Signature ) 4'tlf1Jl).E.r.! ,£?EV. /l)/Jlll46~~ Title (print or type) 2-17 2.14 INSURANCE CERTIFICATES The successful Provider will be required by the Pricing Agreement to have insurance coverage as detailed below. Prior to commencing work , the Provider shall deliver to Fort Worth certificates documenting this coverage . The City may elect to have the Provider submit its entire policy for inspection . "A Commercial General Liability Insurance -$5,000,000 each occurrence . "B. Professional Liability Insurance -$5 ,000 ,000 each claim . "C. Automobile Liability Insurance - a) Coverage on vehicles involved in the work performed under this Pricing Agreement: • $1 ,000 ,000 per accident on a combined single limit basis or: • $500 ,000 Bodily injury/person • $1 ,000,000 Bodily injury/accident • $250 ,000 Property damage b) The named insured and employees of Pricing Agreement shall be covered under this policy . The City of Fort Worth shall be named an Additional insured , as its interests may appear. Liability for damage occurring while loading , unloading and transporting materials collected under the Pricing Agreement shall be included under this policy . "D. Worker's Compensation - a) Statutory limits for Worker's Compensation plus b) Employer's liability at a minimum : • $1 ,000 ,000 each accident ; • $1 ,000 ,000 disease -policy limit; and • $500 ,000 disease -each employee. "E. Environmental Impairment Liability CEIL) and/or Pollution Liability -$2 ,000 ,000 per occurrence. Ell coverage(s) must be included in policies listed in items A and B above; or, such insurance shall be provided under separate policy(s). Liability for damage occurring while loading , unloading and transporting materials collected under the Pricing Agreement shall be included under the Automobile Liability insurance or other policy(s). The following shall pertain to all applicable policies of insurance (1. through 4.) listed above: a. Additional Insured Clause : "The City of Fort Worth , its officers , agents , employees , and representatives are added as additional insureds as respects operations and activities of, or on behalf of the named insured, performed under Pricing Agreement with the City of Fort Worth." Exception ... the additional insured requirement does not apply to 2-20 Workers ' Compensation policies . b. Subcontractors shall be covered under the Primary Laboratory's insurance policies or they shall provide their own insurance coverage ; and , in the latter case , documentation of coverage shall be submitted to the Primary Laboratory prior to the commencement of work and the Primary Laboratory shall deliver such to the City . c. Prior to commencing work under this Pricing Agreement , the Laboratory shall deliver to the City of Fort Worth insurance certificate(s) documenting the insurance required and terms and clauses required . d . Each insurance policy required by this Pricing Agreement shall contain the following clauses : "This insurance shall not be canceled , limited in scope or coverage , or non- renewed until after thirty (30) Days prior written notice has been given to the Director of Environmental Management, City of Fort Worth, 1000 Throckmorton , Fort Worth , Texas 76102 ." e. The insurers for all policies must be licensed/approved to do business in the State of Texas. Except for workers ' compensation , all insurers must have a minimum rating of A: VII in the current A. M. Best Key Rating Guide or have reasonably equivalent financial strength and solvency to the satisfaction of Risk Management. If the rating is below that required, written approval of Risk Management is required. f . The deductible or self-insured retention (SIR) affecting the coverage required shall be acceptable to and approved in writing by the Risk Manager of the City of Fort Worth in regards to asset value and stockholders equity. In lieu of traditional insurance , alternat ive coverage ma intained through insurance pools or risk retention groups must be also approved by the City 's Risk Manager. g. Waiver of rights of recovery (subrogation) in favor of the City of Fort Worth. h. Such insurance policies shall be primary , without right of contribution and not subject to any offset by any other insurance carried by the City7 i. If insurance policies are not written for specified coverage limits , Umbrella or Excess Liability insurance for any differences is required . Excess Liability shall follow form of the primary coverage . j. "Unless otherwise stated , all required insurance shall be written on the "occurrence basis"". If coverage is underwritten on a claims-made bas is, the retroactive date shall be coincident with or prior to the date of the Pricing Agreement and the certificate of insurance shall state that the coverage is claims-made and the retroactive date. The insurance coverage shall be ma intained for the duration of the Pricing Agreement and for five (5) years following completion of the service provided under the Pricing Agreement or for the warranty period , whichever is longer. An annual certificate of insurance subm itted to the City shall evidence such insurance coverage . k. The City , at its sole discretion , reserves the right to review the insurance requirements and to make reasonable adjustments to insurance coverage 's and their limits when deemed necessary and prudent by the City based upon changes in statutory law , court 2-21 decision or the claims history of the industry as well as of the Laboratory to the City of Fort Worth . In the event the City requires the insurance limits to be increased or changes in policy categories or types of coverage , the City shall provide written notice to the Laboratory party. The Laboratory party will have ninety days from the date of notice to comply with the additional requirements . The City shall be entitled , upon request and without expense , to receive copies of policies and endorsements thereto and may make any reasonable requests for deletion or revis ion or modifications of particular policy terms , conditions , limitations , or exclus ions except where policy provisions are established by law or regulations binding upon either of party or the underwriter on any such policies . FOR PURPOSES OF EVALUATING THIS REQUEST FOR PROPOSAL, PLEASE ATTACH A COPY OF YOUR CURRENT INSURANCE CERTIFICATE(S) FOLLOWING THIS PAGE AND BOUND WITHIN THE PROPOSAL PACKAGE. 2-22 Certification of Contractor's Legal and Compliance History Complete ONE of the Following Certifications: Certification of Legal Action Report I certify under penalty of law that the attached Legal Action Report detailing Contractor's, Contractor 's officers , Contractor's employees , and Contractor's proposed subcontractors legal and compliance history relating to the protection of the environment was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system , or those persons directly responsible for gathering the information , the information submitted is , to the best of my knowledge and belief, true , accurate , and complete. I am aware that there are significant penalties for submitting false information , including the possibility of fine and imprisonment for knowing violations . CONTRACTOR : (Company Name) BY : ___________ _ (signature) (title) Certification of NO Legal Action (print or type name of signatory) (date) I certify unde r penalty of law that the legal and compliance history of Contractor, Contractor's officers, Contractor's employees , and Contractor's proposed subcontractors was researched under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted . Based on my inquiry of the person or persons who manage the system , or those persons directly responsible for gathering the information , I hereby certify that no legal action relating to the protection of the environment was brought against Contractor , Contractor's officers , Contractor's employees , or Contractor 's proposed subcontractors within the preceding five years. To the best of my knowledge and belief, this statement is true, accurate , and complete . I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations . CONTRACTOR: /J CCU T £S' r L./l 6' tJ I? 1170/2 IE r C !/l. ,c Co /I 5; ) (Company Na BY :-+--~,q.....;...:.~/.,:,__· ~~~--___J.__ 15'//f//V.EJ.J £?£//. /'7/?M/lbcl( (title) (print or type name of signatory) r/5/~7 (date) 2-25 I m11!!1 ['dACCUTEST. , Quality Systems Manual Volume VII, Revision I: March 2007 Effective Date: March 27, 2007 Document Control Number: ACCUTEST LABORATORIES GULF COAST, INC. HOUSTON LABORATORY OPERATIONS 10165 HARWIN DRIVE, SUITE 150 HOUSTON, TEXAS 77036 713.271.4700 This document is the exclusive property of Accutest Laboratories . Reproduction without the ex pressed written permission of Accutest Laboratories is prohibited r.l~ gjACCUTEST. Page 3 of 96 Revis ion Date : March 2007 Revision I Summary :of Changes Accutest Laboratories Gulf Coast , uality System Manual -March 2007 2.2 7 6 .0 24 6 .3 24 6 .3 25 6 .8 26 7 .1 28 7.4 29 8.4 32 8 .5 32 9 .1 36 9 .3 38 9.4 38 9.12 42 12.2 50 12 .2 50 12.7 55 18 .1 72 19 .2 73 App. II 83 App . Ill 80 Revised organization chart. Modified document control procedure to reflect document tracking . Clarify procedure for issuing uncontrolled copy distribution. Specified correct procedure for issuing electronic version of QSM . Revised to reflect the actual practice of the laboratory. Changed from calibration log to calibration database. Added commercial standards acceptability criteria . Added reporting limit definition for inorganics . Clarified inorganic method reporting requirement Revised statement to include all bottle preservation . Added sampling procedure for field sample collection. New section for laboratory preservation of improperly preserved field samples . Added PCB hazardous waste handling procedure . Mod ified method blank criteria to match corporate criteria Changed NIST/NVLAP appr,oved PT Provider to A2LA approved provider. Revised to reflect actual practice of the laboratory. Adding a corrective action procedure to non-conforming product. Added verbiage on security action from Homeland Security . Removed Data Entry for Sa nn ple login from Sample Management Grouping and added it Project Management Grouping . Updated method list by deleting methods not performed by the laboratory mlt!J (dACCUTEST. Table of Contents Page 4 of 96 Revision Date : March 2007 Rev ision I 1.0 QUALITY POLICY ______ __.. ______________ 9 1.1 Accutest Mission: 9 1.2 Policy Statement: 9 2.0 ORGANIZATION JO 2. 1 Organizational Entity. 10 2.2 Management Responsibilities JO 3.0 QUALITY RESPONSIBILITIES OF THE MANAGEMENT TEAM 12 3. 1 Requirement: 12 3.2 Program Authority: 12 4.0 JOB DESCRIPTIONS OF KEY STAFF 19 4.1 Requirement: 19 4.2 Employee Screening, Orientation, and Training. 20 4.3 Training Documentation. 21 5.0 SIGNATORYAPPROVALS 22 5. 1 Signature Hierarchy. 22 5.2 Signature Requirements. 23 6.0 DOCUMENTATION & DOCUMENT CONTROL 24 6. 1 Form Generation & Control. 24 6.2 Logbook Control. 24 6.3 Controlled Documents. 24 6.4 Standard Operating Procedures (SOPs). 25 6.5 Confidential Business Information (CBI). 26 6.6 Quality Assurance Directory. 26 6. 7 Software Change Documentation & Control. 26 6.8 Report and Data Archiving. 26 6.9 Training. 27 7.0 REFERENCE STANDARD TRACEABILITY 28 7. 1 Traceability of Metric Measurements -Thermometers. 28 7.2 Traceability of Metric Measurements -Calibration Weights. 28 7.3 Traceability of Chemical Standards. 28 7.4 Documentation of Traceability. 29 mll!t ;iACCUTEST. Page 5 of 96 Revision Date : March 2007 Revision I 7.5 Assignment of Reagent and Standard Expiration Dates. 29 8.0 TEST PROCEDURES, METHOD REFE1ENCES, AND REGULATORY PROGRAMS 31 8. 1 Standard Operating Procedures. i 31 8.2 Method Detection Limit Determination. 31 --------------- 8. 3 Instrument Detection Limit Determination. 32 8.4 Method Reporting Limit. 32 8.5 Reporting of Quantitative Data. 32 8.6 Precision and Accuracy Studies. 33 8. 7 Method Selection. 33 8.8 Method Validation. 34 8.9 Estimated Uncertainty. 34 8.10 Demonstration of Capability. 34 8.11 Method Sources & References. 35 8.12 Analytical Capabilities. 35 9.0 SAMPLE MANAGEMENT, LOGIN, CUSTODY, STORAGE AND DISPOSAL 36 9. 1 Order Receipt and Entry. 36 9.2 Sample Receipt and Custody. 37 9.3 Sampling. 38 9.4 Laboratory Preservation of Improperly Preserved Field Samples. 38 9.5 Sample Tracking Via Status Change. 39 9.6 Sample Acceptance Policy. 39 9. 7 Assignment of Unique Sample Identification Codes. 40 9.8 Subcontracted Analysis. 40 9.9 Sample Storage. 42 9.10 Sample Login. 42 9. 11 Sample Retrieval for Analysis. 42 9.12 Sample Disposal. 42 10.0 LABORATORY INSTRUMENTATION AND MEASUREMENT STANDARDS 44 10.1 Mass Tuning-Mass Spectrometers. 44 10.2 Wavelength Verification-Spectrophotometers. 44 10.3 Inter-element Interference Checks (Metals). 44 10.4 Calibration and Calibration Verification. 45 mll!!t E'4ACCUTEST. Pa ge 6 of 96 Revision Date : March 2007 Revis ion I 10.5 Linear Range Verification and Calibration (ICP Metals). 45 I -------- 10. 6 Retention Time Verification (GCJ.1: 46 10. 7 Equipment List. . 46 11.0 INSTRUMENT MAINTENANCE 4 7 11.1 Routine, Daily Maintenance. 4 7 11.2 Non-routine Maintenance. 47 11.3 Scheduled Maintenance. 4 7 11.4 Maintenance Documentation. 48 12.0 QUALITY CONTROL PARAMETERS, PR'OCEDURES, AND CORRECTIVE ACTION 49 12. 1 Procedure. 49 12.2 Methodological Control Parameters and Corrective Action. 50 12.3 Sample Control Parameters and Corrective Action. 52 12.4 Bench Review & Corrective Action. 53 12.5 QA Monitoring. 53 12.6 Data Qualifiers. 54 12. 7 Data Package Review. 55 12.8 Laboratory Derived Quality Control Criteria. 57 12.9 Electronic Data Reduction. 57 12.10 Representativeness. 57 12.11 Comparability. 58 13.0 CORRECTIVE ACTION SYSTEM 59 13.1 Procedure. 59 13 .2 Documentation & Communication. 59 14.0 PROCEDURES FOR EXECUTING CLIENT SPECIFICATIONS 61 14.1 Client Specific Requirements. 61 14.2 Requirements for Non-Standard Analytical Specifications. 61 14.3 Evaluation of Resources. 62 14.4 Documentation. 62 14.5 Communication. 62 14.6 Operational Execution. 63 14. 7 Verification . 63 15.0 CLIENT COMPLAINT RESOLUTION PROCEDURE 64 mll!!t CiACCUTEST. Page 7 of 96 Rev is ion Da te : March 200 7 Revision I 15. 1 Procedure. 64 ---------+----------------- 15. 2 Documentation. 64 15.3 Corrective Action. 64 15.4 QA Monitoring. 64 16.0 CONFIDENTIALITY PROTECTION PROCEDURES 66 16. 1 Client Anonymity. 66 16.2 Documents. 66 16.3 Electronic Data. 66 16.4 Information Requests. 67 16.5 Transfer of Records. 67 17.0 QUALITY AUDITS AND SYSTEM REVIEWS 69 17. 1 Quality System Reviews. 69 17.2 Quality System Audits. 69 17.3 Method Assessments. 69 17.4 Documentation Audits. 69 17.5 Corrective Action Monitoring. 70 17.6 Preventive Action. 70 17. 7 Client Notification. 70 17.8 Management Reports. 70 18.0 CONTROL OF NONCONFORMING PRODUCT 72 18. 1 Corrective Action. 72 19.0 HEALTH AND SAFETY 73 19.1 Policy. 73 19.2 Responsibilities. 73 19.3 Program Elements. 74 CHAIN CUSTODY -·--··-·"'-·-· . ----··-·--···-····-----······---··· Page of ~1 !) ) ,, '; !" ·~ ; FED-EX Tracking # B ottle Order Control # 10165 Harwin, Suite 150 -Houston, TX 77036 -713-271-4700 fax: 713-271-4770 Accutest Q uo te # A ccutest J ob # Client/ Reoortim:i Information I I Project Information Reauested Analyses Matrix Codes Company Nam e Project Name / No. OW -Drinking Water G W -Ground Water Project Co ntact E-M ail Bill to Invoice Attn. WW -Wastewater SO-Soil Addres s Addre ss SL -Sludge 01 -0il LIQ -Other Liquid City State Z ip City State Z ip SOL · Other Solid Phone No . Fa x No , Pho ne No, Fax No. Samplers's Name Client Purchase Order# A ccu test Coll ectio n Number of preserve d bottl es Fie ld ID / Po inl of Co ll ectio n #of I 8 0 0: g :,: w Sample # u 0 £ z LAB USE ONLY :,: z "' () 'li 0 Date Time Matrix bottles :,: 'i' ffi z " z Turnaround Time I Business davsl I Data Deliverable Information Comments I Remarks c=:J 10 Day STANDARD Approved B y :/ Da te: D Commercial "A " D State Forms c=:J 5 Day RUSH D Commercial "B " D EDD Format C=3 4 Day RUSH D Reduced Tier 1 D TRRP C=1 3 Day EMERGENC Y D Full Data Pa cka g e C:=::J 2 Day EMERGENCY C=1 1 Day EMERGENCY Commercial "A " = Res ults Only [:==J Other Commercial "B " = Re s ults & Standard QC Real time analytical data available via Lab/ink I SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESSION , INCLUDING COURIER DELIVERY Re linquished by Sampler : 1Date lime: Hece1ved By: Ke11nqu1s n e a t:1y : I Date Time: Received B y : 1 1 2 2 Re linquis hed b y : IOat e Tim e: Rece ived By : Ke11nqu1 s nea t::;;y: I Date T im e: Received By: 3 3 4 4 Relinquis hed by: I Dat e T ime: Received By: Custody Se al # ---P-reserved where a ppl1caliTe On Ice Cooler Temp. 5 5 D D mt~ !3ACCUTEST. 9.2 Sample Receipt and Custody. Page 37 of 96 Revis ion Date : March 2007 Revision I Samples are delivered to the laboratory using a variety of mechanisms including Accutest couriers , commerc ial shippers, and client self-delivery . Documented procedures are followed for arriving samples to assure that custody and integrity are maintained and that handling/preservation requirements are documented and maintained . Sample custody documentation is initiated when the individual collecting the sample collects field samples. Custody documentation includes all information necessary to provide an unambiguous record of sample collection , sample ident ification , and sample collection chronology . Initial custody documentation employs either Accutest or client generated custody forms. Accutest generates a chain of custody in situations where the individuals who collected the sample did not generate custody documentation in the field . Accutest defines sample custody as fo lj ows : •!• The sample is in the actual custody'or possession of the assigned responsible person , •!• The samp le is in a secure area. The Accutest facility is defined as a secure facil ity. Perimeter security has been established , which limits access to authorized individuals only . Visitors enter the facility through the building lobby and rmust register with the recept ionist pr ior to entering controlled areas . While in the facility, vis itors are required to wear a visitor 's badge and must be accompanied by their hosts at all times . After hours , building access is controlled using a lock and key and coded alarm system . This system limits building access to ind ividuals with a pre-assigned authorization status . After hours visitors are not authorized to be in the building . Clients delivering samples after hours must make advanced arrangements through client services and/or sample management to assure that staff is available to take delivery and maintain custody . Upon arrival at Accutest, the sample custodian reviews the chain of custody for the samples received to verify that the information on the form corresponds with the samples delivered. This includes verification that all listed samples are present and properly labeled , checks to verify that samples were transported and received at the requ ired temperature , verification that the sample was rece ived in prope r containers , verification that sufficient volume is available to conduct the requested analysis , and a check of ind ividual sample containers to verify test specific preservation requ irements includ ing the absence of headspace for volatile compound analysis . C!l!I (jACCUTEST. Page 38 of 96 Rev ision Date: March 2007 Rev ision I The sample custodian prior to completing acceptance of custody documents sample conditions and other observations on variance memo. The sample custodian accepts sample custody upon verification that the custody document is correct. Discrepancies or non-compliant situations are documented and communicated to the Accutest project manager, who contacts the client for resolution . The resolution is documented and communicated to sample management for execution . The sample manager maintains a sample receipt log. This log details all sample- related information . The log records include critical date information , numbers of samples , numbers of bottles for each parameter, descriptions of bottles for each parameter , preservation conditions, bottle refrigerator location , and bottle conditions . During initial login , each bottle is assigned a unique number. Internal custody documentation may be requ ired for compliance w ith regulatory agency or contractual specifications it is used as an additional means of tracking samples in-house . A documented , chronological record of each sample transfer identifying each ind ividual having possession of the sample is created in the laboratory information management system , which can be pr inted and included in data reports to demonstrate continuous custody . 9.3 Sampling. Documented procedures are employed by the field staff for field sample collection and are accessible during sample collection activities . Field measurements are recorded in a controlled notebook . The field staff initiates custody for collected samples at the time of sample collection . Samples are documented , labeled and prese rved accord ing to the specifications of the method and/or regulatory program prior to being shipped to the laboratory . 9.4 Laboratory Preservation of Improperly Preserved Field Samples. Accutest will attempt to preserve field samples that were received without proper preservation to the extent that it is feasible and supported by the methods in use . Laboratory preservation of improperly preserved or handled field samples is routinely performed for metals samples. Special handling procedures may also be applied to improperly preserved volatile organics . Aqueous metals samples that were not nitric acid preserved to pH 2 in the fie ld are laboratory preserved and held for sixteen (16) hours to equilibrate prior to analysis . Aqueous metals samples requiring field filtration may be filtered in the laboratory with in seventy-two (72) hours of rece ipt provided that the sample has not been acid preserved . Unpreserved volatile organics samples may be analyzed within seven (7) days to minimize degradation of volatile organics if the laboratory is notified in advance of the failure to preserve upon collection . Laboratory preservation of unpreserved aqueous ----------··--··----·····-···-· · ,-·· -····· ~r!t gjACCUTEST. ·-·----···------------- Page 39 of 96 Revision Date : March 2007 Revis ion I samples is not possible . A pH check of volatile organic samples prior to analysis will compromise the sample by allowing volatile organics to escape during the check . If the laboratory is not notified of the failure to field preserve an aqueous volatile organic sample , the defect will not be identified · until sample analysis has been completed and the data is qualified accordingly . 9.5 Sample Tracking Via Status Change. Internal Chain of Custody (ICOC) systems records sample exchange transactions between sample administration to various analytical departments . This system tracks all preparation , analytical, and data reporting procedures to which a sample is subjected while in the possession of the laboratory. Each individual receiving samples must acknowledge the change in custody and operational status in the Internal Chain of Custody Logbook . This step is required to maintain an accurate record of sample status , dates of analytical activity, and custody throughout the laboratory . Sample tracking is initiated at login where all chronological information related to sample collection dates and holding times are entered into the LIMS . This information is entered on an individual sample basis . 9.6 Sample Acceptance Policy. Incoming samples must satisfy Accutest's sample acceptance criteria before being logged into the system . Sample acceptance is based on the premise that clients have exercised proper protocols for sample collection . This includes complete documentation, sufficient volume , proper chemical preservation , temperature preservation, sample container sealing and labeling , and appropriate shipping container packing. The sample manager will make every attempt to preserve improperly preserved samples upon arrival. However, if preservation is not possible , the samples may be refused unless the client authorizes analysis . No samples will be accepted if holding times have been exceeded or will be exceeded before analysis can take place unless the client authorizes analysis. Sample acceptance criteria include proper custody and sample labeling documentation . Proper custody documentation includes an entry for all physical samples delivered to the laboratory with an identification code that matches the sample bottle and a date and s ignature of the individual who collected the sample and delivered them to the laboratory. Accutest reserves the right to refuse any sample which in its sole and absolute discretion and judgement is hazardous , toxic and poses or may pose a health , safety or environmental risk during handling or processing . The company will not accept samples for analysis using methodology that is not performed by the laboratory or for ell!! (jACCUTEST. Page 40 of 96 Revis ion Date : March 2007 Rev ision I methods that lab does not hold valid accreditations unless arrangements have been made to have the analysis conducted by a qualified subcontractor. 9.7 Assignment of Unique Sample Identification Codes. Unique identification codes are assigned to each sample bottle to assure traceability and unambiguously identify the tests to be performed in the laboratory . The sample identification coding process begins with the assignment of a unique alphanumeric job number. A job is defined as a group of samples received on the same day, from a specific client pertaining to a specific project. A job may consist of groups of samples received over multi-day period . The first character of the job number is an alpha-character that identifies the laboratory facility . The next characters are numeric and sequence by one number with each new job . Unique sample numbers are assigned to each bottle collected as a discrete entity from a designated sample point. This number begins with the job number and incorporates a second series of numbers beginning at one and continuing chronologically for each point of collect ion . The test to be performed is clearly identified on the bottle label. Multiple sample bottles collected for analysis of the same parameter are numbered bottle 1, 2 , ... etc . Alpha suffixes may be added to the sample number to identify special designat ions such as subcontracted tests , in-house QC checks, or re-logs . Multiple sample bottles for a specific analys is are labeled Bottle 1, Bottle 2 , etc . 9.8 Subcontracted Analysis. Subcontract laboratories are employed to perform analysis not performed by Accutest. The project manager or quality assurance personnel evaluates subcontract laboratories to assure their quality processes meet the standards of the env ironmental laboratory industry prior to engagement. Throughout the subcontract process , Accutest fo ll ows establ ished procedures to assure that sample custody is maintained and the data produced by the subcontractor meets established quality criteria . Subcontracting Procedure. Subcontracting procedures a re initiated through several mechanisms , which originate with sample management. Samples for analysis by a subcontractor are logged into the Accutest system using regular login procedures . If subcontract parameters are part of the project or sample management has received subcontracting instructions for a specific project the project manager creates a subcontract cha in of custody which identifies only the subcontracted samples and the un ique identifier g iven to each sample from the LIMS . The project manager keeps a copy of this subcontract chain and forwards a copy to the sample manager to send out with the subcontracted samples. The approved subcontractor is contacted to place t he subcontract order. ral!I !'iACCUTEST. Pa ge 41 of 96 Revision Date : March 200 7 Revision I Subcontracting within the Accutest Laboratory System allows all information pertaining to each sample to be electronically tra~smitted through the LIMS System . The Sample Manager updates the subcontract log when the samples are shipped to a different location . The Sample manager or Project manager signs the subcontract chain of custody and ships the sample(s) to the subcontractor. The subcontract CoC is filed with the original Coe. Sample management signs the subcontract chain of custody and ships the sample(s ) to the subcontractor . The subcontract CoC is filed with the original CoC and the request for subcontract. Clients are verbally notified of the need to subcontract analysis as soon as the need is identified by the client services staff. This may occur during the initial project setup or at the time of login if the project setup had not been initiated through the cl ient services staff. Copies of the subcontract CoC and the original CoC, which are electronically distributed to clients , constitutes documented client notification of the laboratories intent to subcontract analysis . The technical d irecto r or project manager to assess completeness and quality compliance reviews subcontractor data packages . If completeness defects are detected , the subcontractor is asked to immediately upgrade the data package. If data quality defects are detected , the technical director reviews the package . The project manager or report generation personnel will pursue a corrective action solution before releasing data to the client. The technical d irector or the report generation personnel enters approved subcontract data into the laboratory information management system (LIMS) if possible and incorporates the data into the final report. Copies of original subcontract data are included in the data report depending on the reporting level specified by the client Subcontract Laboratory Evaluation. The QAO or Project manager evaluates subcontract laboratories prior to engagement. The subcontract laboratory must provide Accutest with proof of a valid certification to perform the requested analysis , a copy of the laboratory 's Quality Systems Manual , copies of SOPs used for the subcontracted analys is, a copy of the most recent performance evaluation study for the subcontracted parameter, and copies of the most recent regulatory agency or third party accreditor audit report. Certification verification , audit reports and performance evaluat ion data must be submitted to Accutest annually . If possible , the QAO may conduct a s ite visit to the labo ratory to inspect the quality system. Qualification of a subcontract laboratory may be bypassed if the primary client directs Accutest to employ a specific subcontractor. mll!!t rJACCUTEST. 9.9 Sample Storage. Pag e 42 of 96 Revision Date : March 2007 Rev ision I Following sample custody transfer to the sample custodian , the sample custodian depending upon the test to be performed and the matrix of the samples assign samples to various secured refrigerated storage areas. The location (refrigerator and shelf) of each sample is recorded on the internal chain of custody adjacent to the line corresponding to each samp le number and also entered into LIMS. Samples remain in storage until the laboratory technician retrieves the sample for analysis. Samples for volatile organics analysis are placed in storage in des ignated refrigerators by the sample custodian and immediately transferred to the organics group control. These samples are segregated according to matrix to limit opportunities for cross contaminat ion to occur. Organics staff is authorized to retrieve samples from these storage areas for analys is . When analysis is complete , the samples are placed back into storage . 9.10 Sample Login. Following sample custody transfer to the laboratory, the documentation that describes the clients analytical requirements are delivered to the sample login group for coding and entry to the Laboratory Information management System (LIMS). This process translates all information related to collection time , turnaround time , sample analysis , and deliverables into a code which enables client requirements to be electronically distributed to the various departments within the laboratory for scheduling and execution . 9.11 Sample Retrieval for Analysis. Analysts use the ir da ily work lists to locate where to retrieve samples for analysis . The samples are logged out in the internal chain of custody and the analysts retain custody of the sample at this point. After sample analysis has been completed , the analysts return the sample to the storage area . The analysts relinquish custody of the sample after they have logged the sample back into the internal chain of custody . 9.12 Sample Disposal. Accutest retains all samples under proper storage for a minimum of 30 days following complet ion of the analysis report . Longer storage periods are accommodated on a client specific basis if required . Samples may also be returned to the cl ient for disposal. 91!!1 (jACCUTEST. Page 43 of 96 Revis ion Date : March 2007 Rev ision I Accutest disposes of all laboratory wastes following the requirements of the Resource Conservation and Recovery Act (RCR,4-.). The Company has obtained and maintains a waste generator identification number, !TXCESQG . Sample management generates a sample disposal dump sheet from the LIMS tracking system each month , which lists all samples whose holding period has expired . Data from each sample is compared to EPA hazardous waste characteristics , Texas Class I waste , or the City of Houston Effluent limits . Samples containing constituents at concentrations above the cr iteria are labeled as hazardous and segregated into six separate waste categories for disposal as follows : * Organic extracts : Chlorinated and non-chlorinated solvents * Mixed flammable solvents (hexane, acetone, toluene) * Waste oil * Soil (solids) * Aqueous * Sludges (semi-solids) * PCB Hazardo u s Waste (USEP A 40 CFR 761 cri teri a). Non-hazardous aqueous samples are diluted , neutralized , and disposed directly into the laboratory sink . All aqueous liquids are neutralized before entering the municipal system . Samples classified as PCB hazardous wastes are labeled and packaged according to the requirements in 40 CFR 761 and returned to client for disposal. Solid samples are emptied into consolidation drums and disposed as hazardous waste or non-hazardous wastes depending upon the results of hazardous characteristic determ ination . Sample bottles are broken prior to disposal to minimize waste volume and destroy sample labels. Laboratory wastes are in designated areas throughout the laboratory . Waste are consolidated by the departments and transferred to specific drums for disposal through a permitted waste management contractor . Filled , consolidated drums are tested for hazardous characteristics and scheduled for removal from the facility for appropriate disposal based on the laboratory data . All solvent extracts and digestates are collected for disposal following the thirty-day holding period and drummed according to their specific waste stream category . Chlorinated solvent extracts are drummed as chlorinated wastes (i.e ., Methylene Chloride). Non-chlorinated solvent extracts are drummed as non-chlor inated wastes (i.e., acetone , hexane , methanol , and mixed solvents). Digestates are collected for disposal following the thirty-day holding period and drummed as corrosive liquid containing metals . Ill!! l!;iACCLrrEST. 13.0 CORRECTIVE ACTION SYSTEM Page 59 of 96 Revision Date : March 2007 Revision I Requirement. The laboratory employs polices and procedures for correcting defective processes , systematic errors , and quality defects enabling the staff to systematically improve product quality . The system includes procedures for communicating items requiring corrective action to responsible individuals , corrective action tracking procedures , corrective action documentation , monitoring of effectiveness , and reports to management. The system is fully documented in a standard operating procedure . Individual corrective actions and responses are documented in a dedicated database . 13.1 Procedure. Corrective action is the step that follows the identification of a process defect. The type of defect determines the level of documentation , communication , and training necessary to prevent re-occurrence of the defect or non-conformance . The formal system is maintained by the quality assurance department. Operations management is responsible for working within the system to resolve identified deficiencies . Routine Corrective Action . Routine corrective action is defined as the procedures used to return out of control analytical systems back to control. This level of corrective action applies to all analytical quality control parameters or analytical system specifications . Bench analysts have full responsib ility and authority for performing routine correct ive action . The resolution of defects at this level does not require a procedural change or staff re-training. The analyst is free to continue work once corrective action is complete and the analytical system has been returned to control. Documentation of routine corrective actions can be documented in the logbook comments , on a variance form , or on the data rev iew log for the analysis being performed . Procedural Modifications. Corrective actions in this category require process change. They may be the result of systematic defects identified during audits , the investigation of client complaints , product defects identified during data review , or method updates . Resolution of defects of this magnitude require formal identification of the defect, development and documentation of a corrective action plan , and staff training to communicate the procedural change . 13.2 Documentation & Communication. Rout ine corrective actions are documented as part of the analytical record . Notations are made in the comments section of the analytical chronicle or data sheet detailing the nonconformance . Continuation of the analysis indicates that return to control was successful. elr!!I gJACCLSTEST. Page 60 of 96 Revis ion Date : March 2007 Revision I Corrective actions for process changes are documented, tracked and monitored for effectiveness. Supervisors or senior staff members may initiate corrective actions by generating a corrective action using the corrective action database application . The corrective action database is an Access application . The initiator generates the corrective action investigation form , which is documented , tracked, distributed to responsible parties and archived through the application . The application assigns a tracking number initiation data and due date to each corrective action initiated and copies the corrective action form to the corrective action database. The application also distributes an E-mail message containing the form to the responsible parties for resolution . The responsible party identifies the root cause of the defect, initiates the immediate fix and develops and implements the procedural change . Exist ing documentation such as SOPs are ed ited to reflect the change . The affected staff is informed of the procedural change through a formal training session . The training is documented and copies are placed into individual training files. The corrective action form is completed by the responsible party and returned to the QA staff via e-mail using the database application. Initial and completed corrective action forms are maintained in the corrective action database . This entire database is archived for backup purposes daily. The corrective action tracking form is maintained as an active report in the database . Monitoring . The QA Staff monitors the implemented corrective action until it is evident that the action has been effective and the defect has been eliminated . The co rr ective action database is updated by QA to reflect closure of the corrective action . The QA staff also assigns an error code to the corrective action for classification of the type of errors being committed . If QA determines that the corrective action procedure has not effect ively remedied the deficiency , the process continues with a re-initiation of the corrective action. Corrective action continues until the defective process is eliminated . If another procedural change is required, it is treated as a new corrective action , which is documented and monitored using established procedures . Client Notification. Defective processes , systematic errors , and quality defects , detected during routine audits may have negative impacts on data quality . In some cases , data that has been released to clients may be affected . If defective data has been released for use , Accutest will notify the affected clients of the defect and provide specific details regarding the magnitude of the impact to their data. mlr!! !JACCUTEST. 14.0 PROCEDURES FOR EXECUTING CLIENT SPECIFICATIONS Page 61 of 96 Revision Date : March 2007 Revi si on I Requirement. Systems have been established for evaluating and processing client specifications for routine and non-routine analytical services . The systems enable the client services staff to identify , evaluate, and document the requested specifications to determine if adequate resources are available to perform the analysis . The system includes procedures for communicating the specifications to the laboratory staff for execut ion and procedures for verifying the specifications have been executed . 14.1 Client Specific Requirements. The project manager is the primary contact for clients requesting laboratory services . Client specifications are communicated using several mechanisms. The primary source of information is the client's quality assurance project plan (QAPjP) which details analytical and quality control specifications for the project. In the absence of a QAPjP , projects specifications can also be communicated using contracts , letters of authorization , or letters of agreement , which may be limited to a brief discuss ion of the analytical requirements and the terms and cond itions for the work . These documents may also include pricing information , liabilities, scope of work , in addition to the analytical requirements . QAPjPs include deta iled analytical requirements and data quality objectives, which supersede those found in the referenced methods . This information is essential to successful project completion . The managerial and project management staff provides additional assistance to clients who are unsure of the specifications they need to execute the sampling and analysis requirements of their project. They provide additional support to clients who requ ire assistance in results interpretation as needed , provided they possess the expertise requi red to render an opinion . The project manager is responsibility for obtaining project documents , which specify the analyt ical requirements . Following project management review , cop ies and /or information are distributed to the QA Officer or the appropriate departmental managers for review and comment. The QAPP is filed in the project manager's office . 14.2 Requirements for Non-Standard Analytical Specifications. Client requirements that specify departures from documented policies , procedures , or standard specifications must be submitted to Accutest in writing . These requirements are rev iewed and approved by the technical staff before the project is accepted . Once accepted , the non -standard requirements become analytical specifications, wh ich fol low the routine procedure for communicating client specifications . Departures from documented policies, procedures , or standard specificat ions that do not follow this procedure are not permitted . mtl!t (JACCUTEST. 14.3 Evaluation of Resources. Page 62 of96 Revision Date : March 2007 Revision I A resource evaluation is completed prior to accepting projects submitted by clients. The client service staff who prepares a brief synopsis that includes the logistical requirements of the project initiates the evaluation. Logistical specifications for new projects are summarized in writing for evaluation by the affected departments . The specifications are evaluated by the department manager from a scheduling and hardware resources perspective. The project is not accepted unless the department managers have the necessary resources to execute the project according to client specifications. 14.4 Documentation. New projects are initiated using a project set up form, which is completed prior to the start of the project. This form details all of the information needed to correctly enter the specifications for each client sample into the laboratory information management system (LIMS). The form includes data reporting requirements, billing information , data turnaround times , QA level , state of origin , and comments for detailing project specific requirements. The project manager is responsible for obtaining this information from the client and completing the form prior to sample arrival and login. Sample receipt triggers project creation and the login process . The information on the set-up form is entered into the LIMS immediately prior to logging in the first sample . The set up form may be accompanied by a quotation, which details the analytical product codes and sample matrices . These details are also entered into the LIMS during login. Special information is distributed to the laboratory supervisors and login department in electronic or hardcopy format upon project setup. All, project specific information is retained by the project manager in a secure file . The project manager maintains a personal telephone log, which details conversations with the client regarding the project. Department supervisors or client services prepare summary sheets that detail client specific analytical requirements for each test. Bench analysts use these sheets to obtain information regarding client specific analytical requirements before analyzing samples . A program code is established for each client that links the client specifications to a client project. This code is attached to a project by the project manager at login and listed on the work list for each work group conducting analysis for clients with standing requirements. 14.5 Communication. A pre-project meeting is held between client services and the operations managers to discuss the specifications described in the QAPP and/or related documents . Project ml~ '3ACCUTEST. Page 63 of 96 Revision Date : March 2007 Revis ion I logistics are discussed and finalized and procedures are developed to assure proper execution of the client's analytical specifications and requirements . Questions , raised in the review meeting , are discussed with the client for resolution . Exceptions to any requirements , if accepted by the client , are documented and incorporated into the QAPjP or project documentation records . Non-standard specifications for individual clients are documented in the LIMS at the client account level or program level. Simple specifications are documented as comments for each project. Once entered into the LIMS , these specifications become memorialized for all projects related to the client account. Complex specifications are assigned program codes that link the specification to detailed analytical specifications. Upon sample arrival , these specifications are accessed through a terminal or printed as a hard copy and stored by the project manager. Specifications that are not entered into the LIMS are prohibited unless documented in an interdepartmental memo , which clearly identifies the project , client and effective duration of the specification . 14.6 Operational Execution. A work schedule is prepared for each analytical department on a daily basis . Analytical specifications from recently arrived samples have now been entered into the LIMS database . The database is sorted by analytical due date and holding time , into product specific groups . Samples are scheduled for analysis by due date and holding time. The completed schedule , which is now defined as a work list, is printed. The list contains the client requested product codes and specifications required for the selected sample(s). Special requirements are communicated to the analyst using the comment section or relayed through verbal instructions provided by the supervisor . The bench analyst assumes full responsibility for performing the analysis according to the specifications printed on the work sheet. 14. 7 Verification. Prior to the release of data to the client, laboratory section managers and the report generation staff review the report and compare the completed product to the client specifications documentation to assure that all requirements have been met. Project managers perform a spot check of projects with unique requirements to assure that the work was executed according to specifications . 2.18 FINANCIAL STATEMENT Providers must provide a current certified or comp ilation financial statement within this section of the proposal. The financial statement shall be no more than six months old . INCLUDE A COPY OF THE STATEMENT FOLLOWING THIS PAGE BOUND WITHIN THE PROPOSAL PACKAGE 2-28 Business Information Report: Accutest Corporation DUNS : 01-154-8195 ACCUTEST CORPORATION ACCUTEST LABORATORIES 2235 US HIGHWAY 130 AND BRANCH(ES) OR DIVISION(S) DAYTON NJ 08810 TEL: 732 329-0200 *IN DATE* DATE PRINTED MAY 25 2006 ENVIRONMENTAL TESTING LABORATORY SIC NO. 87 34 SUMMARY RATING 4A2 STARTED SALES F WORTH F EMPLOYS HISTORY 1956 $45,000,125 $19,136,746 325(200 HERE) CLEAR FINANCIAL CONDITION STRONG CHIEF EXECUTIVE: VINCENT J PUGLIESE, CEO * * * CUSTOMER SERVICE * * * ======~----------====-========----========-----===-====-~=====-===------======~ If you have questions about this report, please call our Customer Resource Center at 1-800-234-3867 from anywhere within the U .S. If you are outside the U.S., contact your local D&B office. *** Additional Decision Support Available*** Additional D&B products, monitoring services and specialized investigations are available to help you evaluate this company or its industry. Call Dun & Bradstreet's Customer Resource Center at 1-800-234-3867 from anywhere within the U.S. or visit our website at www.dnb.com . -----==-----=~=--------=-------------==~===--------------------====-==--==~==== * * * SUMMARY ANALYSIS * * * The Surrunary Analysis section ·refl ects information in D&B's file as of May 24, 2006 . RATING SUMMARY The Rating was c hanged on May 23, 2006 because D&B's file shows increased slowness in the company's payment record. The "4A" portion of the Rating (the Rating Classification) indicates that the company has a worth from $10 million to $50 million. The "2" on the right (Composite Credit Appraisal) indicates an overall •good" credit appraisal . This credit appraisal was assigned because the payment information in D&B 's file indicates that the majority of this company's obligations are retired satisfactorily and because of D&B's "strong• assessment of the company's December 31, 2005, abridged, fiscal financial statement . :usiness Information Report: Accutest Corporation Below is an overview of the company's D&B Rating(sl since 03/28/97: RATING DATE APPLIED ------------------ 4A2 05/23/06 4Al 09/21/04 4A2 04/14/04 4A3 04/13/04 3A3 03/04/04 3A2 03/18/03 3Al 06/21/02 4Al 06/09/01 3Al 06 /04/99 3A2 03/28/97 -----==--======--=---------==----------------==-------------------------------- * * * PAYMENT SUMMARY * * * --====------------------------------------------------------------------------- The Payment Sununary section reflects payment information in D&B's file as of the date of this report. The PAYDEX for this company is 69. This PAYDEX score indicates that payments to suppliers average 16 days beyond terms, weighted by dollar amounts . When dollar amounts are not considered, approximately 76% of the company's payments are within terms. Below is an overview of the company's dollar-weighted payments, segmented by its suppliers' primary industries: TOTAL LARGEST % DAYS SLOW TOTAL DOLLAR HIGH W/IN RCV'D AMOUNTS CREDIT TERMS <31 31-60 61-90 91+ ------------------------ # $ $ % % % % % Total in D&B's file 48 384,650 100,000 Top 10 Industries: 1 Nonclassified 5 167,550 100,000 40 60 2 Telephone cornmunictns 3 7,650 7,500 98 1 1 3 Short-trm busn credit 3 5,050 2,500 75 25 4 Whol computers/softwr 2 26,000 25,000 98 2 5 Mfg industrial gases 2 35,000 20,000 50 50 6 Whol office supplies 2 12,500 7,500 30 70 7 Photocopying service 2 5,500 5,000 100 8 Mfg electric test prd 1 60,000 60,000 100 9 Whal misc profsn eqpt 1 35,000 35,000 100 10 Misc business service 1 10,000 10,000 50 50 11 OTHER INDUSTRIES 26 20,400 5,000 66 28 6 Other Payment Categories: cash experiences 0 0 0 Payment record unknown 0 0 0 Unfavorable comments 0 0 0 Placed· for collection with D&B 0 0 other 0 NIA The highest "Now owes" on file is $25,000 Page 2 of 7 ,usincss lnfommtion Report: AcC\.l1est Cort1crration T!le ng,arogat.e dollar <\!?,Ctutt of tho 48 ~o:{ilV"..nt ex:prn:lences in ~S'ti fil~ ec:p.:uus • 3i.: Qt uus Ct::'ll!PMY • 1, average monthly t;a:l es. ln OUn £ .a:radstrcct • s ¢pioian. PQ'lll!Ont ex:peri<?ncc:.; exceeding 1n of <i company's ~ve:rage t:'IOothlY t;.;l~t;: ca."1 be con:;.idi$Utd repri:,s~:H.rtt.lv~ of pilyt11ttnt. r,t1d·orma.,ce. ~-=;.;;.·':~"""· ..... ,;~;.;;.:;=:;::,.~<;:~.=-·::..~• \t'tio:4 ~:;.::::,::;;:::;;:,;:::::=.:=-::~·•·'3111 :;i:;;:,::::.·==-====.:: ·:t-t!!:'., i,:~-1:,;:;::::-:.:==·===: ===-~ ~ ':" ".!:':. P:\':'Hl:!lr:I'S INoounts may be r·omtdw t.o nuresc fi!:t'J:.n:: in prescribed rll..'19Cs) Ant I<i -;mc.icii,ated l P<'.lynwH1t1; l'e<::eived prior to t;it,,t.e of irivoke! Oh,1'! -Dhcou:,ted {Peiymcnts rec~ived within t:raut::: tH!}count. penodl Ppt !'r<s:npt [P,$ytn<mts received within t<.Mrrt:, granted) OS!Oi> 04/0'" O'.i/0 0?/()6 01 ! (jf, U/(h., .U./05 09/0S 07 /0S OS/OS ouos 02/05 (;.l /05 Pp't Fpt Ppt Fpt 1?,Pt Ppt Ppt Fpt Ppt-S!ow lO Pvt.-S QW 10 Pr:.t.-s:.ow 10 :ppt ~slow 10 PJ?t:-s:aw JO Ppt. -S:.O'"' '.'Hl Fptc-S:'iow 30 Ppt-s:ow :so !>pt-S:.ow JO Slow 30 SlrJW JO SJQW lO-JQ rnni Sat.!. dac:tory. ?pt F'pt•Slcw 3-0 ?pt: Pp:: ~ Siow J. D Ppt~s:.aw 10 Pp:;:: Ppt Pp::.. Ppt Ppt. FD~ ~ -Pp': l?p: t??t 1;-p,;: S!-ow JO S10'W 30 Pp":: Ppt .Slo1t.• S-JO Sl<r"'' l 80 r-.. v~ Pvt r..ea:t'..e '11gr(:el'!'.ent. U!GH: cR.EDrr 2SOOO 35000 7500 5000 zscm 100 50 50 20000 1SOOQ '10000 7500 lSOO 2;;00 HH:10 HlOO 500 100000 5000 2~00 UH} 60000 1000 lSO 100 100 100 100 100 35000 250-00 7500 5000 soo so 500 so no UHl 50 SU 500 NOW !~AST sr:u.n,za OW:IS OtrE 't'a~MS 2SOOO 7.$00 2stmo ,ooo N3(. 7500 -o-5000 -0-2500 -0--o--Q--0--0-50 -o-l sooo :0 10000 !000 10000 ~o-sooo 500 NlO 751') -o-~O•· -o-500 -o--o--o-NS.IJ -o--ti--o--o--o--o--o--n-2SOO -<i-soo ·O -0-~O· .N30 100 50 -o-·O· 50 -0--0-~<>-NlO 10000 -0· 2'500 -0-?SO -0· 5000 500 ~o~ -o--()~ -o--o--o-•0--!'J--o--()--o--<>--o--o-t.rlO so ::0 -0--0-NlO !.,AS'!.' SALe tH't!Ut. !. ~ l tto !. ~:; =-f1o l ti!o 6 • 12 t,-.;;;a ~-5 Mos ! f6 l ~.o :. t{Q l fJ.o 1 t.l'.c> l f,',o ' V.o 'l Mo 2-J Mo::. 6-12 Mot: l ¥.a 6<t2 Ma£ 6-12 Y.os ;2 l Mo : t'!O :. 1'10 '.'.. t-to :.. !<!o 6 · 12 fl.OS 6 • !2 fl.OS 6 12 MOE! ! Ho l l{O : i?.O l Mo ! Mo G-12 Mos 6-17 Mos 5-17. Mov fi-1 :, t,!J,;11, <l-S Mof; 6-12 ?>'..;)!! 6-12 P.os 6 12 Mos Pagel of 7 lusiness Information Report: Accutest Corporation FINANCE 05/24/06 Lease agreement Ppt 2500 2500 -0- Ppt 50 -0- -0-N30 6-12 Mos Ppt-Slow 30 2500 2500 2500 2-3 Mos * Payment experiences reflect how bills are met in relation to the terms granted. In some instances payment beyond terms can be the result of disputes over merchandise, skipped invoices etc. * Each experience shown represents a separate account reported by a supplier . Updated trade experiences replace those previously reported. Fiscal Fiscal Dec 31 2003 Dec 31 2004 Curr Assets 15,958,000 18,113,176 Curr Liabs 1,570,000 1,160,060 Current Ratio 10.2 15 .6 Working Capital 14,388,000 16,953 ,116 Other Assets 3,981,000 4,921,170 Worth 14 ,727,000 16,824,334 Sales 37,500,000 41,500,000 Long Term Liab 3,642,000 5,049,952 Fiscal Dec 31 2005 22,148,454 1,618,727 13. 7 20,529 ,727 4,286,872 19,136,746 45,000,125 5,679,853 Submitted MAY 23 2006 by Vincent Russo, CFO. Accountant: Nasberg CPAs, PLLC, New York, NY. ACCOUNTANTS OPINION: A review of the accountant's opinion indicates the financial statements meet generally accepted accounting principles and that the audit contains no qualifications. --0-- ------STATEMENT ITEM EXPLANATIONS------ The complete balance sheet was reviewed in its entirety and the above highlights were extracted for publication. It is noted there are no intangibles. The statement includes no deferred credits. Contingencies: None. Non-current assets consist of deposits, property and equipment. Long term liabilities consist of bank debt and notes payable. CURRENT ASSETS: Consist of cash, accounts receivable and investments. CURRENT LIABILITIES: Consist of accounts payable, accruals and taxes. LIQUIDITY: Liquid assets provide full coverage of current liabilities. On May 24, 2006, Vincent Russo, CFO, confirmed company name, address, principals and operational information using Dun & Bradstreet's Internet-based update method (eUpdate) at www.dnb.com . ---------------------------------------=====~~~-~=---------===================- PUBLIC FILINGS The following data is for information purposes only and is not the official record. Certified copies can only be obtained from the official source. * * * UCC FILING(S) * * * COLLATERAL: Inventory including proceeds and products FILING NO: 1951103 DATE FILED: TYPE: Original LATEST INFO RECEIVED: 12/30/1999 02/16 /2000 qRr P~R'l'Y· PTTNRY ~nWF.~ rRF.OTT rORPORATTON . FILED WITH: SECRETARY OF Page 4 of 7 lusiness Information Report: Accutest Corporation SHELTON, CT DEBTOR: ACCUTEST LABORATORIES SOUTHEAST STATE /UCC DIVISION, NJ COLLATERAL: Leased Inventory including proceeds and products FILING NO: 2074817 DATE FILED: 11/19/2001 02 /11/2002 TYPE: Original SEC. PARTY: CIT TECHNOLOGY FINANCING SERVICES INC, LIVINGSTON, NJ DEBTOR: ACCUTEST CORPORATION LATEST INFO RECEIVED: FILED WITH: SECRETARY OF STATE/UCC DIVISION, NJ COLLATERAL : All Account(s) including proceeds and products -All Chattel paper including proceeds and products -All General intangibles(s) including proceeds and products -All Contract rights including F I LING NO: proceeds and products 1991542 TYPE: Original SEC. PARTY: FLEET BANK, N.A., BRIDGEWATER, NJ DEBTOR: ACCUTEST CORPORATION DATE FILED: LATEST INFO RECEIVED : 08/14/2000 08 /29 /2000 FILED WITH: SECRETARY OF STA'l'E/UCC DIVISION, NJ COLLATERAL: All Account(s) and proceeds -All Chattel paper and proceeds FILING NO: 20826642 DATE FILED: 01/11/2002 TYPE: Original LATEST INFO RECEIVED : 02/22/2002 SEC. PARTY: FLEET NATIONAL BANK, FREEHOLD, FILED WITH : SECRETARY OF NJ STATE/UCC DIVISION, DEBTOR: ACCUTEST CORPORATION NJ COLLATERAL : Account(s} including proceeds and products -Equipment including proceeds and products -General intangibles(s) including proceeds and products -Contract rights including proceeds and products - Chattel paper including proceeds and products FILING NO: 040069787677 DATE FILED : 06 /01/2004 TYPE: Original LATEST INFO RECEIVED: 06 /14/2004 SEC. PARTY: FLEET NATIONAL BANK, N.A ., NEW FILED WITH : SECRETARY OF DEBTOR: YORK, NY ACCUTEST LABORATORIES GULF COAST , INC. STATE/UCC DIVISION , TX COLLATERAL: Account(s) including proceeds and products -Equipment including proceeds and products -General intangibles(s) including proceeds and products -Contract rights including proceeds and products - Chattel paper including proceeds and products FILING NO: 9916 7 056 DATE FILED: 08/16/1999 TYPE: Original LATEST INFO RECEIVED: 09/07 /1999 SEC. PARTY: FLEET BANK, NA, BRIDGEWATER, NJ FILED WITH: SECRETARY OF DEBTOR : ACCUTEST LABORATORIES GULF STATE/UCC DIVISION, COAST' INC . ' HOUSTON I TX COLLATERAL: Account(s) -Equipment FILING NO: 20826666 TYPE: Original SEC . PARTY: FLEET NATIONAL BANK, FREEHOLD, NJ DEBTOR: ACCUTEST CORPORATION COLLATERAL: All Equipment FILING NO: 2005302 TYPE: Original SEC. PARTY: FLEET NATIONAL BANK, BRIDGEWATER NJ DEBTOR: ACCUTEST CORPORATION (F.K.A. PATERSON CLINICAL LABORATORIES, INC.) TX DATE FILED: LATEST INFO RECEIVED : 01 /11/2002 02/22/2002 FILED WITH: SECRETARY OF STATE /UCC DIVISION, NJ DATE FILED : 10/25/2000 LATEST I NFO RECEIVED: 12 /04/2000 FILED WITH: SECRETARY OF STATE /UCC DIVISION, NJ Page 5 of7 lusiness Information Report: Accutest Corporation COLLATERAL: Equipment including proceeds and products FILING NO: 1925024 DATE FILED: 08/20/1999 09/24/1999 TYPE: · SEC. PARTY: Original SUMMIT BANK, HACKENSACK, NJ PATERSON CLINICAL LAB, INC. and OTHERS LATEST INFO RECEIVED: FILED WITH: SECRETARY OF STATE/UCC DIVISION , NJ DEBTOR: COLLATERAL: Equipment FILING NO: 23394568 TYPE: Original DATE FILED: 01/20/2006 LATEST INFO RECEIVED: 02 /13 /2006 FILED WITH: SECRETARY OF SEC. PARTY: BANK OF AMERICA, NA, FARMINGTON, CT STATE/UCC DIVISION, NJ DEBTOR: ACCUTEST CORPORATION There are additional UCC's in D&B 's file on this company available by contacting 1-800-234-3867 . The public record items contained in this report may have been paid, terminated, vacated or released prior to the date this report was printed. ====~;==~======-==-----------=========:===~~==================--------========= HISTORY 05 /24/06 VINCENT J PUGLIESE, PRES-CEO RALPH PUGLIESE JR, V PRES DIRECTOR(S): THE OFFICER(S) VINCENT J RUSSO, EXEC V PRES-CFO RALPH PUGLIESE SR, STOCKHOLDER ***CORPORATE AND BUSINESS REGISTRATIONS*** PROVIDED BY MANAGEMENT OR OTHER SOURCE The Corporate Details provided below may have been submitted by the management of the subject business and may not have been verified with the government agency which records such data . REGISTERED NAME: Accutest Corporation CORPORATION TYPE: PROFIT BUSINESS TYPE: CORPORATION STATE OF ORGANIZATION (INCORPORATION): NEW JERSEY DATE OF ORGANIZATION (INCORPORATION) : 04/07/1956 WHERE FILED: Secretary of State, Trenton, NJ COMMON STOCK: AUTH SHARES -5,000 PAR VALUE -NO PAR VALUE On April 19, 2004, the Secretary Of State confirme d this busines is correctly captioned as a Corporation which is registered in the State of New Jersey. Filing #0100123973. Business started 1956 by Ralph Pugliese Sr. 100 % of capital stock is owned by officers. VINCENT J PUGLIESE born 1955. Graduated from Cook College, New Brunswick, NJ, with BS Degree in Environmental Sciences in 1977 . Active here since 1977. Is currentlv oresident and chief executive Page 6 of7 iusiness Infonnation Report: Accutest Corporation officer. VINCENT J RUSSO born 1957. Graduated Rutgers University , New Brunswick, NJ in 1979 and is a CPA. 1979 to 1982 active with Coopers & Lybrand, New York, NY. 1983 to 1986 active with MR Weiser & Co, CPA's, New York, NY. 1986 to present active here as cfo and executive-vice president. RALPH PUGLIESE JR born 1951. Graduated from Seton Hall University, South Orange, NJ in 1974. Active here since 1974, currently as vice president. RALPH PUGLIESE SR born 1923. Graduated from Denver University, Denver, CO and Jefferson College, Hillsboro, MO . 1943 to 1946 served in the United States Army. 1946 to 1961 employed by American Smelting & Refining Company, Perth Amboy, NJ lastly as director of the medical laboratory. AFFILIATE: The officers also appear as principals in: (1) Pugliese Invesco, partnership of officers, Dayton, NJ. Started 1982 real estate holding company. DUNS #15-055-6256. Owns real estate at captioned address. Intercompany relations confined to landlord-tenant. (2) Accutest Laboratories of New England Inc, located in Marlborough, MA. Started operations in Nov 1990 . DUNS #80-488-7768. Operates as an environmental testing laboratory . No intercompany relations were reported by management. (3) Accutest Laboratories Southeast Inc, Orlando, FL, started 1995. Operates as an environmental testing laboratory. Intercompany relations: None reported by management . (4) Accutest Laboratories Gulf Coast, Inc, located in Houston, TX, started in 1999. Operates as an environmental testing laboratory. Intercompany relation: none reported by management. Business address has changed from 2235 Us Highway 130 Bldg B, Dayton, NJ, 08810 to 2235 Us Highway 130, Dayton, NJ, 08810. ------------------------------------------------------------------------------- OPERATION 05/24/06 Operates an environmental testing laboratory (100%). Terms are contractual basis. Has 500 account(s). Sells to commercial concerns and government. Territory: United States. Nonseasonal. EMPLOYEES: 325 which includes officer(s). 200 employed here. FACILITIES: Rents 50,000 sq. ft. on 1st floor of l story steel building. Rents from sister partnership. LOCATION: Industrial section on well traveled highway. BRANCHES: This business has additional branches; detailed branch information is available in D&B's linkage or family tree products. 05-25 (lBM /866) 99999 001081081 H Fleet Bank © 2006 Dun & Bradstreet Inc . January 14 , 2006 -GTO FULL DISPLAY COMPLETE ------------------····---------------- Page 7 of7 ACCUTEST LABORATORIES GULF COAST, INC. Page: 1 of 1 REMIT TO : 2235 Route 130 Dayton, NJ 08810 (732) 329-0200 FAX (732) 329-3499 FED ID# 22-3654510 To : Attn: Accounts Payable Terms: NET 30 Project description: Invoice Number : Invoice Date: P.O. Number: Account Code : Lab Project Code: Job.#: Date Rec:: Tl8626 os/2§/07 .·.· ~~l9·t1:±- 2 AQ 2 AQ 16 so 16 so 16 so 16 so 1 so Tota-1 FDr Invoice Total Due For Invoice vs260MoGBTx XVOXY5 %SO L V5035KITFL V8260MOGBTX XVOXY5 ENERGY GRO, BTEX, Naphthalene -14 MTBE , TBA, DIPE, TAME, E 14 Solids, Total Percent 14 $12/1 Field Methanol Kit 14 GRO, BTEX, Naphthalene -14 MTBE , TBA, DIPE, TAME, E 14 Energy/Fuel Surcharge 14 Job Total Net T9-13581 60 .00 25 .00 0 .00 12.00 60.00 25.00 7.5 0 120.00 50.00 0 .00 192.00 960 .00 400.00 7.50 1729.50 1729.50 1729.5 0 1729.50 ll]r!j New Jers ey l3At:g~I~ ,, h (, ' <: • '·' ,· !' ACCUTEST LABORATORIES 1956-2006 Technical Report for DEMO Account Demo Site Demo Accutest Job Number : ]131 Sampling Date: 05/26/05 Report to: Demo LabLink Account vjp @accutest.com ATTN: Vince Pugliese Total number of pages in report: 193 Test results con tain ed wit hin this dat a pac ka ge meet th e requirements of the Na tion al Env ironm ent al Laborato ry Accreditation Conference and /or state speci fi c cer tifi ca tion pro grams as appli cab le. e-Hardcopy 2.0 A utomated Report 03 /14 /06 @;e=- President Cer tifi ca tion s: NJ(1 2129). NY (l0983), CA, CT, DE, FL , IL , IN, KS , KY , LA, MA, MD , Ml , MT , NC, PA, RI , SC , TN , VA , WV Thi s report shall not be reproduced, excep t in it s enti re ty, without th e written approva l of Acc ut est Labo rato ri es. New Jersey • 2235 Route 130 • Dayton, NJ 08810 • tel : 732 -329 -0200 • fax : 732-329-3499 • h1tp://www.acc ut es t.co m 111!1 1 o f 193 gACCUTEST. J131 · ,. ' ' ., ., · Sections: Table of Contents -1 - Se cti on 1: Sa mpl e S umm a ry ................................................................................................... 3 Section 2: Case N arrative/Conformance Summary .............................................................. 4 Section 1: "lan1ple J{esults ........................................................................................................ 5 3 I: 1131-1 : E lO ................................................................................................................... 6 3.2: 1131 -2 : E 14 ................................................................................................................... 8 3.3: 1131-3: E5R .................................................................................................................. 10 3.4: 1131-4: PIO ................................................................................................................... 12 3.5: 1131-5 : Pl IA ................................................................................................................ 14 3.6: 1131-6 : Pl4 ................................................................................................................... 16 3.7: 1131-7 : P6 ..................................................................................................................... 18 3.8: 1131-8: P7 ..................................................................................................................... 20 3.9: 1131-9 : Wl4 .................................................................................................................. 2 2 3.10: 11 3 1-10 : Wl7 .............................................................................................................. 2 4 J.11 1131 -11 : W6 ................................................................................................................ 26 3. l 2: 1131 -12: FB .. . .. . . .. . . . . .. .. .. .. .. .. .. .. .. .. .. .. . . . . . . . . .. . .. .. .. .. .. .. .. .. .. .. .. .. .. . . .. .. .. .. .. . . .. .. .. .. .. .. .. .. .. .. .. .. 2 8 Section 4: l\1isc. Forms ............................................................................................................ 30 4. l: Cha in of Custody .. .. . . . . . .. .. . . . .. .. . . . . . . . . . . .. . . . . . .. .. .. . . . . ... . .. . . . . .. .. . . .... . . . .. . . . . . .. . . . . . . . . . . .. . . . . ... . ... . . . . . 31 4.2: S ample Tracking Chronicle ........................................................................................... 32 4.3: Internal Ch a in of Custody .. .. .. .. .. .. .. .. ... .. .. .. .. .. . .. .. .. . .. .. .. ... . . .. ... ... . . . .. . . . .. . . . .. . . . .. .. .. .. . . . . . .. . . . . . 34 Section S: GC/MS Volatiles -QC Data Summaries .............................................................. 43 5.1: M ethod Blank Summary .. . . . .. .. . . . .. .. .. ... .. ... .. .. . . . . . ... . . .. .. . . . . . .. .. ... .. .. . .. .. . . . . .. . . . . .. .. .. . . . . . . . .. . . . . . . 44 5.2: Blank Spike Summary ................................................................................................... 47 5.3: Matri x Spike/M atri x Spike Duplicate Summary ........................................................... 50 5.4: Instrum ent Performance Checks (BFB) ......................................................................... 53 5.5: Internal Stand a rd Are a Summari e s ................................................................................ 59 5.6: Surrogate R ecov ery Summari es ...................................... : .............................................. 63 5.7: Initial and Continuing Ca libration Summarie s .............................................................. 64 Section(): (;(:/1\·tS \'olaHJes -R.a,v Data................................................................................ 67 (,.1 : Samples . . . . . . . . . . . . . . . . .. . . . . . .. .. ... .. .. .. . . . . . . . . . . . .. .. . . . . .. . . .. . . . .. . . . .. . . .. .. . . . .. . . . .. . . . . . .. .. . ... . . . . . . . .. .. .. .. . . . .. . . 6 8 6.2: Method Bla nks............................................................................................................... 132 S ection 7: Metals Analysis -QC Data Summaries ................................................................ 138 7.1: Inst QC M A 15 849 : Pb ................................................................................................... 139 7.2: Inst QC M A 15 8 63 : Pb ................................................................................................... 171 7.3: Prep QC MP30351: Pb .................................................................................................. 189 I I I I II ~l!I 2 of 193 l3ACCUTESI. J131 l :· :: ,, 1 ') ,. ''. \ Accutest LabLink @09 :06 14-Mar-2006 Sample Summary DEMO Account Demo Site Project No: Demo Sample Collected Matrix Number Date Time By Received Code Type J131-1 05/26 /05 14 :30 BB 05 /27 /05 AQ Ground Water J131-2 05/26 /05 15 :45 BB 05 /27 /05 AQ Ground Water J131-3 05 /26 /05 13 :55 BB 05 /27 /05 AQ Ground Water J131-4 05 /26 /05 15:20 JA 05 /27 /05 AQ Ground Water J131-5 05 /26 /05 14:20 JA 05 /27 /05 AQ Ground Water J131-6 05/26 /05 13:50 JA 05/27 /05 AQ Ground Water J131-7 05/26 /05 13 :25 BB 05/27 /05 AQ Ground Water J131-8 05/26 /05 15 : 10 BB 05/27 /05 AQ Ground Water J131-9 05 /26 /05 13:15JA 05 /27 /05 AQ Ground Water ]131 -10 05 /26 /05 15:50 JA 05 /27 /05 AQ Ground Water ]131-11 05 /26 /05 14:50 JA 05 /27 /05 AQ Ground Water ]131-12 05/26 /05 15 :40 BB 05/27 /05 AQ Field Blank Water Job No: Client Sample ID ElO E14 E5R PlO PllA P14 P6 P7 W14 W17 W6 FB I J131 111!1 3 of 193 l3ACCU I ES I. J131 ',, '" ,. ' ., "' Labor,1Lo1 ,e;, SAMPLE DELIVE RY GRO UP CA SE N ARRATIVE C lien t: DEMO Job No J l3 1 S ite : Demo Sit e Rep o rt Date 6/l 7!2005 5 :27:48 P M 1 1 Samp le(s ), 0 Trip Bla nk (s) ru1d I F ie ld Bla nk(s ) were c oll ected o n 05 /26/200 5 a nd were received a t Acc utes t o n 05 /27/2005 p ro p e rl y preserve d , a t 4 .2 Deg. C a nd int ac t. These S amp les rece ived a n Ac c utes t jo b numb er o f J 13 1. A lis tin g o f the La b o rat ory Sample ID , C lie nt Sam p le ID ru1d d ates of co ll ection are prese nt ed in th e Res ult s S ummary Sectio n o f th is re p o rt . Excep t as no te d below, a ll meth o d s p ec ified ca li b ratio ns a nd qua lit y control p erfo miance c rit eria were met fo r th is jo b . Fo r more in fo nn a t io n, p lease re fe r to QC s umm ary p ages. Volatiles by GCMS By Method EPA 624 I Matrix AQ Batch ID : V0 43 66 • A ll samples we re ruia lyzed w ithin th e rec ommend e d m etho d h o ldin g time . • A ll meth od bl a nks fo r th is b atc h meet me th od s p ecifi c c rit eri a. Sample(s) J2 17-I MS , J2 I 7-I MSD were used as th e QC samp les in di cated . • Ma tri x S p ike and Mat rix S pik e Duplicate Recovery(s) fo r Me th y l T e rt B uty l Eth er ar e o ut s id e co ntrol limi ts . O uts id e co ntro l limi ts due to hig h leve l in sam p le rela ti ve to s pike a mo unt. Matri x AQ Batch ID : V0 4367 • A ll s a m p les we re ruia lyzed w ith in th e re co mm e nd ed metho d ho ldin g tim e . • A ll m ethod b la nk s fo r th is b a tc h meet me th o d s p ec ifi c c rit eri a . • Sample(s) J 13 1-IMS , J 13 1-1 MS D were used as th e QC samp les indicated . Matr ix AQ Batch ID : V0 4368 • A ll s a m p les we re ruia lyz ed w ithin th e reco mm e nd ed meth o d ho ldin g tim e . • A ll m etho d bla nks fo r th is b atc h mee t me th o d s p ec ifi c c rit eri a . • Samp le(s) J523 -3MS , J523 -3 M SD w ere used as th e QC samp le s indicate d . • Matrix Sp ike a nd Ma trix S pike D upli cate R eco ve ry(s) fo r Meth yl Tert Butyl Eth er, Terti ary Butyl A lco ho l are o uts id e contro l limits . O utsid e co nt ro l limit s due to hi g h level in s runp le re lativ e to s pike amo u nt. Metals By Method EPA 200.7 I Matri x AQ Batch ID : M P3035 I • A ll samp les w ere d iges ted w ithin th e rec o mm end ed me th o d ho ldi ng tim e . • A ll s a mples were ruia lyzed within th e reco mm end e d meth o d ho lding tim e . • A ll me th od b lanks fo r th is b atc h meet meth o d s p ec ifi c c rite ri a . • Sample(s) .11 3 1-I MS , J 13 1-1 MSD, J 13 1-1 S D L were u se d as th e QC sa mples fo r me tals . T he A ccute s t La bora to ri es o f Ne w Je rs ey certifies th at a ll a na ly sis were p e r fo rm ed w ithin me th o d s p ec ifi catio n . It is furth er re c o mm e nded tliat th is re p o rt to b e us e d in its entir ety.T he Acc utes t La boratories of NJ, Laboratory D irec to r o r ass ig nee as ve rifi ed b y the s ig nature o n the cover page h as a uth o rize d th e re lease o f thi s re p o rt (J 13 I). F rida y,June 17 ,2005 Page 1 ofl 111!1 4 of 193 l:iACCUTEST. J131 l :' :• t ! ') •:' Appendix A Laboratory Data Package Cover Page This data package consists of: This signature page , the laboratory review checklist, and the following reportable data: Rl Field chain-of-custody documentation; R2 Sample identification cross-reference; R3 Test reports (analytical data sheets) for each environmental sample that includes: a) Items consistent with NELAC 5.13 or ISO /IEC 17025 Section 5.10 b) dilution factors, c) preparation methods , d) cleanup methods , and e) if required for the project, tentatively identified compounds (TICs). R4 Surrogate recovery data including: a) Calculated recovery (%R), and b) The laboratory's suITogate QC limits. RS Test reports/summary fom1s for blank samples; R6 Test reports/summary forms for laboratory control samples (LCSs) including: a) LCS spiking amounts , b) Calculated %R for each analyte , and c) The laboratory 's LCS QC limits. R7 Test reports for project matrix spike/matrix spike duplicates (MS/MSDs) including: a) Samples associated with the MS /MSD clearly identified, b) MS /MSD spiking amounts, c) Concentration of each MS/MSD analyte measured in the parent and spiked samples , d) Calculated %Rs and relative percent differences (RPDs), and e) The laboratory's MS /MSD QC limits R8 Laboratory analytical duplicate (if applicable) recovery and precision: a) the amount of analyte measured in the dup licate, b) the calculated RPD , and c) the laboratory's QC limits for analytical duplicates. R9 List of method quantitation limits (MQLs) for each analyte for each method and matrix ; RIO Other problems or anomalies . The Exception Report for every "No" or "Not Reviewed (NR)" item in laboratory review checklist. Re lease Statement: I am responsible for the release of this laboratory data package. This data package has been reviewed by the laboratory and is complete and technically compliant with the requirements of the methods used, except where noted by the laboratory in the attached exception reports . By me signature below, I affirm to the best of my knowledge , all problems/anomalies, observed by the laboratory as having the potential to affect the quality of the data , have been identified by the laboratory in the Laboratory Review Checklist, and no information or data have been knowingly withheld that would affect the quality of the data. Check, if app li cable: [ ] This laboratory is an in-house laboratory controlled by the person responding to rule. The official signing the cover page of the rule-required report (for example, the AP AR) in which these data are used is responsible for releasing this data package and is by signature affirming the above release statement is true. Ron Martino Lab Director 9/5/2007 Name (Printed) Signature Official Title (printed) Date RG-366 /TRRP-13 December 2002 A l 1. It ems identified by the letter "R" must be in clud ed in th e laboratory data package sub mitte d in th e TRRP -requ ired report (s). Items identified by the lett er "S" should be retain ed and made avai lable upon requ es t fo r th e appropriat e retention period. Appendix A (cont'd): Laboratory Review Checklist: Reportable Data Labo rato ry Name: Acc ut est Laboratories Gu lf Coas t LRC Date : 9/5/2007 Project ame: Borke Property Laboratory Job Number : Tl 8665 Rev iew er Na me: Ron Marti no Prep Batch Numb er(s): #I A2 Description Yes No NA 3 NR4 ER#5 Chain-of-cu sto dy (C -0-C) RI 0 1 Did sa mple s meet the laboratory's sta ndard co nditions of sa mpl e acceptability upon rece ipt ? X Were a ll departure s from standard co ndition s descr ib ed in an exce ption re port? X R2 0 1 Sa mple and quality control (OC) identification Are a ll field samp le ID numbers cross -r eferenced to the laboratory ID numb ers? X Are a ll laborator y ID numb e rs cross -refe renced to th e correspondin g Q C data ? X R3 0 1 Test reports Were a ll samp les prepared and ana lyze d within holdin g tim es? X Other th an tho se res ult s < MQL , were a ll other raw va lu es bracketed by calibration sta nd ards? X We re calculation s checked by a peer or sup erviso r? X We re all analyte identificat ions checked by a peer or sup erv isor? X Were samp le quantitation lim it s reported fo r a ll ana lytes not detected? X Were al l resu lt s for so il and sed im ent sa mpl es re ported on a dry weight bas is ? X Were% moi sture (or so li ds) reported for a ll soi l and sed im ent sa mpl es? X If required for th e project , T ICs reported ? X R4 0 S urrogate recovery dat a We re s ur rogates added prior to extr actio n? X Were s urro ga te percent recoveries in al l samp les within the la bo ra tor y QC limits ? X RS OI Test reports/s ummary forms for blank sa mples We re a ppropri ate type(s) of bla nks ana lyzed? X Were b lanks a nal yze d at t he approp ri ate freq uency? X Were method bl a nks taken throu gh the entire ana lytica l process , includin g preparation and , if X ap pli cab le, cleanup procedures ? Were bl ank concen tra ti ons < MQL? X R6 0 1 Laboratory control sa mples (LCS): Were a ll COCs inc lu ded in the LCS? X Was eac h LCS take n through the ent ir e ana lytica l pro ced ur e, in c lud ing prep a nd c le anup steps? X Were LCSs ana lyz ed at th e required fr equency? X Were LCS (and LCSD , if app lic ab le) %Rs withi n the la borato ry QC limit s? X Does the detectabi li ty data docum ent th e labora to ry's capab ilit y to detec t the COCs at the MDL use d X to ca lcu late the SQLs ? Was the LCSD RPO within QC limit s? X R7 0 1 Matrix s pike (MS) an d matrix spike duplicate (MSD) data Were the project/method specified ana lyte s inc lu ded in the MS an d MSD ? X Were MS /MSD ana lyze d at the appropr iat e frequency ? X Were MS (a nd MSD, ifaoo li cab le) %Rs within the laborato ry QC limits? X 2 Were MS /MSD RPD s wit hin la borato ry QC limits ? X RS 0 1 A nal yt ical duplicate data Were appropr iate ana lyt ical dup li cates ana lyze d for each matri x? X Were ana lytica l dup li cates ana lyze d at the appro pri ate fr equ enc y? X We re RPD s or re lati ve sta ndard deviations wi thin the laboratory QC limits? X R9 0 1 Method quantitation limit s (MQLs): Are the MQL s for eac h met hod ana lyte in c luded in the la borato ry data package? X Do the MQLs correspond to the conce ntrati on of the lo west non-z ero calibration standard? X Are unadju ste d MQL s includ ed in the laboratory data package? X RIO 01 Other problems/anom alies Are a ll known problems/ano malies/special co nditi ons noted in th is LRC and ER? X We re all ne cessary co rr ective ac tions performed for the reported data? X Was a pplicable a nd ava il ab le techno lo gy used to lower the SQL minimi ze th e matrix int erfer ence X affects on the sa mple results? 2 . = orga ni c ana lyses ; I = inorganic analyses (a nd ge neral chemistry, when ap pli ca bl e); 3. NA= No t ap pli cab le; 4. NR = No t reviewed; 5. ER#= Exce ption Report identification numb er (an Excep ti on Report shou ld be com pl eted for an it em if "NR" or "No" is checked). RG -366/TRRP -1 3 Dece mber 2002 A2 Appendix A (cont'd): Laboratory Review Checklist: Reportable Data 1 Laboratory Na me : Accutest Laboratories Gulf Coast LRC Date: 9/5/2007 \,_!Project Na me : Borke Prop ert y La boratory Job Number : Tl 8665 \. Reviewer Na me: Ron Martino Prep Batch Number(s): #' St S2 S3 S4 ss S6 S7 .;s S9 S IO S I I S l 2 S l3 S l6 S IS S l6 A2 Description Yes No NA 3 NR4 0 1 Initial calibration (ICAL) Were re spo nse factors and /or rel at ive response facto rs fo r eac h analyte within QC limit s? X Were per ce nt RSD s or correl at ion coefficient criteria met? X Was the number of standards recommended in the met hod use d for a ll ana lytes? X Were a ll points ge nerated between the lowest a nd hi ghest sta nd ard used to ca lc ul ate th e curve? X Are !CA L data ava il a ble for a ll in struments used? X Has the initi a l ca libration c ur ve be en ver ifi ed us in g a n a ppropriate sec ond so ur ce standard ? X OI Initial and continuing calibration verification (ICCV and CCV) and continuing calibration Was the CCV ana lyz ed at the method-required frequenc y? X Were per ce nt differences for eac h ana lyte within the met hod -r equi red QC limit s? X Was the ICAL curve ver ifi ed for eac h analvt e? X Was the abso lut e va lue of th e ana lyte concentratio n in the ino rga ni c CC B < MDL ? X 0 Mass spectral tuning: Wa s the a ppropri ate co mp o und for the method used for tunin g? X Were ion a bund ance dat a within the met hod-required QC limit s? X 0 Internal standards (IS): Wer e IS are a co unt s and retention time s wit hin the method-req uir ed QC limits? X 0 1 Raw data (N ELAC section 1 annendix A e:lossary. and section 5 .12 or ISO /IEC 17025 section Were th e raw data (for examp le, chrom atograms , s pectra l data) reviewed by an ana lyst? X Were data associated wit h ma nual int egrations fl agged on the raw data? X 0 Dual column confirmation Did dua l co lumn confirmatio n results meet the met hod-requ ir ed QC? X 0 Tentatively identified compound s (Tl Cs): If TI Cs we re reque sted , were the mass spectra and TIC dat a s ubj ect to appropr iate checks? X I Interference Check Sample (ICS) results: Were pe rcent recoveries within met hod QC limits? X X I Serial dilutions po st die:estion spikes and method of standard additions Were percent diffe rences, recoveries, and th e linear ity within th e QC li mits spec ifi ed in the method ? X OI Method detection limit (MDL) studies Was a MDL st ud y performed for each reported ana lyte? X Is the MDL eit her adjusted or s upported by the ana lysis of DCS s? X 01 Proficiency test reports: Was the laborator y's pe rformance acce pt a bl e o n the aoo li cab le proficie ncy tests or eval uation stud ie s? X 01 Standards documentation Are a ll sta nd a rds used in the ana lyse s N IST-trac eable or obta in ed from other approp ri ate so urces? X 0 1 Compound/analyte identification procedures Are the procedures fo r compo und /ana lvte id entifi cation documented ? X OI Demon stration of analyst competency (DOC) Was DOC conducted consistent w ith NELAC Chapte r SC or ISO/IE C 4? X Is docum ent ation of the ana lvs t 's co mo etenc v uo-t o-d ate and on file ? X 0 1 Verification/validation documentation for methods (NE LAC Chap 5 or !SO /TEC 17025 Section 5) Are a ll the methods use d to ge nerate the data do c um ent ed, ver ifi ed , and va li da ted, where a ppli cab le? X 0 1 Laboratory standard operating procedures (SOPs): Are la boratory SOPs current and on file for eac h met hod performed ? X Item s ide nt ified by the letter "R" shoul d be in clud ed in the labo ratory data package submitt ed to the TCEQ in the TRRP-required report(s). Item s id entified by th e letter "S" sh ould be retained and made avai lable up on requ est for th e ap propr iate retention peri od . 2 0 = organic ana lyses ; I = inorganic ana lyses (and genera l chemis tr y, when app li cable). 3 NA = Not applicab le. 4 NR = Not Revi ewed . 5 ER#= Excep ti on Report identification numb er (an Exception Repor t shou ld be comp leted for an item if "NR" or "No" is checked). RG-366 /TRRP -13 Dece mber 2002 A3 ER#5 Appendix A (cont'd): Laboratory Review Checklist: Exception Reports Laboratory Name: Accutest Laboratories Gulf Coast LRC Date : 9/5/2007 Project Name : Borke Property Laboratory Job Number : Tl 8665 Reviewer Name: Ron Martino Prep Batch Num ber(s): ER#1 DESCRIPTION 1 For reporting pmposes, the MQL is defined in the report as the RL. The unadjusted MQL/RL/SDL is reported in the 2 3 m ethod blank. The SDL/SQL/MDL is defined in the report as the MDL. All anoma li es are discussed in the case narrative. All sample analysis were evalu ated to the MDL/SDL/SQL as per TRRP-1 3 ER#= Exception Report id entification number (an Exception Report should be completed for an item if"NR" or "No" is checked o n the LRC) RG-366/TRRP-13 December 2002 A4 lll)r!!I New Jersey r;jA~Jg~ ,1 !, G • ,~ f ~-:, Sample Results Report of Analysis Section 3 m)l!:j 5 of 193 (iACCUTES I. J131 t:•:'I<.!') •;\ Accutest LabLink @09:06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID : ElO Lab Sample ID : J131-1 Date Sampled : 05/26 /05 Matrix : AQ -Ground Water Date Received : 05/27 /05 Method : EPA 624 Percent Solids : n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096966.D 1 06 /05 /05 SWD n/a n/a V04367 Run #2 096967 .D 5 06 /05 /05 SWD n/a n/a V04367 IRoo #1 Purge Volume 5 .0 ml 5 .0 ml Run #2 Purgeable Aromatics, MTBE, TBA , Naphthalene CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 0 .33 ug/1 108 -88 -3 Toluene ND 1.0 0.11 ug/1 100-41 -4 Ethyl benzene ND 1.0 0.22 ug/1 1330-20-7 Xylenes (total) ND 1.0 0.26 ug/1 1634-04-4 Methyl Tert Butyl Ether 488 a 5 .0 2 .1 ug/1 75-65-0 Tertiary Butyl Alcohol ND 25 10 ug/1 91-20-3 Naphthalene ND 2 .0 0.69 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 l ,2-Dichloroethane-D4 (SUR) 99 % 97 % 63-136 % 2037-26-5 Toluene-DB (SUR) 103% 101 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 85 % 85 % 80-115 % (a) Result is from Run # 2 ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analy te found in associated method blank N = Indicates presumptive evidence of a compound 111!1 6 of 193 l:iACCU I ES r. J131 ',." •' • ., · ,, ' Accutest LabLink @09:06 14-Mar-2006 Client Sample ID : ElO Lab Sample ID : ]131 -1 Matrix : AQ -Ground Water Project : Demo Site Report of Analysis Date Sampled: 05 /26 /05 Date Received : 05 /27 /05 Percent Solids : n/a Metals Analysis Analyte Result RL 3 .0 Units OF Prep Analyzed By Method Lead < 3.0 (1) Instrument QC Batch: MA15849 (2) Prep QC Batch: MP30351 RL = Reporting Limit ug/1 06 /13/05 06/15 /05 JDM EPA 200 .7 I Page 1 of 1 Prep Method EPA200 .72 I fll!t 7 of 193 (iACCUTEST. J131 l :' ~l' i, I ') ,. •:' Raw Data: C•UW..M•M Accutest LabLink @09:06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID: E14 Lab Sample ID : J131-2 Date Sampled : 05/26 /05 I Matrix : AQ -Ground Water Date Received: 05/27/05 Method: EPA 624 Percent Solids : n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096955 .D 50 06 /04 /05 SWD n/a n/a V04366 Run #2 IR"" #1 Purge Volume 5.0 ml Run #2 Purgeable Aromatics, MTBE , TBA, Naphthalene CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 56.0 50 16 ug/1 108-88 -3 Toluene 59 .7 50 5.3 ug/1 100-41-4 Ethylben zene 460 50 11 ug/1 1330-20-7 Xylenes (total) 1570 50 13 ug/1 1634-04-4 Methy l Teri Butyl Ether 6210 50 21 ug/1 75 -65-0 Tertiary Butyl Alcohol ND 1300 510 ug /1 91-20-3 Naphthalene ND 100 34 ug/1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1 , 2-Dichloroethane-D4 (SUR) 102% 63-136 % 2037-26-5 Toluene-D8 (SUR) 102 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 89 % 80-115 % ND = Not detected MDL -M ethod Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 111!1 8 of 193 l3ACCU I ES I. J131 SC' ''" " '> '' ' Accutest LabLink @09:06 14-Mar-2006 Client Sample ID: E14 Lab Sample ID : ]131-2 Matrix : AQ -Ground Water Project: Demo Site Report of Analysis Date Sampled : 05 /2 6/05 Date Received : 05 /2 7 /05 Percent Solids : n/a Metals Analysis Analyte Res ult RL 3.0 Units OF Prep Analyzed By M ethod Lead 10 .3 (1) Instrument QC Batch : MA15863 (2) Prep QC Bat ch : MP30351 RL = Reporting Limit ug /1 06 /13 /05 06 /16 /05 KL EPA 200 .7 1 Page 1 of 1 Prep Method EPA 200 .7 2 I fiial!j 9 of 193 l3ACCU I ES I, J 131 ,,., .•• ,., .,. Raw Data: M•Ui/Mil•W Accutest LabLink @09 :06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID : E5R Lab Sample ID: ]131-3 Date Sampled: 05 /26 /05 Matrix : AQ -Ground Water Date Received: 05/27 /05 Method : EPA 624 Percent Solids : n/a Project: Demo Site File ID OF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096956 .D 1 06 /04 /05 SWD n/a n/a V04366 Run #2 IRun #I Purge Volume 5.0 ml Run #2 Purgeable Aromatics , MTBE , TBA. Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 0.33 ug /1 108-88-3 Toluene ND 1.0 0 .11 ug /1 100-41-4 Ethylbenzene ND 1.0 0 .22 ug/1 1330-20-7 Xylenes (total) ND 1.0 0.26 ug/1 1634-04-4 Methyl Tert Butyl Ether 4.2 1.0 0.41 ug/1 75-65-0 Tertiary Butyl Alcohol ND 25 10 ug/1 91 -20 -3 Naphthalene ND 2 .0 0 .69 ug/1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07 -0 l ,2-Dichloroethane-04 (SUR) 102 % 63-136 % 2037-26-5 Toluene-DB (SUR) 101 % 90-110 % 460-00 -4 4-Bromofluorobenzene (SUR) 88 % 80-115 % ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound fflll!i 1 O of 193 ;;iACCUTEST. J131 ,,. "• "' ., "• Accutest LabLink @09:06 14-Mar-2006 Client Sample ID : E5R Lab Sample ID : J131-3 Matrix : AQ -Ground Water Project: Demo Site Report of Analysis Date Sampled : 05 /26 /05 Date Received : 05 /27 /05 Percent Solids : n/a Metals Analysis Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead <3.0 (1) Instrument QC Batch: MA15863 (2) Prep QC Batch : MP30351 RL = Reporting Limit ug /1 06/13/05 06 /16/05 KL EPA 200 . 7 I Page 1 of 1 Prep Method EPA 200.7 2 I IJl!t 11 of 193 l;iACCUTEST. J131 ~ :' {' f <I I ') •:' Accutest LabLink @09 :06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID : PlO Lab Sample ID: J131-4 Date Sampled: 05/26 /05 Matrix: AQ -Ground Water Date Received: 05 /27/05 Method: EPA 624 Percent Solids: n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096960.D 200 06 /05 /05 SWD n/a n/a V04367 Run #2 096961.D 1000 06 /05/05 SWD n/a n/a V04367 IR·" #I Purge Volume 5.0 ml 5 .0 ml Run #2 Purgeable Aromatics, MTBE , TBA , Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene 83.9 200 65 ug/1 J 108-88 -3 Toluene ND 200 21 ug/1 100-41-4 Ethylbenzene ND 200 44 ug/1 1330-20-7 Xylenes (total) ND 200 51 ug/1 1634-04-4 Methyl Tert Butyl Ether 126000 a 1000 410 ug/1 75-65-0 Tertiary Butyl Alcohol 28300 5000 2000 ug/1 91-20-3 Naphthalene ND 400 140 ug/1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 l ,2-Dichloroethane-D4 (SUR) 103 % 97 % 63-136 % 2037-26-5 Toluene-D8 (SUR) 102 % 103 % 90-110 % 460 -00 -4 4-Bromofluorobenzene (SUR) 85 % 83 % 80-115 % (a) Result is from Run # 2 ND = Not dete cted MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 1!11!! 12 of 193 l:;iACCU I ES I, J131 """"•''' .,. Accutest LabLink @09 :06 14-M ar-2006 Client Sample ID : PIO Lab Sampl e ID : ]131-4 Matrix : AQ -Ground Water Project : Demo Site Report of Analysis Date Sampled : 05 /26 /05 Date Received: 05 /27 /05 Percent Solids : n/a M etals Analysi s Analy t e Result RL 3 .0 Units DF Prep Analyzed By Method Lead 6 .1 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch : MP30351 RL = Reportin g Limit ug /1 06 /13 /05 06 /16/05 KL EP A 200 .7 1 Page 1 of 1 Prep Method EPA Z00 .7 2 ~l!j 13of193 13ACCUTEST. J131 t '.' (i ' <! I '} •: ~ Accutest LabLink @09:06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID: PllA Lab Sample ID : Jl31-5 Date Sampled: 05/26/05 Matrix : AQ -Ground Water Date Received : 05 /27/05 Method : EPA 624 Percent Solids : n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096990 .D 20 06 /06 /05 SWD n/a n/a V04368 Run #2 IRuo #I Purge Volume 5 .0 ml Run #2 Purgeable Aromatics , MTBE , TBA, Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene 3000 20 6.5 ug/1 108-88-3 Toluene 20 .8 20 2.1 ug/1 100-41-4 Ethylbenzene 150 20 4.4 ug /1 1330-20-7 Xylenes (total) 20 .8 20 5 .1 ug /1 1634-04-4 Methyl Teri Butyl Ether 396 20 8.3 ug/1 75-65-0 Tertiary Butyl Alcohol ND 500 200 ug /1 91-20-3 Naphthalene ND 40 14 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 l ,2-Dichloroethane-D4 (SUR) 107% 63-136 % 2037-26-5 Toluene-DB (SUR) 106% 90-ll0% 460-00-4 4-Bromofluorobenzene (SUR) 99% 80-ll5% ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 111!1 14of193 g;JACCU I ES I, J131 • "'' "., ... Accutest LabLink@09:06 14-Mar-2006 Client Sample ID: P11A Lab Sample ID : J131 -5 Matrix : AQ -Ground Water Project : Demo Site Report of Analysis Date Sampled : 05 /26 /05 Date Received : 05 /27 /05 Percent Solids : n/a Metals Analysis Analyte Result RL 3.0 Units OF Prep Analyzed By Method Lead 11.3 (1) Instrument QC Batch : MA15863 (2) Pre p QC Batch : MP30351 RL = Reporting Limit ug /1 06/13/05 06 /16/05 KL EPA 200 .7 I Page 1 of 1 Prep Method EPA 200 .7 2 811!'.1 15 of 193 ;iACCUTEST. J1 31 ',."' •' > ., • Raw Data: ••»MWH•M Accutest LabLink @09:06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID : P14 Lab Sample ID: ]131-6 Date Sampled: 05 /26 /05 Matrix: AQ -Ground Water Date Received: 05/27 /05 Method : EPA 624 Percent Solids: n/a Project : Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096991.D 20 06 /06 /05 SWD n/a n/a V04368 Run #2 IRun #1 Purge Volume 5 .0 ml Run #2 Purgeable Aromatics , MTBE , TBA , Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene 3170 20 6 .5 ug/1 108-88-3 Toluene 59.5 20 2 .1 ug /1 100-41-4 Ethylbenzene 153 20 4.4 ug/1 1330-20-7 Xylenes (total) 138 20 5.1 ug/1 1634-04-4 Methyl Tert Butyl Ether 1450 20 8.3 ug/1 75-65-0 Tertiary Butyl Alcohol ND 500 200 ug/1 91-20-3 Naphthalene ND 40 14 ug/1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 l ,2-Dichloroethane-04 (SUR) 108 % 63-136 % 2037-26 -5 Toluene-OS (SUR) 105 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 105% 80-ll5 % ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ill!I 16of193 l;'iACCU I ES I. J 131 '' ,. • '' ., ., • Accutest LabLink @09 :06 14-Mar-2006 Client Sample ID : Pl4 Lab Sample ID: J131-6 Matrix : AQ -Ground Water Project: Demo Site Report of Analysis Date Sampled: 05/26 /05 Date Received: 05 /27 /05 Percent Solids: n/a Metals Analysis Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead 28.0 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch : MP30351 RL = Reporting Limit ug /1 06 /13 /05 06 /16/05 KL EPA 200 .7 I Page 1 of 1 Prep Method EPA 200 .7 2 ~I! 17 of 193 l3ACCUiESt J131 ,,. "• •' ., "' Accutest LabLink@09 :06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID: P6 Lab Sample ID : J131-7 Date Sampled: 05 /26 /05 Matrix: AQ -Ground Water Date Received : 05 /27 /05 Method: EPA 624 Percent Solids : n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096964.D 200 06 /05 /05 SWD n/a n/a V04367 Run #2 096965.D 1000 06 /05 /05 SWD n/a n/a V04367 IRun #1 Purge Volume 5 .0 ml 5.0 ml Run #2 Purgeable Aromatics , MTBE , TBA, Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene ND 200 65 ug /1 108-88-3 Toluene 467 200 21 ug /1 100-41-4 Ethy lbenzene 220 200 44 ug /1 1330-20-7 Xylenes (total) 1630 200 51 ug /1 1634-04-4 Methyl Teri Butyl Ether 115000 a 1000 410 ug /1 75 -65-0 Tertiary Butyl Alcohol 32200 5000 2000 ug /1 91-20-3 Naphthalene ND 400 140 ug /1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1, 2-Dichloroethane-D4 (SUR) 101 % 99% 63-136 % 2037-26-5 Toluene-D8 (SUR) 102% 103 % 90-110 % 460 -00 -4 4-Bromofluorobenzene (SUR) 87 % 86% 80-115 % (a) Result is from Run # 2 ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound l)l!j 18of193 l:ilACCUIESI, J1 31 } :'. :, '. <. 1 ·> ". Accutest LabLink @09 :06 14 -Mar-2 006 Client Sample ID : P6 Lab Sample ID: J131-7 Matrix : AQ -Ground Water Project : Demo Site Report of Analysis Date Sampled: 05 /26 /05 Date Received: 05 /27 /05 Percent Solids: n/a M etals Analysis Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead < 3 .0 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch: MP30351 RL == Report in g Limit ug/1 06 /13 /05 06 /16 /05 KL EPA 200.7 I Page 1 of 1 Prep Method EPA 200.7 2 111!'.1 19 of 193 liACCU 1ES I. J131 t '.' !'' <l t ') I)< Raw Data: M•UfiUB•M Accutest LabLink@09:06 14 -Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID: P7 Lab Sample ID : J131-8 Date Sampled : 05/26 /05 Matrix : AQ -Ground Water Date Received : 05/27 /05 Method : EPA 624 Percent Solids : n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096971 .D 1 06 /05 /05 SWD n/a n/a V04367 Run #2 IRon •1 Purge Volume 5.0 ml Run #2 Purgeable Aromatics , MTBE , TBA , Naphthalene CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 0.33 ug/1 108-88-3 Toluene ND 1.0 0.11 ug/1 100-41-4 Ethylbenzene ND 1.0 0 .22 ug/1 1330-20 -7 Xylenes (total) ND 1.0 0.26 ug /1 1634 -04 -4 Methyl Tert Butyl Ether 2 .2 1.0 0.41 ug /1 75 -65-0 Tertiary Buty l Alcohol ND 25 10 ug /1 91-20-3 Naphthalene ND 2 .0 0 .69 ug /1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 l ,2-Dichloroethane-04 (SUR) 100 % 63-136 % 2037-26-5 Toluene-OS (SUR) 103 % 90-110 % 460-00 -4 4-Bromofluorobenzene (SUR) 85 % 80-115 % ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound £11!1 20 of 193 ~ACCUIESI. J131 . t :-:·'" 1 ·) ,, • Accutest LabLink @09 :06 14-Mar-2006 Client Sample ID: P7 Lab Sample ID : J131-8 Matrix : AQ -Ground Water Project: Demo Site Report of Analysis Date Sampled : 05 /26 /05 Date Received: 05 /27 /05 Percent Solids : n/a Metals Analysis Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead 6.4 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch: MP30351 RL = Reporting Limit ug /1 06 /13 /05 06/16/05 KL EPA 200 .7 I Page 1 of 1 Prep Method EPA 200 .7 2 w 00 fll!I 21 of 193 13ACCUTEST. J131 ',. • · ,. '., ., · Accutest LabLink @09:06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID : Wl4 Lab Sample ID : 1131 -9 Date Sampled : 05 /26 /05 Matrix : AQ -Ground Water Date Received : 05 /27 /05 Method : EPA 624 Percent Solids: n/a Project : Demo Site File ID DF Analyzed By Prep Date Prep Batch Analy tical Batch Run #1 096992.D 1 06 /06 /05 SWD n/a n/a V04368 Run #2 096972 .D 5 06 /05 /05 SWD n/a n/a V04367 IRun •1 Purge Volume 5 .0 ml 5.0 ml Run #2 Purgeable Aromatics , MTBE , TBA , Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene 78.2 1.0 0 .33 ug/1 108-88-3 Toluene 2.0 1.0 0 .11 ug/1 100 -41-4 Ethylbenzene 5.2 1.0 0 .22 ug/1 1330-20 -7 Xy lenes (total) 2.2 1.0 0 .26 ug/1 1634-04-4 Methyl Tert Butyl Ether 1673 5 .0 2 .1 ug /1 75 -65-0 Tertiary Butyl Alcohol ND 25 10 ug /1 91-20-3 Naphthalene ND 2.0 0.69 ug /1 CAS No . Surrogate Recoveries Run# 1 Run# 2 Limits 17060 -07-0 l ,2-Dichloroethane-D4 (SUR) 111 % 100 % 63-136 % 2037-26 -5 Toluene-DB (SUR) 107 % 102 % 90-110 % 460 -00 -4 4-Bromofluorobenzene (SUR) 104 % 86 % 80-115 % (a) Result is from Run # 2 ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ~l!'j 22 of 193 [ilACCU I ES I. J131 • ·" · •' ., "' Accutest LabLink @09 :06 14-Mar-2006 Client Sample ID: Wl4 Lab Sample ID: J131-9 Matrix : AQ -Ground Water Project : Demo Site Report of Analysis Date Sampled: 05/26 /05 Date Received: 05/27 /05 Percent Solids: n/a Metals Analysis Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead <3 .0 (1) Instrument QC Batch: MA15863 (2) Prep QC Batch : MP30351 RL = Reporting Limit ug /1 06/13/05 06/16/05 KL EPA 200 . 7 I Page 1 of 1 Prep Method EPA 200.7 2 111!1 23 of 193 l3ACCU I ESt. J131 • ,. "·'' ., ...• • Raw Data: K•UtiU!•M Accutest LabLink@09 :06 14-Mar-2006 Rep ort of Analysis Page 1 of 1 Client Sample ID: W17 Lab Sample ID : J131-10 Date Sampled: 05/26 /05 Matrix : AQ -Ground Water Date Received : 05/27 /05 Method: EPA 624 Percent Solids: n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096973 .D 1 06 /05 /05 SWD n/a n/a V04367 Run #2 IRun '1 Purge Volume 5.0 ml Run #2 Purgeable Aromatics , MTBE, TBA , Naphthalene CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 0 .33 ug/1 108-88-3 Toluene ND 1.0 0 .11 ug/1 100-41-4 Ethyl benzene ND 1.0 0.22 ug/1 1330-20-7 Xylenes (total) ND 1.0 0.26 ug/1 1634-04-4 Methyl Teri Butyl Ether 1.8 1.0 0.41 ug/1 75-65-0 Tertiary Butyl Alcohol ND 25 10 ug/1 91-20-3 Naphthalene ND 2 .0 0 .69 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 17060 -07-0 l ,2-Dichloroethane-D4 (SUR) 101 % 63-136 % 2037-26-5 Toluene-OS (SUR) 101 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 83% 80-115 % ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound IJl!i 24 of 193 l:iACCUTEST. J131 "' ,. ' " ') '" Accutest LabLink @09 :06 14-Mar-2006 Client Sample ID: Wl 7 Lab Sample ID : J131-10 Matrix : AQ -Ground Water Project : Demo Site Report of Analysis Date Sampled : 05 /26 /05 Date Received: 05 /27 /05 Percent Solids: n/a Metals Analysis Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead <3.0 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch: MP30351 RL = Reporting Limit ug /1 06/13 /05 06/16 /05 KL EPA 200 .7 I Page 1 of 1 Prep Method EPA 200 .7 2 ial!I 25 of 193 1'3ACCU 11:::S I. J 131 ,,.,., .. ,., ,,, Raw Data: M•UPfZ!•M Accutest LabLink@09:06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID: W6 Lab Sample ID : 1131-11 Date Sampled: 05/26 /05 Matrix: AQ -Ground Water Date Received : 05 /27 /05 Method: EPA 624 Percent Solids: n/a Project : Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096974 .D 20 06 /05 /05 SWD n/a n/a V04367 Run #2 IRuu #I Purge Volume 5 .0 ml Run #2 Purgeable Aromatics, MTBE , TBA, Naphthalene CAS No . Compound Result RL MDL Units Q 71-43-2 Benzene 2180 20 6.5 ug/1 108 -88-3 Toluene 426 20 2.1 ug/1 100-41 -4 Ethylbenzene 1370 20 4.4 ug/1 1330-20 -7 Xylenes (total) 1680 20 5.1 ug/1 1634-04-4 Methyl Tert Butyl Ether 251 20 8.3 ug/1 75 -65-0 Tertiary Butyl Alcohol ND 500 200 ug /1 91-20-3 Naphthalene 323 40 14 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1 , 2-Dichloroethane-D4 (SUR) 103 % 63-136 % 2037-26 -5 Toluene-D8 (SUR) 103 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 94% 80-115 % ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound 1)1!1 26 of 193 lil3ACCU1ES I. J131 ',. ,. ''' ., ,, ' Accutest LabLink @09 :06 14-Mar-2006 Client Sample ID : W6 Lab Sample ID : J131-ll Matrix: AQ -Ground Water Project: Demo Site Report of Analysis Date Sampled: 05 /26 /05 Date Received : 05 /27 /05 Percent Solids: n/a Metals Analy sis Analyte Result RL 3.0 Units OF Prep Analyzed By Method Lead 6.7 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch: MP30351 RL = Reporting Limit ug/1 06/13 /05 06/16/05 KL EPA 200.7 I Page 1 of 1 Prep Method EPA 200 .7 2 fll!t 27 of 193 l;iACCU I ES I. J1 31 I I'; , (< 1 ') •) t Raw Data: M•UPUJ•M Accutest LabLink @09 :06 14-Mar-2006 Report of Analysis Page 1 of 1 Client Sample ID: FB Lab Sample ID : J131-12 Date Sampled : 05/26/05 Matrix: AQ -Field Blank Water Date Received : 05/27/05 Method : EPA 624 Percent Solids: n/a Project: Demo Site File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 096975.D 1 06 /05 /05 SWD n/a n/a V04367 Run #2 IRua #I Purge Volume 5.0 ml Run #2 Purgeable Aromatics, MTBE , TBA, Naphthalene CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 1.0 0 .33 ug/1 108-88-3 Toluene ND 1.0 0.11 ug/1 100-41-4 Ethylbenzene ND 1.0 0.22 ug/1 1330-20-7 Xylenes (total) ND 1.0 0.26 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.41 ug/1 75-65-0 Tertiary Butyl Alcohol ND 25 10 ug/1 91-20-3 Naphthalene ND 2.0 0.69 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 l ,2-Dichloroethane-D4 (SUR) 102% 63-136 % 2037-26-5 Toluene-D8 (SUR) 101 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 84% 80-115% ND = Not detected MDL -Method Detection Limit J = Indicates an estimated value RL = Reporting Limit E = Indicates value exceeds calibration range B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound ffill(!j 28 of 193 gACCUIESJ. J 131 ',."' •. '., "' Accutest LabLink @09:06 14-Mar-2006 Client Sample ID: FB Lab Sample ID : ]131-12 Matrix : AQ -Field Blank Water Project: Demo Site Report of Analysis Date Sampled : 05/26 /05 Date Received : 05/27 /05 Percent Solids : n/a Metals Analys is Analyte Result RL 3 .0 Units DF Prep Analyzed By Method Lead < 3 .0 (1) Instrument QC Batch : MA15863 (2) Prep QC Batch : MP30351 RL = Reporting Limit ug /1 06 /13 /05 06/16 /05 KL EPA 200 .7 I Page 1 of 1 Prep Method EPA 200 .7 2 111!1 29 of 193 ~ACCUTEST. J131 ' •. "' ,, ' ., ,. ,, ' ii)t!j New Jersey l3A~JJ::::~ 0 Misc. Forms Custody Documents and Other Forms Includes the following where applicable : • Ch ain of Custody • Sampl e Tracking Chronicle • Int ern al Chain of Custody Section 4 a •n 30 of 193 IIACCUIESI. J131 ' !' " " ' ., '" CHAIN OF CUSTODY 223 5 Route 130 Da yton NJ OKKIO lil!.i CiACCUTES'T: 732-329-0 200 FAX : 732 -329-H99/)4KO FED-E:X Tr.1cking II l ?l /) n r ,I I C, I'! e :;, ~uen t-<eoo mna n orma 1or _...;mpanyName DEMO Addreu 123-4 Mialn St. ICIiy Slate "• Pro ect n ormat,on Project Name: Street ICIiy state 0 w ~ ~ 0 0 ~ ~ oi o ANYTOWN USA ..,. -J D ~.-~~,~ci~C~~~ .. ~ct-,~~~~~~~~~~~-.-~-,-,,~~~~.-,o-j~-,-.~~~~~~~~~~~~~~~~---<~i ~~ ~.-00-.-.• ~~~~~~~~~~~~~~~~~~-+-,-.,-.~~~~~~~~~~~~~~~~~---,E ~ ~~ 00 D u o ~.-,m-.-,,-.,-.,-.-,=~~~~~~~~~~~~~~~~-+c-11,-.-,.-.-"-.,-,-,o-,-.,-,-.~~~~~~~~~~~~-1~~ ~ 0 - 0 • ~~ MIA-,~-u-,e-.-,~~~~~~~~~~~~.-u-M-~--,~~~~~~,o-1-1e-c1-10-n~~~~~~~N-u-m~b-er-o~,o,-es-e-N-e~d~tl,ot~t1,-,---<o o ~~ D o Sa mple # Field ID / Point of Collection MECH Vial Date Time Sampled b Matrix ~n7!, g i j i ~ j © ~ ~ ~ ~ ~ Th is chain of custody is for demonstration purposes only. Turnaround Time ( Business da s) CL] Std.15 Bus iness Dillys ~ 10DayRUSH ~ 5DayRUSH C=::J 3 Day EMERGENCY C:J 2 Day EMERGENCY [===i 1 Day EMERGENCY [===i oth.r ApproVfl!By;/Oillte Em ergen cy TIA data available VIA Lablink Data Delivef able lnfOJmation (]] Commerclal"A"' D Commerclilll "B" D NJ Red uced O NJFull O o1her __ _ D FULLCLP D NYASP Category A D NY ASP Category B O stateForms D EDD Format __ _ Commercial ""A""• Results Only I Sample Custod y must be d ocumented below each lime samples change possession, inc l udlng courier delive ry . 1/:Cl!IVl!lltly: 11nqu1,,. ...... y uate 1me: , .... ,,I/; m q u lf 1/:u y K l/; 1r,qu .... ~u y eCl!IVl!Ol:ly: u t. ...... y eat• r re1erv 10M1ere1pp1cao11 D 8 otUeOfderCoritrolll Accut,ulJob# Keauestea na1v s1s Comments I Remarks e<:e1veo1:1y: Kel\'ecl tly: 1Ma n x \..Ooes r:>N-Or~Wattl GW-Gn;,und w.1 .. w.N-Water SW-Su rfKe Water SO-Soi SL..Studpa OI-Oit UO-Othe1Uquid AIR-Ar S01..Qtlw1 S0W V,,,,-Wipe LAB USE ONLY vr, u 1.-0011' t mp . D Jl 31 : Chain of Custody Page 1 of 1 I 111!1 31 of 193 l3ACCU I ES r. J131 """ <· ' ., Accutest Laboratories Internal Sample Tracking Chronicle Demo Account Job No : Demo Site Project No: P0#4506358942 WBS#08 Sample Number Method Analyzed By Prepped By Test Codes J131-1 ElO J131-1 J131-1 J131-1 J131-2 E14 J131-2 J131-2 J131-3 ESR J131-3 J131-3 J131-4 PIO J131-4 J131-4 J131-4 J131-5 PUA J131-5 J131-5 1131-6 P14 J131-6 Jl 31-6 Collected : 26-MAY-05 14:30 By: BB Received : 27-MAY-05 By: CJP EPA 624 EPA 624 EPA 200 .7 05-JUN-05 03 :08 SWD V624BTXMTN 05-JUN-05 03 :35 SWD V624BTXMTN 15-JUN-05 05 :01 JDM 13-JUN-05 JDM PB Collected: 26 -MAY-05 15 :45 By: BB Received: 27-MAY-05 By: CJP EPA 624 EPA 200.7 04-JUN-05 22 :09 SWD V624BTXMTN 16-JUN-05 16:28 KL 13-JUN-05 JDM PB Collected: 26-MAY-05 13 :55 By : BB Received: 27-MAY-05 By: CJP EPA 624 EPA 200 .7 04-JUN-05 22 :36 SWD V624BTXMTN 16-JUN-05 16 :34 KL 13-JUN-05 JDM PB Collected: 26 -MAY-05 15 :20 By: JA Received: 27-MAY-05 By: CJP EPA 624 EPA 624 EPA 200 .7 05-JUN-05 00 :26 SWD 05 -JUN-05 00:53 SWD 16-JUN-05 16 :39 KL V624BTXMTN V624BTXMTN 13-JUN-05 JDM PB Collected: 26-MAY-05 14:20 By : JA Received : 27-MAY-05 By : CJP EPA 624 EPA 200.7 06-JUN-05 16 :22 SWD V624BTXMTN 16-JUN-05 16:45 KL 13-JUN-05 JDM PB Collected: 26-MAY-05 13 :50 By: JA Received: 27-MAY-05 By: CJP EPA 624 EPA 200.7 06-JUN-05 16 :50 SWD V624BTXMTN 16-JUN-05 16 :50 KL 13-JUN-05 JDM PB Page 1 of 2 j131 I fll!j 32 of 193 l3ACCU I ES I. J131 t :· :•' « 1 '} ". Accutest Laboratories Internal Sample Tracking Chronicle Demo Account Job No: Demo Site Project No: P0#4506358942 WBS#08 Sample Number Method Analyzed By Prepped By Test Codes ]131-7 P6 ]131-7 ]131-7 ]131-7 ]131-8 P7 ]131-8 ]131-8 ]131-9 Wl4 ]131-9 ]131-9 ]131-9 ]131-10 W17 Collected: 26-MA Y-05 13 :25 By: BB Received: 27-MAY-05 By: CJP EPA 624 EPA 624 EPA 200.7 05-JUN-05 02:14 SWD 05-JUN-05 02:41 SWD 16-JUN-05 16:56 KL V624BTXMTN V624BTXMTN 13-JUN-05 JDM PB Collected : 26-MAY-05 15: 10 By: BB Received: 27-MAY-05 By: CJP EPA 624 EPA 200.7 05-JUN-05 05:23 SWD 16-JUN-05 17:01 KL V624BTXMTN 13-JUN-05 JDM PB Collected : 26-MAY-05 13:15 By: JA Received: 27-MAY-05 By: CJP EPA 624 EPA 624 EPA 200.7 05-JUN-05 05:50 SWD 06-JUN-05 17:17 SWD 16-JUN-05 17:07 KL V624BTXMTN V624BTXMTN 13-JUN-05 JDM PB Collected: 26-MA Y-05 15:50 By: JA Received: 27-MAY-05 By: CJP ]131-10 EPA 624 05-JUN-05 06:18 SWD V624BTXMTN ]131-10 EPA 200 .7 16-JUN-05 17:22 KL 13-JUN-05 JDM PB ]131-11 W6 Collected: 26-MAY-05 14:50 By: JA Received: 27-MA Y-05 By: CJP ]131-11 ]131-11 EPA 624 EPA 200.7 05-JUN-05 06:45 SWD 16-JUN-05 17:28 KL V624BTXMTN 13-JUN-05 JDM PB ]131-12 FB Collected: 26-MAY-05 15:40 By : BB Received: 27 -MAY-05 By: CJP ]131 -12 EPA 624 05-JUN-05 07:11 SWD V624BTXMTN ]131-12 EPA 200 .7 16-JUN -05 17:33 KL 13-JUN-05 JDM PB Page 2 of 2 J131 I ffill!j 33 of 193 ;iACCUTES r. J131 t :! :~ ( " 1 ') ,: 1 Accutest Internal Chain of Custody Job Number: J131 Account: DEMO Demo Account Project : Demo Site Received : 05/27 /05 Sample .Bottle Transfer Transfer Number FROM TO J131-1.1 Secured Storage Todd Shoemaker J131-1.1 Todd Shoemaker Julie Hong J131-1.1 Julie Hong Secured Storage Jl31-1.1 Secured Storage Dave Hunkele J131-l.l Dave Hunkele Michael Wassef J131-1.1 Michael Wassef Joan D. McCormack J131-1.1 Joan D . McCormack Secured Storage J131-1.l Dave Hunkele J131-1.l. l Joan D . McCormack Metals Digestion J131-l.l.l Metals Digestion Michael Wassef J131-1.l .l Micha el Wassef Metals Digestate Storage J131-l.l.l Metals Digestate Storage Jl31-l.l.2 Joan D. McCormack Metals Digestion J131-1.1 .2 Metals Digestion Michael Wassef J131-l. l.2 Michael Wassef Metals Digestate Storage ]131-1.1.2 Metals Digestate Storage Kathy Lukenda J131-1.l.2 Kathy Lukenda Metals Digestate Storage ]131-1.1.2 Metals Digestate Storage Kathy Lukenda J131-l.l.2 Kathy Lukenda Metals Digestate Storage J131-l.l.2 Metals Digestate Storage Kathy Lukenda ]131-1.1.2 Kathy Lukenda Metals Digestate Storage J131-l.l.2 Metals Digestate Storage J131-l.2 Secured Storage Saraswathi Doddi J131-l.2 Saraswathi Doddi VOA Prep Storage J131-l.2 VOA Prep Storage Sarah A . Chin J131-l .2 Sarah A . Chin GCMSO J131-l .2 GCMSO Saraswathi Doddi J131-l.2 Saraswathi Doddi Secured Storage J131-l.2 Dave Hunkele J131-1.3 Secured Storage Saraswathi Doddi J131-l.3 Saraswathi Doddi Secured Storage ]131-1.3 Dave Hunkele ]131-2 .1 Secured Storage Todd Shoemaker J131-2 .l Todd Shoemaker Julie Hong J131-2.l Julie Hong Secured Storage ]131-2.1 Secured Storage Dave Hunkele J131-2 .l Dave Hunkele Michael Wassef J131-2 .l Michael Wassef Joan D . McCormack ]131-2 .1 Joan D . McCormack Secured Storage Date/Time 06 /10/05 08 :07 06 /10/05 08 :08 06/10/05 12 :15 06 /13 /05 08:20 06/13/05 08:21 06 /13/05 08:45 06 /13/05 09:57 07 /15 /05 06:00 06 /13 /05 09 :26 06 /14/05 10:55 06 /14 /05 10 :55 08/22/05 09 :00 06 /13 /05 09:56 06 /13 /05 13 :25 06 /13 /05 13 :25 06 /14 /05 22 :03 06 /15 /05 00 :51 06 /15 /05 15 :25 06/16/05 00 :13 06 /16/05 17:05 06 /17/05 01:12 08/22 /05 09:00 06 /03 /05 16:41 06 /03 /05 16:41 06 /04 /05 08: 50 06 /04/05 08: 51 06 /06 /05 08 : 1 7 06 /06 /05 08 : 17 07 /15 /05 06 :00 06 /02/05 13 : 58 06 /02/05 17 : 19 07 /15 /05 06 : 00 06 /10/05 08 :07 06/10 /05 08 :08 06 /10 /05 12:15 06 /13 /05 08 :20 06 /13 /05 08:21 06 /13 /05 08:45 06 /13 /05 09:57 Page 1 of 9 ~ <,.l Reason II Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Di gestate from Jl 31-1.1 Digestate from J 131-1.1 Return to Storage Disposed Digestate from J131-l.l Digestate from J 131-1.1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Retrieve from Storage Load on Instrument Unload from Instrument Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage 11!1 34 of 193 gjACCUTEST. J131 ~:•:•!,.I ')'~' Accutest Internal Chain of Custody Job Number: J131 Ac count : DEMO Demo Account Project: Demo Site Received : 05 /2 7/05 Sample.Bottle Transfer Transfer Number FROM TO ]131-2 .1 Dave Hunkele J131-2 .l.l Joan D . McCormack Metals Digestion ]131-2 .1.1 Metals Digestion Michael Wassef J131-2 .l.l Michael Wassef Metals Digestate Storage J131-2.1.1 Metals Digestate Storage J131-2 .1.2 Joan D . McCormack Metals Digestion J131-2.1.2 Metals Digestion Michael Wassef J131 -2.1.2 Michael Wassef Metals Digestate Storage J131-2 .1.2 Metals Digestate Storage Kathy Lukenda ]131-2 .1.2 Kathy Lukenda Metals Digestate Storage J131-2 .1.2 Metals Digestate Storage Kathy Lukenda J131-2.1.2 Kathy Lukenda Metals Digestate Storage ]131-2 .1.2 Metals Digestate Storage Kathy Lukenda ]131-2 .1.2 Kath y Lukenda Metals Digestate Storage J131-2.1.2 Metals Digestate Storage J131 -2.2 Secured Storage Saraswathi Doddi J131-2 .2 Saraswathi Doddi Secured Storage J131-2.2 Dave Hunkele J131-3 .1 Secured Storage Todd Shoemaker J131-3 .1 Todd Shoemaker Julie Hong ]131-3 .1 J ulie Hong Secured Storage ]131-3 .1 Secured Storage Dave Hunkele J131-3 . l Dave Hunkele Michael Wassef J131-3 .1 Michael Wassef Joan D. McCormack J131-3 .1 Joan D . McCormack Secured Storage ]131-3 .1 Dave Hunkele J131-3 .1.1 Joan D . McCormack Metals Digestion J131-3 .1.1 Meta ls Digestion Michae l Wassef ]131-3 .1.1 Michael Wassef Meta ls Digestate Storage J131-3 .1.1 Meta ls Digestate Storage J131-3.1.2 Joan D . McCormack Meta ls Digestion J131-3 .1.2 Meta ls Digestion Michae l Wassef J131-3 . l .2 Michael Wassef Metals Digestate Storage J131-3 .1.2 Metals Digestate Storage Kathy Lukenda J131 -3.1.2 Kathy Lukenda Metals Digesta te Storage J131 -3 .1.2 Metals Digestate Storage Kathy Lukenda J131-3 .1.2 Kathy Lukenda Meta ls Digestate Storage J131 -3 .l.2 Metals Digestate Storage Kat hy L ukenda Date/Time 07 /15 /05 06 :00 06 /13 /05 09 :26 06/14 /05 10 :55 06 /14 /05 10 :55 08 /22/05 09 :00 06 /13 /05 09 :56 06 /13 /05 13 :25 06 /13 /05 13:25 06 /14 /05 22 :03 06 /15 /05 00 :51 06 /15 /05 15 :25 06 /16 /05 00 :13 06 /16 /05 17:05 06 /17 /05 01:12 08/22 /05 09 :00 06 /02 /05 13:58 06 /02/05 17:19 07 /15 /05 06:00 06 /10 /05 08:07 06 /10 /05 08:08 06 /10/05 12: 15 06 /13 /05 08:20 06 /13/05 08:21 06/13/05 08 :45 06 /13/05 09:57 07 /15/05 06:00 06 /13 /05 09 :26 06 /14 /05 10:55 06 /14 /05 10:55 08/22/05 09:00 06 /13 /05 09 :56 06 /13 /05 13 :25 06 /13 /05 13 :25 06 /14 /05 22:03 06 /15/05 00:51 06 /15 /05 15 :25 06 /16/05 00 :13 06 /16 /05 17:05 Page 2 of 9 !>- (,J Reason I Disposed Digestate from J131-2 .l Digestate from J131-2 .1 Return to Storage Disposed Digestate from J131-2 .l Di gestate from J 131-2 .1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J 131-3 .1 Digestate from J131-3.1 Return to Storage Disposed Digestate from J131-3 .1 Digestate from Jl 31-3 .1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage lll!i 35 of 193 (jACCUTEST. J131 . i :·::, "'1 ') •: • Accutest Internal Chain of Custody Job Number: J131 Account : DEMO Demo Account Project : Demo Site Received: 05/27 /05 Sample.Bottle Transfer Transfer Number FROM TO J131-3 .l.2 Kathy Lukenda Metals Digestate Storage ]131-3 .1.2 Metals Digestate Storage J131-3 .2 Sec ured Storage Saraswathi Doddi J131-3 .2 Saraswathi Doddi VOA Prep Storage J131-3.2 VOA Prep Storage Sarah A. Chin J131-3 .2 Sarah A. Chin GCMSO J131-3 .2 GCMSO Saraswathi Doddi J131-3 .2 Saraswathi Doddi Secured Storage J131-3 .2 Dave Hunkele ]131-4 .1 Secured Storage Todd Shoemaker ]131-4.1 Todd Shoemaker Julie Hong J131-4. l Julie Hong Secured Storage J131-4 . l Secur ed Storage Dave Hunkele J131-4 . l Dave Hunkele Michael Wassef ]131-4 .1 Michael Wassef Joan D . McCormack J131-4 .l Joan D . McCormack Secured Storage J131-4 .1 Dave Hunkele J131-4 .l.1 Jo an D . McCormack Metals Digestion J131-4 .l.1 Metals Digestion Michael Wass ef ]131-4 .1.1 Michael Wassef Metals Digestate Storage J131 -4 .l.1 Metals Digestate Storage Jl 31-4 .1. 2 Joan D. McCormack Metals Digestion J131-4 .l.2 Metals Digestion Michael Wassef J131-4 .l.2 Michael Wassef Metals Digestate Storage J131-4 .1.2 Metals Digestate Storage Kathy Lukenda J131-4 .1.2 Kathy Lukenda Metals Digestate Storage Jl31-4 .l.2 Metals Digestate Storage Kathy Lukenda J131-4 .1.2 Kath y Lukenda Metals Digestate Storage ]131-4 .1.2 Metals Digestate Storage Kathy Lukenda J131-4 .l.2 Kath y Lukenda Metals Digestate Storage ]131-4 .1.2 Metals Digestate Storage J131-4 .2 Secured Storage Saraswathi Doddi J131-4 .2 Saraswathi Doddi Secured Storage J131 -4 .2 Dav e Hunkele J131-5 .1 Secured Storage Todd Shoemaker J131-5 .1 Todd Shoemaker Juli e Hong J131-5.1 Julie Hong Secured Storage ]131-5 .1 Secured Storag e Dave Hunkele Date/Time 06 /17 /05 01 : 12 08 /22 /05 09 :00 06 /02/05 13 :55 06 /02/05 13 :55 06 /04 /05 08 :53 06 /04 /05 08:53 06 /06 /05 08: 17 06 /06 /05 08: 17 07 /15 /05 06:00 06 /10/05 08 :07 06 /10/05 08:08 06 /10/05 12 :15 06 /13 /05 08 :20 06/13 /05 08 :21 06 /13 /05 08:45 06 /13 /05 09:57 07 /15 /05 06 :00 06 /13 /05 09:26 06 /14 /05 10 :55 06 /14 /05 10 :55 08 /22 /05 09 :00 06 /13 /05 09 :56 06 /13 /05 13 :25 06 /13 /05 13 :25 06 /14 /05 22 :03 06 /15 /05 00:51 06 /15 /05 15 : 25 06 /16/05 00 : 13 06 /16/05 17 :05 06 /17 /05 01 : 12 08 /22/05 09 :00 06 /02/05 13 :58 06 /02/05 17 : 19 07 /15 /05 06 :00 06 /10 /05 08 :07 06 /10/05 08 :08 06 /10/05 12 :15 06 /13 /05 08 :20 Page 3 of 9 ~ (,J Reason I Return to Storage Disposed Retrieve from Storage Return to Storage Retrieve from Storage Load on Instrument Unload from Instrument Return to Storage Disposed Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J 131-4 .1 Digestate from J 131 -4 .1 Return to Storage Disposed Digestate from J131-4 .l Digestate from J 131-4 .1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage lll!i 36 of 193 [dACCU I ES I. J131 l :-;i / "1 ') •:. Accutest Internal Chain of Custody Job Number: J131 Account: DEMO Demo Account Project : Demo Site Received : 05/27 /05 Sample .Bottle Transfer Transfer Number FROM TO ]131-5 .1 Dave Hunkele Michael Wassef J131-5.l Michael Wassef Joan D. McCormack J131-5 .1 Joan D. McCormack Secured Storage J131-5 .1 Dave Hunkele ]131-5 .1.1 Joan D . McCormack Metals Digestion J131-5.l.1 Metals Digestion Michael Wassef J131-5 .l.1 Michael Wassef Metals Digestate Storage J131-5 .l.1 Metals Digestate Storage J131-5 .1.2 Joan D. McCormack Metals Digestion ]131-5 .1.2 Metals Digestion Michael Wassef J 131-5 .1. 2 Michael Wassef Metals Digestate Storage J131-5.1.2 Metals Digestate Storage Kathy Lukenda J131-5 .1.2 Kathy Lukenda Metals Digestate Storage J131-5.1.2 Metals Digestate Storage Kathy Lukenda J131-5 .1.2 Kathy Lukenda Metals Digestate Storage J131-5.1.2 Metals Digestate Storage Kathy Lukenda ]131-5.1.2 Kathy Lukenda Metals Digestate Storage J131-5 .1.2 Metals Digestate Storage J131-5.2 Secured Storage Saraswathi Doddi J131-5.2 Saraswathi Doddi Secured Storage J131 -5.2 Dave Hunkele J131-5.3 Secured Storage Saraswathi Doddi J131-5.3 Saraswathi Doddi Secured Storage J131-5 .3 Dave Hunkele J131-6 .1 Secured Storage Todd Shoemaker J131-6 .1 Todd Shoemaker Julie Hong ]131-6 .1 Julie Hong Secured Storage J131-6.1 Secured Storage Dave Hunkele J131-6.1 Dave Hunkele Michael Wassef J131-6 .1 Michael Wassef Joan D . McCormack J131-6 .1 Joan D . McCormack Secured Storage J131-6 .1 Dave Hunkele ]131 -6 .1.1 Joan D . McCormack Metals Digestion ]131-6.1.1 Metals Digestion Michael Wassef J131 -6 .l.1 Michael Wassef Metals Digestate Storage J131-6 .l.1 Metals Digestate Storage J131-6.1.2 Joan D . McCormack Metals Digestion Date/Time 06 /13 /05 08:21 06/13 /05 08:45 06/13 /05 09 :57 07/15 /05 06 :00 06 /13 /05 09:26 06 /14 /05 10:55 06 /14 /05 10:55 08/22/05 09 :00 06/13 /05 09:56 06 /13 /05 13 : 25 06 /13 /05 13:25 06 /14 /05 22:03 06 /15 /05 00 :51 06 /15 /05 15: 25 06/16 /05 00:13 06 /16 /05 17 :05 06 /17 /05 01:12 08/22 /05 09:00 06 /02/05 13 :58 06 /02/05 17: 19 07 /15 /05 06:00 06 /06/05 11 : 17 06 /06 /05 15: 14 07 /15 /05 06:00 06/10 /05 08 :07 06 /10/05 08:08 06 /10/05 12: 15 06 /13 /05 08 : 20 06 /13 /05 08:21 06 /13 /05 08 :45 06 /13/05 09:57 07 /15/05 06 :00 06 /13 /05 09:26 06 /14 /05 10:55 06 /14 /05 10 :55 08/22 /05 09:00 06 /13 /05 09:56 Page 4 of 9 ~ (,J Reason I Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J 131-5 .1 Digestate from ]131-5 .1 Return to Storage Disposed Digestate from J 131 -5 .1 Digestate from J131-5 .1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J 131-6 .1 Digestate from Jl 31-6 .1 Return to Storag e Disposed Digestate from J 131-6 .1 111!:1 37 of 193 l3ACCU I ES I. J131 i :• :i, "1 ') ,i i Accutest Internal Chain of Custody Job Number: J131 Account: DEMO Demo Account Project: Demo Site Received: 05 /27 /05 Sample . Bottle Transfer Transfer Number FROM TO J131-6 .1.2 Metals Digestion Michael Wassef J131-6 .1.2 Michael Wa ssef Metals Digestate Storage J131-6.1.2 Metals Digestate Storage Kathy Lukenda J131-6 .1.2 Kathy Lukenda Metals Digestate Storage ]131-6 .1.2 Metals Digestate Storage Kathy Lukenda ]131-6 .1.2 Kathy Lukenda Metals Digestate Storage J131-6 .1.2 Metals Digestate Storage Kathy Lukenda J131 -6.1.2 Kathy Lukenda Metals Digestate Storage J131-6.1.2 Metals Digestate Storage ]131-6 .2 Secured Storage Saraswathi Doddi ]131-6 .2 Saraswathi Doddi Secured Storage J131-6 .2 Dave Hunkele J131-6.3 Secured Storage Saraswathi Doddi J131-6 .3 Saraswathi Doddi Secured Storage J131 -6 .3 Dave Hunkele J131-7 .l Secured Storage Todd Shoemaker J131-7 .1 Todd Shoem aker Julie Hong J131-7.1 Julie Hong Secured Storage J131-7 .1 Secured Storage Dave Hunkele ]131-7 .1 Dave Hunkele Michael Wassef J131 -7 .1 Michae l Wassef Joan D. McCormack ]131-7 .1 Joa n D . McCormack Secured Storage ]131 -7 .1 Dave Hunkele J131-7 .1.1 Joan D . McCormack Metals Digestion J131-7 .1.1 Meta ls Digestion Michael Wassef J131-7 .1.1 Michael Wassef Metals Digestate Storage J131-7.1.1 Metals Diges tate Storage J131-7 .1.2 Joan D . McCormack Metals Digestion J131-7.1.2 Metals Digestion Michael Wassef J131 -7 .1.2 Michael Wassef Metals Digestate Storage J131-7 .1.2 Metals Digestate Storage Kathy Lukenda ]131 -7 .1.2 Kathy Lukenda Metals Digestate Storage J131-7 .1.2 Metals Digestate Storage Kathy Lukenda J131-7 .1.2 Kathy Lukenda Metals Digestate Storage J131 -7 .1.2 Meta ls Digestate Storage Kathy Lukenda J131-7 .1.2 Kath y Lukenda Metals Digestate Storage ]131-7 .1.2 Metals Digestate Storage J131 -7 .2 Secured Storage Saraswathi Doddi Date /Time 06 /13 /05 13:25 06 /13 /05 13:25 06 /14 /05 22 :03 06 /15 /05 00: 51 06 /15 /05 15: 25 06 /16 /05 00:13 06 /16 /05 17 :05 06 /17 /05 01:12 08 /22/05 09 :00 06 /02 /05 13 :58 06 /02 /05 17 : 19 07 /15 /05 06 :00 06 /06 /05 11: 17 06 /06 /05 15: 14 07 /15 /05 06:00 06 /10/05 08:07 06 /10/05 08:08 06 /10/05 12 : 15 06 /13 /05 08 :20 06 /13 /05 08:21 06 /13 /05 08 :45 06 /13 /05 09 :57 07 /15 /05 06 :00 06 /13 /05 09 :26 06 /14 /05 10:55 06 /14/05 10 :55 08/22 /05 09:00 06 /13 /05 09 :56 06 /13 /05 13 :25 06 /13 /05 13:25 06 /14 /05 22:03 06 /15 /05 00:51 06 /15 /05 15:25 06 /16 /05 00 :13 06 /16 /05 17 : 05 06 /17 /05 01 : 12 08 /22/05 09 :00 06 /02/05 13 : 58 Page 5 of 9 ,fl>, (,J Reason a Digestate from J131-6 .1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retri eve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Custod y Transfer Return to Storage Retri eve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Dige state from J 13 1-7 .1 Digestate from J 131-7 .1 Return to Storage Disposed Digestate from J 131 -7 .1 Digestate from J 131-7 .1 Return to Storage Retriev e from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage gl!I 38 of 193 ;iACCUTEST. J131 • •. "•, t ., ., • Accutest Internal Chain of Custody Job Number : J131 Account : DEMO Demo Account Project : Demo Site Received: 05 /2 7/05 Sample. Bottle Transfer Transfer Number FROM TO J131-7 .2 Saraswathi Doddi Secured Storage J131-7 .2 Dave Hunkele J131-8 .1 Secured Storage Todd Shoemaker J131-8 .l Todd Shoemaker Julie Hong J131-8 .1 Julie Hong Secured Storage ]131-8 .1 Secured Storage Dave Hunkele J131-8 .1 Dave Hunke le Michael Wassef J13 1-8 .1 Michael Wassef Joan D . McCormack J13 1-8 .1 Joan D. McCormack Secured Storage ]131-8 .1 Dave Hunkele ]131-8 .1.1 Joan D. McCormack Metals Digestion J131-8 .1.1 Meta ls Digestion Michael Wassef J131-8 .1.1 Michael Wassef Metals Digestate Storage ]131-8 .1.1 Metals Digestate Storage J131-8.1.2 Joan D . McCormack Metals Digestion J131-8 .1.2 Metals Digestion Michael Wassef J131-8.1.2 Michael Wassef Metals Digestate Storage J131-8 .1.2 Metals Digestate Storage Kathy Lukenda J131-8 .1.2 Kath y Lukenda Metals Digestate Storage J131-8 .1.2 Metals Digestate Storage Kathy Lukenda J131-8 .1.2 Kathy Lukenda Metals Digestate Storage J131-8 .1.2 Metals Digestate Storage Kathy Lukenda J131-8 .1.2 Kathy Lukenda Metals Digestate Storage J131-8.1.2 Metals Digestate Storage J131-8 .3 Se cured Storage Saraswathi Doddi J131-8 .3 Saraswathi Doddi VOA Prep Storage J131-8 .3 VOA Prep Storage Sarah A . Chin J131-8 .3 Sarah A . Chin GCMSO J131-8 .3 GCMSO Saraswathi Doddi J131-8 .3 Saraswathi Doddi Secured Storage J131-8 .3 Dave Hunkele J131 -9.1 Secured Storage Todd Shoemaker J131-9 .1 Todd Shoemaker Julie Hong J131-9 .1 Julie Hong Secured Storage J131-9 .1 Secured Storage Dave Hunkele J131-9 .1 Da ve Hunkele Michael Wassef J131-9 .1 M ichael Wassef Joan D. McCormack J131-9 .1 Joan D. McCormack Secured Storage J131 -9 .1 Dave Hunkele Date /Time 06 /02/05 17: 19 07 /15 /05 06:00 06 /10 /05 08:07 06 /10 /05 08:08 06 /10/05 12 :15 06 /13 /05 08:20 06 /13 /05 08 :21 06 /13 /05 08 :45 06 /13 /05 09 :57 07 /15 /05 06 :00 06 /13 /05 09 :26 06 /14 /05 10 :55 06 /14 /05 10:55 08/22/05 09 :00 06 /13 /05 09 :56 06 /13 /05 13: 25 06 /13 /05 13 :25 06 /14 /05 22 :03 06 /15 /05 00 :51 06 /15 /05 15: 25 06 /16 /05 00:13 06 /16 /05 17:05 06 /17 /05 01 : 12 08/22/05 09 :00 06 /02 /05 13:55 06 /02 /05 13 :55 06 /04 /05 08:53 06 /04 /05 08 :53 06 /06 /05 08 : 17 06 /06 /05 08 : 17 07 /15 /05 06:00 06 /10/05 08:07 06 /10 /05 08:08 06 /10/05 12 :15 06 /13 /05 08 :20 06 /13 /05 08 :21 06 /13 /05 08 :45 06 /13 /05 09:57 07 /15 /05 06:00 Page 6 of 9 ~ <,J Reason I Return to Storage Dispo sed Retriev e from Storage Custody T ransfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J 131-8 .1 Digestate from J 131-8 .1 Return to Storage Disposed Digestate from J131-8 .1 Digestate from J131-8 .1 Return to Sto rage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Retrieve from Storage Load on Instrument Unload from Instrument Return to Storage Disposed Retriev e from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed iial!I 39 of 193 l3ACCUTEST. J131 ' 'CO"'<' '> '' ,. Accutest Internal Chain of Custody J ob Number : J131 Acc ount : DEMO Demo Account Proj ect : Demo Sit e Receiv ed : 05 /27 /05 Sample .Bottle Transfer Transfer Number FROM TO J131-9 . l.1 Joan D . McCormack M etals Digestion J131-9 .1.1 Metals Digestion Michael Wassef J131-9 .1.1 Michael Wassef Metals Digestate Storage J131-9 .1.1 Metals Digestate Storage J131-9 .l.2 Joan D . McCormack Metals Digestion J131-9 .1.2 Metals Digestion Michael Wassef J131-9 . l.2 Michael Wassef Metals Digestate Storage J131-9 .l.2 Metals Digestate Storage Kathy Lukenda J131-9 . l.2 Kathy Lukenda Metals Digestate Storage J131-9 .l.2 Metals Digestate Stor age Kathy Lukenda J131-9 . l.2 Kathy Lukenda Metals Digestate Storage J131-9 .l.2 Metals Digestate Storage Kathy Lukenda J131-9 .1.2 Kath y Lukenda Metals Digestate Storage J131-9 .1.2 Metals Digestate Storage J131-9 .2 Secured Storage Saraswathi Doddi J131-9 .2 Saraswathi Doddi Secured Storage J131-9 .2 Dave Hunkele J131-9 .3 Secured Storage Saraswathi Doddi J131 -9 .3 Saraswathi Doddi GCMSO J131-9 .3 GCMSO Saraswathi Doddi J131-9.3 Saraswathi Doddi Secured Storage J131-9 .3 Dave Hunke le J1 3 1-10 .1 Secured Storage Todd Shoemaker J131-10 .1 Todd Shoemaker Julie Hong J131-10.1 Julie Hong Secured Storage J131-10 .l Secured Storage Dave Hunkele J131-10 .1 Dave Hunkele Michae l Wassef J131-10 .1 Michael Wassef Joan D. McCormack J131-10 .1 J oan D . McCormack Secure d Storage J131-10 .1 Dave Hunkele J131-10 .1.1 Joan D . McCormack Meta ls Digestion ]131-10.1.1 Metals Digestion Michae l Wassef J131 -10.1.1 Michael Wassef Metals Digestate Storage J131 -10 .1.1 Metals Digestate Storage J131-10 .l.2 Joan D . McCormack Meta ls Digestion J131-10 .l.2 Meta ls Digestion Michae l Wassef J131-10 . l.2 Michael Wassef Metals Diges tate Storage Date/Time 06 /13 /05 09 :26 06 /14 /05 10:55 06 /14 /05 10:55 08 /22/05 09 :00 06 /13 /05 09 :56 06 /13 /05 13 : 25 06 /13 /05 13 : 25 06 /14 /05 22 :03 06 /15 /05 00 :51 06 /15 /05 15 : 25 06 /16/05 00 :13 06 /16/05 17 : 05 06 /17 /05 01 : 12 08 /22/05 09 :00 06 /02/05 13 : 58 06 /02/05 1 7 : 19 07 /15 /05 06 :00 06 /06 /05 11 : 16 06 /06 /05 11: 16 06 /07 /05 10 :00 06 /07 /05 10:00 07 /15 /05 06 :00 06 /10/05 08 :07 06 /10/05 08 :08 06 /10 /05 12 :15 06 /13 /05 08:20 06 /13 /05 08:21 06 /13 /05 08:45 06 /13 /05 09:57 07 /15 /05 06: 00 06 /13 /05 09:26 06 /14 /05 10:55 06 /14 /05 10:55 08 /22/05 09:00 06 /13 /05 09 :56 06 /13 /05 13 :25 06 /13 /05 13:25 Page 7 of 9 ~ <,J Reason I Digestate from J131-9 .1 Digestate from J131-9 .1 Return to Storage Disposed Digestate from J131-9 .1 Digestate from J131-9 .1 Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed Retrieve from Storage Load on Instrument Unload from Instrument Return to Storage Disposed Retriev e from Storage Custody Transfer Return to Storage Retriev e from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J131-10.1 Digestate from J 131-10.1 Return to Storage Disposed Digestate from J 131 -10 .1 Digestate from J13 1-10 .1 Return to Storage Ml!i 40 of 193 ;iACCU l"EST. J131 """'"'' ,,, Accutest Internal Chain of Custody Job Number : J131 Account: DEMO Demo Account Project : Demo Site R eceived: 05 /27 /05 Sample.Bottle Transfer Transfer Number FROM TO J131-10.l.2 Metals Digestate Storage Kathy Lukenda J131-10. l.2 Kath y Lukenda Metals Digestate Storage J131-10 .l.2 Metals Digestate Storage Kath y Lukenda J131-10.l.2 Kathy Lukend a Meta ls Digestate Storage J1 3 1-10. l.2 Metals Digestate Storage Kathy Lukenda J131-10 .l.2 Kath y Lukenda Metals Digestate Storage j131 -10 .l.2 Metals Digestate Storage J131 -10 .2 Secured Storage Saraswathi Doddi J131 -10 .2 Saraswathi Doddi VOA Prep Storage J131-10 .2 VOA Prep Storage Sarah A . Chin J131-10 .2 Sara h A. Chin GCMSO Jl31-10.2 GCMSO Saraswathi Doddi J131-10 .2 Saraswathi Doddi Secured Storage J13 1-10 .2 Dav e Hunkele J131-1 l.l Secured Storage Todd Shoemaker J131-1 l.l Todd Shoemaker Julie Hong J131 -l l. l Julie Hong Secured Storage J131-1 l.l Secur ed Storage Dave Hunkele J131-ll .l Dave Hunkele Michael Wassef J131-ll.l Michael Wassef Joan D . McCormack j131 -ll.l Joan D . McCormack Secured Storage J131-ll.l Dave Hunkele J131 -11.l.l Joan D . McCormack Meta ls Digestion j131-11.l.1 Metals Digestion Michael Wassef J131-11. l.1 Michae l Wassef Metals Digestate Storage J131-ll.l .l Meta ls Digestate Storage J131-11.1.2 Joan D . McCormack Metals Digestion J131-11.l.2 Metals Digestion Michae l Wassef J131 -11.l.2 Michae l Wassef Metals Digestate Storage J131-11.l.2 Metals Digestate Storage Kathy L ukenda J131-11.l.2 Kath y Lukenda Metals Digestate Storage J131-ll.l .2 Metals Digestate Storage Kathy Lukenda ]131-11.1 .2 Kathy Lukenda Meta ls Digestate Storage J131-11.1.2 Metals Digestate Storage Kathy Lukenda J131-1 l.l .2 Kath y Lukenda Metals Digestate Storage ]131-11.1.2 Meta ls Digestate Storage Jl31-ll.3 Secured Storage Saraswathi Doddi j131-ll.3 Saraswathi Doddi Secured Storage J131 -ll.3 Dave Hunkele Date/Time 06 /14 /05 22 :03 06 /15 /05 00: 51 06 /15 /05 15 : 25 06 /16 /05 00:13 06 /16/05 17 : 05 06 /17 /05 01 :12 08 /22/05 09:00 06 /02/05 13 :55 06 /02 /05 13:55 06 /04 /05 08 :53 06 /04 /05 08:53 06 /06 /05 08: 17 06 /06 /05 08 : 17 07 /15 /05 06 : 00 06 /10/05 08 :07 06 /10/05 08 :08 06 /10 /05 12 : 15 06 /13 /05 08 :20 06 /13/05 08 :21 06 /13 /05 08 :45 06 /13 /05 09:57 07 /15 /05 06:00 06 /13 /05 09:26 06 /14 /05 10:55 06 /14 /05 10:55 08 /22 /05 09:00 06 /13 /05 09 :56 06/13 /05 13: 25 06 /13 /05 13:25 06 /14 /05 22 :03 06 /15 /05 00 :51 06 /15 /05 15 :25 06 /16/05 00:13 06 /16/05 17:05 06 /17/05 01 :12 08 /22/05 09 :00 06 /02/05 13 : 58 06 /02/05 17: 19 07 /15 /05 06:00 Page 8 of 9 ~ <,J Reason I Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Retrieve from Storage Load on Instrument Unload from Instrument Return to Storage Disposed Retrieve from Storage Custody Transfer Return to Storage Re trieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J131 -11.1 Digestate from J 131-11.1 Return to Storage Disposed Digestate from J 131-11.1 Digestate from J131-11.l Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Disposed IDl!i 41 of 193 11\;iACCU l"ES r. J131 Accutest Internal Chain of Custody Job Number: Jl31 Account : DEMO Demo Account Project : Demo Site Received: 05 /27 /05 Sample .Bottle Transfer Transfer Number FROM TO J131-12 .l Secured Storage Todd Shoemaker J131-12 .l Todd Shoemaker Julie Hong J131-12 .l Juli e Hong Secured Storage J131-12 .l Secured Storage Dave Hunkele J 131-12 .l Dave Hunkele Michael Wassef J131-12. l Michael Wassef Joan D. McCormack 1131-12 .1 Joan D. McCormack Secured Storage J131-12. l Dave Hunkele Jl31-12.l.l Joan D . McCormack Metals Digestion J131-12. l.l Metals Digestion Michael Wassef J131-12 .l.l Michael Wassef Metals Digestate Storage J131-12 .l.l Metals Digestate Storage J131-12 .l.2 Joan D . McCormack Metals Digestion J131-12 .l.2 Metals Digestion Michael Wassef J131-12 .l.2 Michael Wassef Metals Diges tate Storage J131-12 .l.2 Metals Digestate Storage Kathy Lukenda Jl31-12 .l.2 Kathy Lukenda Metals Digesta te Storage J131-12 .l.2 Metals Digestate Storage Kathy Lukenda J131-12 .l.2 Kathy Lukenda Metals Digestate Storage J131-12 .l.2 Metals Digestate Storage Kathy Luken da J131-12. l.2 Kathy Lukenda Metals Digestate Storage 1131-12 .1.2 Metals Digestate Storage J131-12.3 Secured Storage Saraswathi Dodd i J131 -12 .3 Saraswathi Doddi VOA Prep Storage J131-12 .3 VOA Prep Storage Sarah A . Chin J131-12.3 Sarah A . Chin GCMSO J131-12 .3 GCMSO Saraswathi Doddi J131-12.3 Saraswathi Doddi Secured Storage J131-12.3 Dave Hunkele Date/Time 06 /10 /05 08 :07 06 /10 /05 08 :08 06 /10 /05 12:15 06 /13 /05 08 :20 06 /13 /05 08:21 06 /13 /05 08:45 06 /13 /05 09 :57 07 /15 /05 06 :00 06 /13 /05 09:26 06 /14 /05 10 :55 06 /14 /05 10:55 08/22/05 09 :00 06 /13 /05 09 :56 06 /13 /05 13 :25 06 /13 /05 13 : 25 06 /14 /05 22 :03 06 /15 /05 00:51 06 /15/05 15:25 06 /16/05 00 :13 06 /16/05 17 :05 06 /17 /05 01: 12 08 /22/05 09 :00 06 /02 /05 13:55 06 /02/05 13:55 06 /04 /05 08 : 53 06 /04 /05 08 : 53 06 /06 /05 08 : 17 06 /06 /05 08 : 17 07 /15 /05 06 :00 Page 9 of 9 ~ (,.) Reason I Retrieve from Storage Custody Transfer Return to Storage Retrieve from Storage Custody Transfer Custody Transfer Return to Storage Disposed Digestate from J131 -12 .l Digestate from J131-12 .l Return to Storage Disposed Digestate from Jl 31-12 .1 Digestate from J131-12.l Return to Storage Retrieve from Storage Return to Storage Retriev e from Storage Return to Storage Retrieve from Storage Return to Storage Disposed Retrieve from Storage Return to Storage Retrieve from Storage Load on Instrument Unload from Instrument Return to Storage Disposed 1111!1 42 of 193 l3ACCUTEST. J131 }. :) '.) ( (, 1 ') I)< IJJl!j New Jersey l3A~__i_'4#~ !r S All I N lHt tHfMlSTR'V GC/MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Instrument Performance Checks (BFB) • Internal Standard Area Summaries • Surrogate Recovery Summaries • Initial and Continuing Calibration Summaries Section 5 IJl!t 43 of 193 l;3ACCUTEST. J131 C l :• ~· r <' 1 ') • 1> < Method Blank Summary Job Number : ]131 Account : DEMO Demo Account Project: Demo Site Sample File ID DF V04366-MB1 096932.D 1 Analyzed By 06 /04 /05 SWD Prep Date n/a The QC reported here applies to the following samples : ]131-2 , ]131-3 CAS No . Compound Result RL MDL Units 71-43-2 Benzene ND 1.0 0 .33 ug /1 100-41-4 Ethylbenzene ND 1.0 0.22 ug /1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.41 ug/1 91-20-3 Naphthalene ND 2.0 0.69 ug /1 75-65-0 Tertiary Butyl Alcohol ND 25 10 ug /1 108-88-3 Toluene ND 1.0 0 .11 ug /1 1330-20 -7 Xy lenes (total) ND 1.0 0.26 ug /1 CAS No . Surrogate Recoveries Limits 17060-07-0 l ,2-Dichloroethane-D4 (SUR) 103 % 63-136 % 2037 -26-5 To luene -DB (SUR) 101 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 87 % 80-115% Page 1 of 1 Prep Batch Analytical Batch n/a V04366 Method : EPA 624 Q 111!:1 44 of 193 (dACCUTEST. J131 ',."' • • ., · '"· Method Blank Summary Job Number : J131 Account: DEMO Demo Account Project: Demo Site Sample File ID OF V04367-MB1 096958 .D 1 Analyzed By 06 /04 /05 SWD Prep Date n/a The QC reported here applies to the following samples: J131-1, J131-4, J131-7, J131-8, J131-9, J131-10, J131-ll, J131-12 CAS No . Compound Result RL MDL Units 71-43-2 Benzene ND 1.0 0.33 ug/1 100-41-4 Ethylbenzene ND 1.0 0.22 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.41 ug /1 91-20-3 Naphthalene ND 2.0 0.69 ug /1 75-65-0 Tertiary Butyl Alcohol ND 25 10 ug /1 108-88-3 Toluene ND 1.0 0.11 ug/1 1330-20-7 Xylenes (tota l) ND 1.0 0 .26 ug /1 CAS No . Surrogate Recoveries Limits 17060-07-0 1 , 2-Dich loroethane-D4 (SUR) 97% 63-136 % 2037-26-5 Toluene-OS (SUR) 103 % 90-110 % 460-00-4 4-Bromofluorobenzene (SUR) 82 % 80 -115 % Page 1 of 1 Prep Batch Analytical Batch n/a V04367 Method: EPA 624 Q 45 of 193 ACCUTESr. J131 '' ,, , .. , ,. AC & 1 cST ~ oo GU r vOA , SOIL MDL STUDY -3 '/6010B T JA TRACE 1 Date UNITS Al Sb As Ba Be B Cd Ca Cr Co Cu Fe Pb mg/I 0 .11276 0 .02003 0 .00888 0 .00459 0.00077 0 .01645 0 .00189 0 .13112 0 .0051 0.00412 0 .0024 0 .13771 0.00393 mg/I 0 .14809 0 .01845 0 .01052 0 .00471 0 .00079 0 .01465 0.00161 0 .14343 0.00463 0 .00346 0 .00264 0 .15513 0.00374 mg/I 0.12957 0.02031 0 .00882 0 .00474 0.00074 0 .01535 0 .00187 0 .13671 0.00475 0.00259 0 .00294 0.15435 0.00291 mg/I 0.14863 0.01951 0 .00943 0.0048 0.00064 0 .01446 0.00162 0 .12821 0.00467 0.00347 0 .00342 0.13946 0.00245 mg/I 0 .15175 0.02027 0 .00864 0 .0051 0 .00061 0.01501 0 .00172 0.13314 0 .00465 0.0037 0.00304 0 .15227 0.00206 mg/I 0.14061 0.01902 0.00923 0 .00506 0 .0007 0 .01464 0 .00192 0 .14148 0 .00491 0.00266 0.0024 0.14769 0 .0045 mg/I 0 .14621 0.01824 0 .0094 0.00494 0.00069 0 .01499 0 .00258 0 .13427 0.00519 0 .00291 0.0024 0 .14312 0 .00457 03-JAN-07 MDL in mg/I 0 .04379 0 .00268 0 .00197 0 .00060 0.00021 0 .00212 0 .00104 0 .01718 0 .00072 0.00179 0 .00125 0 .02244 0 .00401 T15647-2 Spike Amt in mg/I 0 .15 0 .02 0.01 0.004 0.0004 0 .02 0.002 0 .15 0 .005 0 .004 0.005 0 .15 0.005 1 OX rule met? OK OK OK OK OK OK OK OK OK OK OK OK OK RL in mg/I 0 .2 0.01 0.01 0.2 0.005 0 .1 0.005 5 0 .01 0 .05 0 .025 0 .1 0 .01 MDL< RL OK OK OK OK OK OK OK OK OK OK OK OK OK Spike in mg/kg 15 .00 2.00 1.00 0.40 0 .10 2.00 0 .20 15 .00 0 .50 0.40 0 .50 15 .00 0.50 RL in mg/kg 20 .00 1.00 1.00 20 .00 0 .50 10 .00 0 .50 500 .00 1.00 5 .00 2 .50 10.00 1.00 MDL in mg/kg 4 .38 0.27 0 .20 0 .06 0.02 0 .21 0.10 1.72 0 .07 0 .18 0 .12 2.24 0.40 Verification 1 .0733 0 .00421 0.00537 0 .21265 0.00485 0 .09343 0 .00377 2.7038 0.01229 0 .04691 0 .04103 0 .11268 0 .01012 Date UNITS Mg Mn Mo Ni K Se Ag Na Tl Ti V Zn Sr Sn mg/I 0 .35986 0 .00189 0.00528 0 .00818 0.47523 0 .01841 0 .00535 1.373 0.00864 0 .00333 0 .0037 0.01158 0 .0136 0.0302 mg/I 0.36366 0 .00175 0 .00655 0 .00878 0.40252 0 .0186 0 .00518 1.362 0 .00773 0.00373 0.00432 0 .01152 0 .0138 0.0309 mg/I 0 .36229 0 .00203 0 .00524 0 .00863 0.41003 0 .01679 0.00516 1.282 0.01019 0.00298 0.00472 0.01168 0.0139 0.0313 mg/I 0.35757 0.00171 0.00613 0.00829 0 .35642 0.01901 0 .0051 1.182 0.01152 0 .00353 0 .00432 0.01146 0 .014 0 .0297 mg/I 0 .36653 0 .00234 0.00557 0 .00791 0 .31789 0 .01903 0 .00511 1.25 0.01229 0.00309 0.00425 0 .01227 0.0137 0.0311 mg/I 0 .36449 0 .00177 0 .0057 0 .00806 0 .60335 0 .01853 0.00541 1.149 0 .0106 0.00362 0 .00486 0.01158 0.0137 0.0319 mg/I 0.36756 0 .0021 0.00607 0 .00908 0 .52386 0 .01821 0.00577 1.313 0 .01087 0.0035 0 .0043 0 .01494 0 .0136 0.0301 MDL in mg/I 0 .01115 0 .00072 0 .00151 0 .00133 0 .31175 0.00238 0 .00075 0 .26824 0 .00500 0.00087 0.00117 0 .00396 0.00047 0.00243 03-Jan-07 Spike Amt in mg/I 0 .04 0 .002 0.005 0 .01 1 0 .02 0 .005 1 0 .02 0 .005 0.005 0 .01 0 .015 0 .015 1 OX rule met? OK OK OK OK OK OK OK OK OK OK OK OK REDO OK RL in mg/I 5 0 .015 0 .01 0 .04 5 0 .01 0 .01 5 0 .01 0.02 0.05 0 .02 0.02 0 .02 MDL< RL OK OK OK OK OK OK OK OK OK OK OK OK OK OK Spike in mg/kg 4.00 0 .20 0 .50 1.00 100 .00 2 .00 0.50 100 .00 2 .00 0 .50 0 .50 1.00 1.50 1.50 RL in mg/kg 500 .00 1.50 1.00 4 .00 500 .00 1.00 1.00 500 .00 1.00 2 .00 5 .00 2 .00 2 .00 2.00 MDL in mg/kg 1.11 0.07 0 .15 0 .13 31 .1 8 0 .24 0 .08 26 .82 0 .50 0.09 0 .12 0.40 0.05 0.24 Verification 2.239 0 .01647 0.0071 0 .04007 2 .5727 0.00396 0.00981 2 .228 0 .0055 0 .01765 0 .05263 0 .07461 0 .009 0.025 Accfu 11::ST l.:Atj~ GU r 1..,0A , Water MDL STUDY - 3 V6010B T JA TRACE 1 Month Year ------ Date UNITS Al Sb As Ba Be B Cd Ca Cr Co Cu Fe mg/I 0 .13409 0 .00505 0 .00588 0 .00223 0.00531 0.00592 0.00092 0.09988 0 .00265 0.00074 0 .00596 0 .10685 mg/I 0 .12 342 0.00502 0.0066 0 .00313 0 .00521 0 .00806 0 .0015 0 .1188 0 .00254 0 .00058 0.0052 0.08491 mg/I 0 .13404 0 .00672 0 .00449 0 .00258 0 .00522 0 .00667 0 .00125 0 .1363 0 .00166 0 .0087 0.00559 0 .09415 mg/I 0.20463 0.00679 0 .00592 0 .00247 0.00525 0 .00588 0.00099 0.11427 0.00291 0.00042 0 .00536 0.08887 mg/I 0 .13 308 0.00565 0.00573 0 .00279 0 .00518 0 .00644 0.00242 0.22925 0.00257 0.00061 0.00552 0.09318 mg/I 0.13651 0 .00664 0 .00415 0 .00427 0.00516 0.00826 0.00087 0.22898 0 .0023 0 .00065 0.00587 0 .08683 03-Jan-07 mg/I 0 .13991 0.00504 0 .00505 0.00395 0 .0054 0 .00665 0.00075 0.18437 0 .00309 0.00087 0.0068 0 .08515 MDL in mg/I 0 .08588 0.00265 0.00274 0.00243 0 .00026 0 .00301 0 .00181 0 .17248 0.00145 0.00957 0.00590 0 .02425 Spike Amt in mg/I 0 .100 0 .005 0.005 0 .002 0.005 0.006 0 .001 0.050 0 .005 0 .002 0.005 0.100 10X rule met? OK OK OK OK OK OK OK OK OK OK OK OK RL in mg/I 0 .2 0 .005 0 .005 0 .2 0.005 0.1 0 .004 5 0 .01 0.05 0.025 0 .1 MDL< RL OK OK OK OK OK OK OK OK OK OK OK OK Verification 0 .1258 0 .02453 0 .01265 0 .11408 0 .00261 0.38905 0.00239 0.18784 0.00534 0 .00453 0.00393 0 .14187 Date UNITS Mg Mn Mo Ni K Se Ag Na TL Ti V Zn mg/I 0 .04346 0.00629 0.00399 0 .00062 0.22273 0.00449 0 .00168 1.017 0.00429 0 .00075 0.00119 0 .00931 mg/I 0.05115 0 .0087 0.00478 0.00009 0 .14598 0 .00502 0 .00223 0 .8096 0.0027 0.00064 0.00093 0.00868 mg/I 0.04735 0.00637 0.00449 0.00079 0 .2121 0.00415 0.00206 0.9527 0.00198 0.00052 0.00041 0.01076 mg/I 0 .0396 0.00713 0 .0047 0 .00089 0 .20327 0 .00356 0 .00245 1.042 0 .0031 0 .00052 0.00061 0 .00801 mg/I 0.04711 0.00833 0.00475 0.00259 0 .18448 0 .00334 0 .00254 1.04 0.00361 0.00075 0.00114 0.01517 03-JAN-07 mg/I 0.04454 0.00538 0.00403 0.0008 0 .12594 0 .00299 0.00192 0 .81 0 .00204 0 .00041 0.0011 0 .01022 NI 05 -JAN -07 Al ,Be ,Cr ,Cu ,Fe ,K, mg/I 0.05053 0.00548 0.00496 0.00028 0.08474 0 .00446 0.00171 1.016 0.00245 0.00109 0.00072 0.00903 Na ,Pb ,TI MDL in mg/I 0 .01277 0 .00411 0 .00119 0 .00256 0 .16032 0 .00228 0 .00107 0.32564 0.00266 0.00071 0 .00094 0.00750 10-JAN -07 Spike Amt in mg/I 0.050 0 .005 0 .002 0.002 0 .300 0 .005 0.002 0.300 0.010 0.002 0 .002 0.002 1 OX rule met? OK OK OK OK OK OK OK OK OK OK OK OK RL in mg/I 5 0.015 0.01 0 .04 5 0 .005 0 .01 5 0.01 0.02 0 .05 0.02 MDL< RL OK OK OK OK OK OK OK OK OK OK OK OK Verification 0 .12923 0 .0153 0 .01356 0 .00428 0 .01169 0 .00663 0 .9982 0 .00621 0 .00414 0.00443 0 .1538 MDL Solution= (10ml of Soln 1 + 10ml of Soln 2+ 10ml of Soln 3 + 10ml of Soln 4 + 10ml of Soln 5 + 30ml HN03 + 50ml HCL) to 1 L Soln 1 [Al,Ca ,Fe,Mg,K,Na] = 0.05 ml of 10,000ppm each Al ,Ca ,Fe ,Mg ,K + 0.10 ml of 10,000ppm Na+ 3ml HN03 + 5ml HCI to 100 ml. Soln 2 [Sb ,As ,Pb,Mn,Se,TI] = 0 .05 ml of 1000ppm each+ 3ml HN03 + 5ml HCL to 100ml Soln 3 [Ba ,Cr,Co,Cu,Mo ,Ni ,Ag,Ti ,V ,Zn] = 0.02 ml of 1000ppm each+ 3ml HN03 + 5ml HCL to 100ml Soln 4 [Be ,Cd] = 0 .010 ml of 1 OOOppm each + 3ml HN03 + 5ml HCL to 100ml Soln 5 [B ,Sr,Sn] = 0 .06 ml of 1000ppm B + 0 .10 ml of 1000ppm Sr,Sn + 3ml HN03 + 5ml HCL to 100ml Digest MBlk and 7 individual vessels of MDL soln,each containing 50 ml of the MDL soln. Pb 0.00577 0.00543 0.00596 0.0043 0.00431 0.00433 0.00358 0.00283 0.003 OK 0.003 OK 0 .01126 Sr Sn 0 .0079 0.0083 0 .0093 0.0099 0.0088 0.0087 0.0085 0.0095 0.0095 0 .0099 0.0086 0 .0095 0.0093 0.0092 0.00177 0.00189 0.010 0.010 OK OK 0.02 0 .02 OK OK 0 .0263 0.0283 Method: lnstrument(s): Analyst: Cmpd./Element/Parm. Name Ace naph thene Ace naphthy lene Anthracene Benzo( a )anthra cene Be nzo(a )pyre ne Benzo( b )fi uora nthene Benzo(g,h,i)pe ry lene Be nzo(k )fiu oranthe ne Ch rvs ene Dibenzo(a ,h )anthracene Fluo ra nthene Fluorene lnde no(1,2,3-cd)pyrene 1-Methy lnaphthalene 2-Methylnaphtha lene Naphthalene Ph e na nthre ne Pyrene FALSE Accutest Laboratories Annual Method Detection Limit Determination Houston, Tx Facility SW846 82 70C B Y SIM (AB8270SIM ) GCMSA, GCMSH , P ool e d Analys is Spike R1 R2 Date ug/kg ug/kg ug/kg 10-Jan -0 7 5.56666 11 6 .00 5 .04 10-Ja n-07 5.56666 11 4 .74 4 .0 1 9-Ja n-0 7 5.56666 11 6 .84 7 .40 9 -Jan -07 5.56666 11 4.98 5 .37 9-Jan-07 5 .56666 11 8 .92 7.46 9-Jan-07 5 .56666 11 4 .63 5 .41 10-Jan -0 7 5 .56666 11 6 .66 6.16 9-Ja n-07 5.566661 1 7 .13 7 .94 10-Jan-07 5 .56666 11 5 .65 5.15 9 -J an-07 5 .5 6666 11 8 .26 8.46 10 -Jan-07 5.56666 11 7 .63 7 .56 10-Jan-07 5 .56666 11 3 .85 3.35 9-Ja n-0 7 5.56666 11 8 .34 7.80 9-Jan-0 7 5 .566661 1 7 .6 1 7 .00 9-Jan-0 7 5.5666611 2 .02 2.36 9-Jan-0 7 5 .566661 1 4 .1 8 4.27 9-Ja n-0 7 5 .56666 11 5 .29 4 .64 10-Jan-07 5.56666 11 7 .54 7 .80 Replicate Spikes R3 R4 RS R6 R7 ug/kg ug/kg ug/kg ug/kg ug/kg 5 .52 6.14 5.32 5 .20 5 .62 3 .84 4.4 7 3.7 1 3.57 4 .05 6.24 7.54 7.77 7.66 7 .7 1 4.52 4 .10 5 .17 3.90 4 .7 3 7.47 7.25 8.43 7.18 7.07 5.05 5 .22 4 .56 4 .62 4.49 6 .86 7 .5 1 5 .53 6 .20 5.95 7 .03 6 .92 7 .17 6.40 6 .58 6.06 5 .82 4.7 1 5.24 5.49 8.01 7.62 6 .96 7.38 7 .77 7.17 7.10 6.89 6 .35 6 .80 3.07 3 .69 3 .11 3.00 3.45 8.77 7 .8 1 8.13 6 .75 8 .36 8.9 0 8.12 8.46 8.68 10 .4 6 2.19 2.50 2.32 2.49 2 .63 4 .29 4.46 3.62 4.4 1 2.98 4.47 4.94 5 .65 5.64 6.13 8.77 8.48 6 .59 8.42 8.80 Matrix : Quant Factor: Study Period : X-Bar X-Bar ug/kg %Recov . 5 .55 99.65 4 .06 72 .86 7.3 1 13 1.28 4.68 84 .08 7 .68 138 .05 4 .85 87.18 6.4 1 115 .15 7.03 126 .21 5.45 97.84 7.78 139 .76 7 .0 7 127 .04 3.36 60 .33 7.99 14 3.6 1 8.46 152 .02 2.36 42 .39 4 .0 3 72.38 5 .25 94 .35 8 .06 144.75 so 33.33 Jan ua ry ,2007 STD .Dev . ug/kg 0 .40 0.4 2 0 .57 0 .54 0 .7 1 0 .37 0.65 0.50 0.45 0.52 0.44 0.32 0.64 1.10 0 .2 1 0 .54 0 .6 0 0 .80 MDL Spike/MDL Ratio 1.27 4.3 7 1.3 1 4.25 1.78 3.13 1.7 1 3 .25 2 .22 2.5 1 1.1 5 4 .84 2.05 2.71 1.56 3.57 1.43 3 .9 1 1.63 3.42 1.39 4.0 0 1.02 5.45 2.02 2.75 3.45 1.6 1 0 .65 8 .60 1.69 3.29 1.89 2.94 2 .52 2.2 1 Method: lnstrument(s): Analyst: Cmpd./Element/Parm. Name Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene lndeno(1,2,3-cd)pyrene 1-Methylnaphthalene 2-Methvlnaphthalene Naphthalene Phenanthrene Pyrene FALSE Accutest Laboratories Annual Method Detection Limit Determination Houston, Tx Facility SW846 8270C BY SIM (AB8270SIM) GCMSA, GCMSH Pooled Analysis Spike R1 Date ug/1 ug/1 9-Jan-07 0.2 0.19 9-Jan-07 0.2 0.10 9-Jan-07 0.2 0.11 9-Jan-07 0.2 0.14 9-Jan-07 0.2 0.29 9-Jan-07 0.2 0.19 9-Jan-07 0.2 0.32 9-Jan-07 0.2 0.13 9-Jan-07 0.2 0.25 9-Jan-07 0.2 0.11 9-Jan-07 0.2 0.13 9-Jan-07 0.2 0.10 9-Jan-07 0.2 0.28 9-Jan-07 0.2 0.20 9-Jan-07 0.2 0.09 9-Jan-07 0.2 0.14 9-Jan-07 0.2 0.16 9-Jan-07 0.2 0.17 R2 ug/1 0.22 0.10 0.12 0.17 0.31 0.24 0.32 0.16 0.24 0.13 0.14 0.11 0.30 0.15 0.09 0.17 0.22 0.17 Replicate Spikes R3 R4 RS R6 R7 ug/1 ug/1 ug/1 ug/1 ug/1 0.21 0.18 0.16 0.16 0.18 0.10 0.08 0.06 0.06 0.07 0.11 0.11 0.09 0.12 0.12 0.14 0.17 0.13 0.15 0.14 0.28 0.26 0.32 0.24 0.24 0.23 0.20 0.23 0.20 0.22 0.35 0.37 0.34 0.33 0.32 0.15 0.12 0.15 0.13 0.15 0.21 0.21 0.23 0.20 0.21 0.11 0.11 0.12 0.11 0.12 0.12 0.12 0.09 0.09 0.09 0.11 0.09 0.07 0.07 0.07 0.29 0.21 0.28 0.30 0.24 0.22 0.24 0.16 0.17 0.20 0.09 O.D7 0.05 0.05 0.05 0.19 0.12 0.12 0.10 0.11 0.20 0.18 0.16 0.15 0.16 0.19 0.16 0.12 0.13 0.14 Matrix: Quant Factor: Study Period: X-Bar X-Bar ug/1 %Recov. 0.19 94.03 0.08 41.03 0.11 56.15 0.15 74.39 0.28 138.64 0.22 107.89 0.34 168.47 0.14 71.17 0.22 110.03 0.12 57.78 0.11 55.52 0.09 44.70 0.27 136.21 0.19 96.30 0.07 33.59 0.13 67.09 0.18 87.80 0.15 76.76 AQ 1.00 January,2007 STD.Dev. ug/1 0.02 0.02 0.01 0.02 0.03 0.02 0.02 0.01 0.02 0.01 0.02 0.02 0.03 0.03 0.02 0.03 0.03 0.03 MDL Spike/MDL Ratio 0.07 3.04 0.05 3.68 0.04 5.46 0.06 3.62 0.10 2.02 0.06 3.61 0.06 3.41 0.05 4.33 0.06 3.43 0.03 6.29 0.07 2.81 0.06 3.25 0.11 1.86 0.11 1.84 0.06 3.09 0.11 1.89 0.08 2.39 0.08 2.47 Tamara Welch Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 WP-144 WatR™Pollution Study Open Date: 01/15/07 Close Date: 03/01/07 Report Issued Date: 03/22/07 Final Report March 22 , 2007 Tamara Welch Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 Enclosed is your final report for ERA's WatR™Pollution Proficiency Testing (PT) Study , WP-144. Your final report includes an evaluation of all results submitted by your laboratory to ERA. Data Evaluation Protocols: All analytes in the WatR™Pollution Proficiency Testing Study, WP-144 , have been evaluated using the following tiered approach . If the analyte is listed in the most current National Environmental Laboratory Accreditation Conference (NELAC) PT Field of Testing tables , the evaluation was completed by comparing the reported result to the acceptance limits generated using the criteria contained in the NELAC FoPT tables . If the analyte is not included in the NELAC FoPT tables , the reported result has been evaluated using the procedures outlined in ERA's Standard Operating Procedure for the Generation of Performance Acceptance Limits (SOP 0260). Corrective Action Help: As part of your accreditation(s), you may be required to identify the root cause of any "Not Acceptable" results , implement the necessary corrective actions , and then satisfy your PT requirements by participating in a Supplemental (QuiK™ Response) or future ERA PT study . ERA's technical staff is available to help your laboratory resolve any technical issues that may be impairing your PT performance and possibly affecting your routine data quality. Our laboratory and technical staff have well over three hundred years of collective experience in performing the full range of environmental analyses . As part of our technical support, ERA offers QC samples that can be helpful in helping you work through your technical issues . Thank you for your participation in ERA's WatR™Pollution Proficiency Testing Study , WP-144 . If you have any questions , please contact myself, or Curtis Wood , Quality Assurance Director , at 1-800-372- 0122 . Sincerely, Shawn Kassner Proficiency Testing Manager attachments smk 6000 West 54th Ave., Arvada, CO 80002 Curtis J . Wood Quality Assurance Director 800 -372-0122 fax (303) 42 1-0159 www.eraqc.com Report Recipient Contact/Phone Number Reporting Type Arkansas Jane Hurley/ 501-682-0 938 All Analytes Florida Steve Arms / 904-791-1599 A ll Ana lytes Kansas Jack McKenzie / 785-296-1639 All Analytes Lou is iana Ka ren Varnado/ 225-2 19-9800 A ll A nalytes Oklahoma David Caldwell/ 405-702-1024 All Analytes Texas Max Phillips/ 512-239-3518 All Analytes WP-144 Definitions & Study Discussion Study Dates: 01/15/07 -03/01/07 WP Study Definitions The Reported Value is the value that the laboratory reported to ERA. The ERA Assigned Values are compliant with the most current USEPA/NELAC FoPT tables . A parameter not added to the standard is given an Assigned Value of "O" per the guidelines contained in the USEPA's Criteria Document and NELAC standards. The Acceptance Limits are established per the criteria contained in the most current USEPA/NELAC FoPT tables, or ERA's SOP for the Generation of Performance Acceptance Limits ™ as applicable. The Performance Evaluation: Acceptable = Reported Value falls within the Acceptance Limits . Not Acceptable = Reported Value falls outside the Acceptance Limits . No Evaluation = Reported Value cannot be evaluated. Not Reported = No Value reported . The Method Description is the method the laboratory reported to ERA. Report Issued: 03/22/07 WP Study Discussion ERA's WatR™Pollution Proficiency Testing Study, WP-144, has been reviewed by ERA Senior Management and certified compliant with the requirements of the USEPA's National Standards for Water Proficiency Testing Studies Criteria Document (December 1998), and the criteria contained in the most current NELAC FoPT tables. ERA's WatR™Pollution Study, WP-144 , standards were examined for any anomalies. A full review of all homogeneity, stability and accuracy verification data was completed . All analytical verification data for all analytes met the acceptance criteria contained in the USEPA's National Criteria Document for Water Proficiency Testing Studies , December 1998, and the criteria contained in the most current NELAC FoPT tables. The data submitted by participating laboratories was also examined for study anomalies. There were no anomalies observed during the statistical review of the WatR ™ Pollution Proficiency Testing Study , WP-144 , data. WatR™Pollution Study reports shall not be reproduced except in their entirety and not without the permission of the participating laboratories. The report must not be used by the participating laboratories to claim product endorsement by any agency of the U . S. government. If you have any questions regarding ERA's WatR™Pollution Proficiency Testing Study, WP-144 , please contact Shawn Kassner, Proficiency Testing Manager, or Curtis Wood , Quality Assurance Director, at 1-800-372-0122. Study: WP-144 ERA Laboratory Code: A116001 Laboratory Name: Accutest Gulf Coast Page 1 of 18 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 ANn al. Analyte 0. Oil & Grease 0104 Oil & Grease (Gravimetric) 1860 Oil & Grease (Infrared) Total Residual Chlorine I 0098 !Total Residual Chlorine Trace Metals 0001 Aluminum 0016 Antimony 0002 Arsenic 1015 Barium 0003 Beryllium 1025 Boron 0004 Cadmium 0006 Chromium 0005 Cobalt 0007 Copper 0008 Iron 0012 Lead - 0010 Manganese 0074 Molybdenum 0011 Ni ckel 0013 Se lenium 0017 Silver 0075 Strontium 0018 Thallium 0014 Vanadium 0015 Zinc - WP-144 Final Complete Report Un it s mg/L mg/L mg/L µg/L µg/L µg/L µg /L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg /L µg /L µg /L µg/L µg /L µg /L µg /L µg/L µg/L EPAID: ERA Laboratory Code: TX01484 A116001 03/22/07 Report Issued : Study Dates: 01/15/07 -03/01/07 Reported Ass igned Acceptance Performance Method Descript ion Value Value Limits Evaluation 34 67 .5 45 .8 -80 .3 Not Acceptable EPA 1664 83 .0 57 .8 -97 .4 Not Reported 1.28 1.41 1.01-1 .74 Acceptable EPA 330.5 708 .73 618 485 -749 Acceptable EPA 60108 309 .17 307 209-372 Acceptable EPA 60108 400.71 401 335 -470 Acceptable EPA 60108 2 112.6 2080 1810 -2350 Acceptable EPA 60108 82 .69 80.8 67.5-91.4 Acceptable EPA 60108 1838.0 1890 1540 -2200 Acceptable EPA6010B 641.62 673 574 -764 Acceptable EPA 60108 574.72 568 495-642 Acceptable EPA 60108 584 .69 585 514 -656 Acceptab le EPA 60108 657.17 660 594 -726 Acceptable EPA 60108 599 .12 604 532-685 Acceptable EPA 60108 645 .51 647 565-726 Acceptable EPA6010B 235 .20 227 202 -252 Acceptable EPA 60108 105.42 104 83.2 -124 Acceptable EPA 60108 172 .93 175 152 -199 Acceptable EPA 60108 1000.8 991 788 -1150 Acceptable EPA 60108 181 .72 181 155-208 Acce ptable EPA 60108 85.3 91 .1 76 .9 -105 Acceptable EPA6010B 547 .27 552 446 -662 Acce ptable EPA 60108 1503.9 1530 1340-1710 Acceptable EPA 60108 184.76 169 143 -200 Acceptable EPA6010B Page 3 of 18 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 ANnal. Analyte o . Tin & Titanium 1175 Tin 0076 Tita nium Tin & Titanium 1175 Tin 0076 Titanium WP-144 Final Complete Report Un its µg/L µg/L µg /L µg/L EPA ID : ERA Laboratory Code: TX01484 A116001 03/22/07 Report Issued: Study Dates : 01/15/07 -03/01/07 Reported Assigned Acceptance Performance Method Description Value Value Lim its Evaluation 1688 1700 1340 -2060 Acceptable EP A 6010 B 194 .82 190 163-214 Acceptab le EPA 60 10 B 1688 1700 1340 -2060 Acceptable EPA 200 .7 194 .82 190 163 -214 Acceptab le EPA 200 .7 Page 5 of 18 All analytes are incl ud ed in ERA's A2LA accreditatio n. Lab Code : 1539 -01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 ANnal. Analyte 0. Trace Metals 0001 Aluminum 0016 Antimony 0002 Arseni c 1015 Barium 0003 Beryllium 1025 Boron 0004 Cadmium 0006 Chromium 0005 Cobalt 0007 Copper 0008 Iron 0012 Lead 0010 Manganese 0074 Molybdenum 0011 Nickel 0013 Selenium 0017 Silver 0075 Strontium 0018 Tha lli um 0014 Vanadium 00 15 Zinc Minerals 0027 Alkalinity as CaC03 0028 Chloride 0020 Conductivity at 25 °C 0029 Fluoride 0026 Potassium 0025 Sodium 0030 Sulfate . - 0021 Total Dissolved Solids at 180°C 1950 Total Solids at 105°C Hexavalent Chromium I 1045 !H exava lent Chromium Nitrite I 1840 !N itrite as N Turbidit 2055 Turbidity .. -. --- WP-144 Final Complete Report Units µg/L µg /L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg /L µg /L µg /L µg /L µg /L µg/L µg /L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L mg/L µmhos/cm mg/L mg/L mg/L mg /L mg/L mg /L µg/L mg/L NTU EPAID: ERA Laboratory Code: Report Issued: TX01484 A116001 03/22/07 Study Dates: 01/15/07 -03/01/07 Reported Ass igned Acceptance Value Va lue Limits 708 .73 618 485 -749 309 .17 307 209-372 -- 400 .71 401 335 -470 2112.6 2080 1810 -2350 82.69 80.8 67.5 -91.4 ·-·- 1838.0 1890 1540 -2200 64 1.62 673 574 -764 574.72 568 495-642 584 .69 585 514-656 657 .17 660 594 -726 599 .12 604 532 -685 645 .51 647 565-726 235 .20 227 202 -252 105.42 104 83 .2 -124 172 .93 175 152 -199 1000.8 991 788 -1150 181 .72 181 155 -208 85 .3 91.1 76.9-105 547 .27 552 446-662 1503 .9 1530 1340-1710 184 .76 169 143 -200 16 16 .4 10 .1 -22 .2 16 16.4 10 .1 -22 .2 44 44 .6 38 .3 -51.4 48 39 .3 33 .1 -46.2 303 278 246 -311 1.9 2.53 2.09 -2.98 25 .53 20 .9 17 .2-25.0 45 .08 44.9 38 .1 -51 .6 18 .93 19 .3 15 .0 -23 .2 156 194 141-247 208 20 7 171-242 177 793 648 -931 2.427 2.46 2.08 -2.84 5 .6 3.67 2.95-4 .37 Page 4 of 18 Performance Evaluat ion Acceptable Acceptab le Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Not Acceptable Acceptable Not Acceptable Not Acceptable Acceptable Acceptable Acceptable Acceptable Method Descr iption EPA 200.7 EPA 200 .7 EPA 200 .7 EPA 200 .7 EPA 200 .7 EPA 200.7 EPA200.7 EPA 200 .7 EPA 200.7 EPA 200 .7 EPA 200 .7 EPA 200 .7 EPA 200.7 EPA 200 .7 EPA 200 .7 EPA 200 .7 EPA 200.7 EPA 200.7 EPA 200 .7 EPA 200 .7 EPA 200 .7 EPA 7470A EPA 245.1 EPA310.1 EPA 325 .3 EPA120.1 340.2 EPA 6010B EPA 6010B 375 .3 EPA160.1 EPA 160 .3 ! Not Acceptable ! EPA 7196A Ac ceptable EPA 353 .2 Not Acceptable EPA180.1 All analytes are included in ERA's A2LA accreditation . Lab Cod e: 1539-01 ~ Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No . H 0019 pH H 0019 pH Hardness 0072 Non-Filterable Residue (TSS) 0023 Calcium 0024 Magnesium 1550 Calcium Hardness as CaC03 0022 Total Hardness as CaC03 Hardness 0072 Non-Filterable Residue (TSS) 0023 Calcium 0024 Magnesium 1550 Calcium Ha rdness as CaC03 0022 Total Hardness as CaC03 Demand 00 38 BOD 0102 CBOD 0036 COD 0037 TOC Demand 0038 BOD 0102 CBOD 0036 COD 0037 TOC s· I N 1mpe utr,ents 0031 Ammonia as N 1820 Nitrate + Nitrite as N 0032 Nitrate as N 003 3 ortho-Phosphate as P s· I N t . t ,mp,e u r,en s 0031 Ammonia as N 1820 Nitrate + Nitrite as N 0032 Nitrate as N 0033 ortho-Phosphate as P 0034 Total Kjeldahl Nitrogen . WP-144 Final Complete Report Units S .U. S.U . mg/L mg/L mg/L mg/L mg /L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L . mg/L mg/L mg/L mg/L mg/L . mg/L mg/_L mg/L mg/L mg/L mg/L mg/L mg/L EPAID: ERA Laboratory Code: Report Issued : TX01484 A116001 03/22/07 Study Dates: 01/15/07 -03/01/07 Reported Assigned Acceptance Value Value Limits 5 .6 5 .6 68.0 73.43 27 .12 80 .16 300 73.43 27.12 32 34 47.3 19 .4 32.0 34.0 19.4 6 .13 0.753 0 .753 2 .14 0 .753 9.6 0 .32 Page 2 of 18 5.70 5.70 51.6 75 .2 28 .0 188 303 51.6 75.2 28 .0 188 303 29 .3 25 .3 47 .1 18.6 29.3 25 .3 47 .1 18.6 6 .34 0 .853 0 .853 2 .19 6 .34 0 .853 0.853 2 .19 14 .2 8.86 0.329 5.50 -5 .90 5.50-5 .90 40 .2 -58.9 67.3 -85.1 24 .0 -32 .2 168 -213 267 -345 40.2 -58.9 67 .3 -85.1 24 .0 -32 .2 168-213 267-345 14.5 -44.1 11 .3 -39 .3 31 .3 -59 .3 15.4-21 .8 14 .5 -44 .1 11 .3 -39 .3 31 .3 -59.3 15 .4-21 .8 4 .64 -8 .03 0.688 - 1.01 0.660 -1.05 1.77 - 2 .63 4 .64 -8 .03 0 .688 -1.01 0.660 -1.05 1.77-2.63 9.41 -18.4 7.33 -10.5 0 .171 -0.493 Performance Evaluation Acceptable Acceptable Not Acceptable Acceptable Acceptable Not Acceptable Acceptable Not Reported Acceptable Acceptable Not Reported Not Reported Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Not Reported Acceptable Acceptable Acceptable Acceptable Acceptable Not Reported Not Reported Acceptable Not Reported Not Reported Acceptable Acceptable Method Description EPA150.1 EPA 9040B EPA 160.2 EPA 6010B EPA 6010B EPA 130.2 EPA 130 .2 EPA 200 .7 EPA 200 .7 EPA405.1 SM 5210 B EPA410.4 EPA415.1 SM 5210 B EPA 405.1 EPA 9060 EPA 350 .1 EPA 353 .2 EPA 353 .2 EPA 365.2 SM 4500 N03-E EPA 365.2 EPA 335.3 All analytes are included in ERA's A2LA accreditation. Lab Code: 1539-01 Study: WP-144 ERA Laboratory Code: A 116001 Laboratory Name: Accutest Gulf Coast Page 6 of 18 WP-144 Final Complete Report Tamara Welch EPAID: ERA Laboratory Code: Report Issued: TX01484 A116001 03/22/07 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Study Dates: 01/15/07 -03/01/07 Houston, TX 77036 713-271-4700 ANnal. Analyte o . Volatiles 4315 Acetone . 4320 Acetonitrile 4325 Acrolein 434_0 . l\cr,,lc_>~itr~le 0065 Benzene 0060 Bromod ic hloromethane 0062 Bromoform 4950 Bromomethane 4410 2-Butanone (M~K) 5000 tert-Butyl methyl ether (MTBE) 4450 Carbon disulfide 0058 Carbon tetrachloride 0064 Chlorobenzene Units Reported Assigned Acceptance Value Value Limits µg/L 120 µg/L < 10 _ yQI~-< 10 µg/L < 10 µg/L 45 .9 µg /L 33.7 µg/L 35 .7 µg /L < 2 µg/L < 10 µg/L < 2 µg/L 57.5 yQI~ .. _ . __ ?1.]. ". _ .~Q/L 49.6 118 0.00 0.00 0.00 43 .5 33.4 31 .8 0.00 0.00 0.00 48.8 20.5 47.7 23.5-192 31 .1-55.6 23 .3 -45.0 19.6 -43.4 25 .9 -76 .6 11.7 -28.4 • ~ V, ~ N N N o 34.4 -59.9 Performance Evaluation Acceptable Acceptable . _ A.,cceptable . .A.c_cep!a_b_le Acceptable .A.cceptable Acceptable Acceptable Acceptable Acceptable Acceptable .. .A.c_c_epta_b_le Acc_ep!a_ble Method Description EPA 8260B EPA 8260B EPA8260B EPA8260B EPA8260B EPA 8260B EPA 8260B EPA 8260 B EPA 8260B EPA 8260B EPA 8260B EPA8260B EPA8260B 0061 Chlorodibromomethane 4485 Chloroethane µg/L 43.8 42.6 29.0 -56.5 Acceptable EPA 8260B -~QI~ < 2 0 .00 4500 2~C::~lorc_>e_th}'.lvinyle~her 0055 Chloroform 4960 Chloromethane V ~ ,, •. 0 V, V, V, -~gt~ µg/~. 4570 1,2 -Dibromo-3-chloropropane (DBCP) .. ~QI~ -- µQ/L µg/L 4585 1,2-Dibromoethane (EDB) 4595 Dibromomethane 0094 1,2-Dichlorobenzene 0096 1,3-Dichlorobenzene , V V •• ...... -· ........ ~QI~-- .. µg/L YQI~- < 10 22.5 <2 <2 <2 <2 36.4 9.6 0095 1,~-~)c_h~c_>n:>~E_)~z_e_n_e _. _ • ______ .• _ .•. __ •. __ YQI~ ... 39.3 <2 32 .7 25.7 <2 <2 <2 50.7 <2 4625 Dichlorodifluoromethane µg/L 4630 1, 1-Dichloroethane ~QI~ 0054 1,?-~ich!c_>ro eth_a~!:l --~Q/L .. 4640 1 '.1-Dichloroethylene 4645 cis-1 ,2~Di ~hloroet~}'.le ~e_ .. 4 700 trans-1,2-Dichloroe!hylene 4655 1,2-Dichloropropane 4680 cis -1 ,3-Dichloropropylene µg/L µg/L . ~g/L µg/L µg/L Page 7 of 18 All analytes are in cluded in ERA's A2LA accreditation . Lab Code: 1539-01 0.00 20.7 0.00 0.00 0.00 0.00 39.8 10 .9 42.6 0.00 28 .5 24.2 0.00 0.00 0.00 47.2 0.00 14.2 -27.7 27 .3-51.9 6.56 · 14 .5 28.6 -54.0 19.2 -38.9 16.7 -32 .7 30.7 -62.6 • _.A.c_c_ep!a_b]e_ _ •. ___ ~~~A269~. __ . .A.cceptable Acceptable A.,cc_ep!a_b_le Accepta_ble Acceptable .• .A.c_c_ep)a_b_le_ .• Acceptable Ac_ceptable .A.cc_ep)a_b~e _ .. Acceptable __ Acc.eptable .A.ccepta_ble Acceptable Acceptable Acceptable Acceptable Acceptable EPA8260B EPA8260B EPA 8260B EPA 8260B EPA 8260B EPA8260B EPA 8260B EPA 8260B EPA8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. A lyt No. na e Volatiles Continued 4685 trans-\3-~ich]oropropylene 0066 Et~~l~El ~~e_nE:1 . . . . • ••.... 4835 Hexachlorobutadiene 4860 2-Hexanone 0063 .. ~E:t~~IEl~El 7h19 ~9t; • • • • • • • •••.••• 4995 4-Methyl-2-pentanone (MIBK) 5005 Nap_ht~a_lene 5100 8_tyr~~: .•••• 5105 1 , 1, 1,2-Tetrachloroethane 5110 1, 1,2,2-Tetrac hloroethane 0059 T_etra 7~1oroe_thylen e. 0067 Toluene 5155 1,2,4-Trichlorobenzene . . .. 0056 1, 1, 1-T richloroethane . . 5165 1, 1,2-Trichloroethane 0057 Trichl_o:~e.thylE:1ne 5175 Trichlorofluoromethane 5180 1,2 ,3-Trichloropropane (TCP) 5225 Vinyl acet_a!e. .. 5235 Vinyl c~l_oride 5260 Xylenes , total WP-144 Final Complete Report EPA ID: ERA Laboratory Code: Report Issued: TX01484 A116001 03/22/07 Study Dates: 01/15/07 -03/01/07 Units µg/~ -~gl~ •.. µg_/L ~g_l~. Reported Assigned Acceptance Value Value Limits <2 40 .6 48 .5 <2 29.9 -55 .7 6 .32 -78.8 . . -~g_l~ .. _ ... 6~·.1 ... 0 .00 43 .6 63 .2 0 .00 63 .0 µg/L 87 .6 82 .0 .. -~9!~. 29 .4 42 .5 . . -~g_l~ --.. ""~1-3 .. "' .. ~~} ... 38 .6 -87 .7 38.2 -123 13 .4 -53.7 21 .9 -45 .0 µg/L __ µg_/L µg_/~ •.• µg/L µg/L µg/~ µg/L µg/L µg/~ µg/L .~9-'l . µg/~ µg/L <2 34 14.2 45 <2 45 .1 102 39 .4 <2 <2 < 10 29.8 127 Page 8 of 18 0.00 32 .3 14.6 44 .8 0 .00 42.5 93.9 37 .8 0 .00 0 .00 0.00 21.4 132 17 .5-49.3 7 .00 -19.5 31 .1-56.4 26.6 -56 .2 65 .0 -121 23 .9 -49 .8 8.56-34.2 75.6 -178 Performance Evaluation Acceptable A,ccep !able Acceptable Acceptable _ A,e:e:ep!abl E: •• Acceptable _ A,~c_epta_bl E:1 •• ~e:e:ep!~ble Acceptable Acc_eptable _ • ~~cep!~b}E:_ _ • Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable . Acc_eptab!E:1 . ~~c.ep !able Acceptable Method Description EPA 8260B EPA 8260B EPA 8260B EPA8260B EPA 8260B EPA 8260B EPA8260B EPA 8260B ~~~ .. N#N, •. ~~~~- EPA 8260B EPA8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA8260B EPA8260B EPA8260B EPA 8260B EPA 8260B All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 WP-144 Final Complete Report Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 EPAID: ERA Laboratory Code: Report Issued: Study Dates: TX01484 A116001 03/22/07 01/15/07 -03/01/07 ANnal. Analyte o. Units Reported Assigned Acceptance Value Value Limits Performance Evaluation Method Description Volatiles 4315 Acetone 4320 Acetonitrile 4325 Acrolein 4340 Acl')'.lonitrBe 0065 Benzene 0060 Bromodichloromethane 0062 Bromoform 4950 Bromomethane 4410 2~Butanone (MEK) .. 5000 _tE_J~-B_u!~l .rr,e_t~yl etherJ~TBE) 4450 Carbon disulfide 0058 Carbon tetrachloride 0064 Chlorobenzene 0061 Chlorodibromomethane 4485 Chloroethane 4500 2-Chlo ~oe thylvi ny lE_Jther 0055 Chloroform 4960 Chloromethane 4570 __ 1 !2-D!br?mo:~-7hlor.oprnpan_e (DBC:P)_ . 4585 1!~-!)ibrorn.aeth__a_nE_J _(~!)B) .. 4595 Dibromomethane µg/L -~g_l~. . -~Q/L ~QI~. ~Q/L µg/L ~Q/L ~QI~ •• µg/L .. µg/~ ~QI~ .. - µg/L µg/L µg/L µg/L µg/L .. ~g/~ µg/L .. µg/~- µg/L µg/L 0094 . 1 ,~-!)!c_h!~r??E:~:z:e_n.e _______________ .•• _ . __ ~Qi~. 0096 1_.3-Dichloroben:z:e_ne _ µQi~ 0095 1,4-Dichlorobenzene 4625 Dichlorodifluoromethane 4630 1, 1-Dichloroethane 0054 1,2-Dichloroethane 4640 1, 1_-!)ic_h!~r?e_it_hy~e_nE_J _ . _ 4645 c1s~ 1,?:Dichloroet~~lene 4700 tra_ns-_1,2-Dic_h_loroethy)e ne 4655 _1 !~-!)!c_h}~r?p r_op~~E_l ___ _ 4680 cis-1,3-Dichloropropylene µg/L . -~Qil _ .. µg /L µQ/L -_ µQ/L µg/~- .. _µg/L .•. -~QI~ µg/L 120 < 10 < 10 < 10 45.9 33.7 35.7 <2 < 10 <2 11 8 0.00 0.00 0.00 43.5 33.4 31.8 0 .00 0.00 0.00 57.5 48.8 21.1 49.6 43.8 <2 < 10 22.5 <2 <2 <2 <2 20.5 47.7 42.6 0.00 0.00 20.7 0.00 0.00 0.00 0.00 36.4 39 .8 9.6 10.9 39.3 <2 32.7 25.7 <2 <2 <2 50.7 <2 42.6 0.00 28.5 24.2 . ._PP9 . 0.00 0.00 47.2 0.00 Page 9 of 18 All analytes are included in ERA's A2LA accreditation. Lab Code: 1539 -01 23.5-192 31.1 -55.6 23 .3 -45.0 19 .6 -43.4 Acc_eptab_le Ac_c_ep!a_ble Acceptable . Acc_eptable _ i:,ccep!a_bl~ Acceptable i:,cceptable __ i:,c_cep!a_bl~ Acceptable . i:,cceptab}e 2?._9_ --~6.-~ __ . __ i:,c_c_ep!a_b}~ __ 11.7-28.4 34.4 -59.9 29.0-56 .5 14.2 -27.7 Acceptable i:,cc_eptable Acceptable Acceptable Acceptable Acceptable Acceptable Accep!able • Accepta_ble Acceptable _ ??-_3_-_ ~1:9 . _ •• i:,c_c_ep!a_b)~ •• 6.56 -14.5 Acceptable 28 .6 -54.0 19 .2 -38.9 16.7 -32.7 30.7 -62.6 Acceptable _ . i:,cc_ep!a_b)~ __ . Acceptable Acceptab_le • _ i:,c_c_ep!a_b_le • _ Acceptab)e Acceptable • _ i:,c_cep!a_b_le _ • Acceptable EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 EPA 624 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Volatiles (Continued) 4685 tra_n~--1_,3-_D~ch loropropylene 0066 ~t~xlb~~ze_n~ .. . . . . . ,..., ........ .. 4835 Hexachlorobutadiene 4860 2-Hexanone .. 0063 N .. -......... ., ., N -N ... ME:t~~le~~ ~~l_o~~E: • " " " N ,--, .. N W .... •, " -,, • N N n 4995 4-Methyl-2-pentanone (M IBK ) 5005 Naphthalene .. -.. 5100 5_tyre~e . . ... ......... .. .. .. ' ......... .,,., .,, 5105 1 , 1 , 1,2-Tetrachloroethane 5110 1, 1,2 ,2-Tetrachloroethane . . ,. ., .... 0059 T_eJr!l ~~l?~o_e_t~'.)'.IE_:ne .... . ..... ........... ._,.,.,,.,,.,,. ...... , .... , .. ,.,,.. .. 0067 Toluene 5155 1,2,4-Trichlorobenzene . ·-.. -· 0056 1 , 1, 1-Trichloroethane ... 5165 1 , 1 ,2-Trichloroethane 0057 T richloroeth ylene . .. 5175 Trichlorofluoromethane 5180 1,2 ,3-Trichloropropane (TCP) 5225 Vinyl acetate 5235 ~i~yl c~lo_ride . .. .. . . 5260 Xylenes, total PCBs in Water 0040 Aroclor 1016 .. 8885 Aroclor 1221 0042 Aroclor 1232 . .. .. . . . 0040 Aroclor 1242 . 0044 Aroclor 1248 0045 Aroclor 1254 0046 Aroclor 1260 PCBs in Water 0040 Aro cl or 1016 8885 Aroclor 1221 0042 Aroclor 1232 0040 Aroclor 1242 .. . . . 0044 Aroclor 1248 , .. , 0045 Aroclor 1254 0046 Aroclor 1260 PCBs in Oil 0099 Aroclor 1016/1242 0100 Aroclor 1254 0 101 Aroclor 1260 . WP-144 Final Complete Report EPA ID: ERA Laboratory Code: Report Issued: TX01484 A116001 03/22/07 Study Dates: 01/15/07 • 03/01/07 Units Reported Ass igned Acc e ptance Va lue Value Limits µQi~ <2 0.00 , . _µQ_i~. 40 .6 43.6 29.9 -55.7 , . ,,.,. '"• ... .. .,,.,.,,,,. . . .... ., " "'"' .... µg/L _ 48.5 63.2 6.32 · 78.8 .. µg/~ <2 0.00 .. . .. . . . . . -~QI~". 69.1 63.0 38 .6 · 87 .7 ·-,.,,,.,, ............ , .... '.,,..,.,,., . . ........ ., . . µg/L 87 .6 82.0 38 .2 -123 µQi~. 29.4 42 .5 13.4 · 53.7 . . . µg/~. 34.3 33 .3 21.9 -45 .0 .. •NNN • .... . . . . ., µg /L <2 0 .00 µQi~ 34 32 .3 17 .5 -49 .3 ... µQi~ •.. 14.2 14.6 7.00 -19 .5 , NNN 'N N A· -A ...... " .,,..,..,. .. ' = ......... , N N N A· A µg/L 45 44.8 31 .1-56.4 µg/~ <2 0 .00 ... . µg/~ 45 .1 42 .5 26 .6 -56 .2 .. ... . . . .. µg/L 102 93 .9 65 .0 -121 ygl~ 39.4 37.8 23 .9 -49 .8 , . y ". ... , . .. µg/L <2 0 .00 µg /L <2 0 .00 µg/L < 10 0.00 .. -~g/L 29 .8 21.4 8.56 • 34 .2 . NNA A ..... , .. µg/L 127 132 75.6 · 178 ~g/L < 0 .50 0.00 . . µg/L < 0 .50 0.00 µg/L < 0 .50 0 .00 .. .. . µg/L < 0 .50 0 .00 . . . .. µg/L < 0 .50 0.0 0 µg /L 4.20 4 .50 2.10 • 5.88 µg/L < 0 .50 0.00 µg/L < 0 .50 0 .00 µg/L < 0.50 0.00 A,-A<• µg /L < 0 .50 0 .00 µg/~ < 0.50 0.00 .. . µg/L < 0 .50 0 .00 . .. . . µg/L 4 .20 4 .50 2.10 · 5.88 µg/L < 0 .50 0.00 mg/kg 32.8 43 .6 8.20 · 58 .0 mg/kg <5 0.00 mg/kg <5 0.00 Page 10 of 18 Performance Evaluati on Accep!able . _.~cc_ep !ab!~ • Acceptable Acceptable .. A~c_ep !~b_lE: •. Acceptable A<:Ceptable Acceptable Acceptable Acceptable _ • ~~c.ep!~bl~ ... Acceptable Acceptable Acceptable Acceptable Accep!a_bl E: _ Acceptable Acceptable Acceptable Acceptable Acceptable Acce ptable Acce_ptable Acceptable Acceptable Acceptable Acce ptable Acceptable Acce ptable Acceptable Ac ceptable Accepta_ble Acceptable Acceptable Acceptable Acce ptable Acce ptable Acceptable Method Description EPA 624 EPA 624 .. . . EPA 624 EPA624 EPA 624 .. ' ........ ~ ' EPA624 EPA624 EPA 624 EPA 624 EPA624 EPA 624 .. .. EPA 624 EPA624 EPA 624 EPA 624 EPA 624 . . EPA624 EPA 624 EPA624 EPA 624 EPA 624 EPA 8082 EPA 8082 EPA 8082 EPA 8082 EPA 8082 EPA 8082 EPA 8082 EPA 608 EPA 608 EPA 608 EPA 608 EPA 608 EPA 608 EPA 608 EPA 8082 EPA 8082 EPA 8082 All analytes are included in ERA's A2LA accre ditation. Lab Code : 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No . 0 raanoc hi orine Pestici 0047 Aldrin ... 7110 alpha-BHC 7115 beta-BHC 7105 delta-BH C d es 7120 g_a~11_1a.-.s.~~(~in_d_a~e )_ •• 7240 alpha-Chlordane 7245 gan:ma-C_hlo_r9a~~ ... -.. 0049 4 ,4'-DDD .. N N N N N A " " ....... -N N N ... ... ..... ._ __ ' WP-144 Final Complete Report Un its µg/L µg/L µg/L µg/L .YQ'~ .. - .µg/L µg/L . . EPA ID: ERA Laboratory Code: Report Issued: TX01484 A116001 03/22/07 Study Dates: 01/15/07 · 03/01/07 Reported Assigned Acceptance Value Va lue Limits 3 .0 3.26 0.934-4.51 8 .6 8.85 3.92 -12 .0 5.7 4.65 1.90 -6.43 3.5 2.74 0 .874 -3.85 2.4 2.19 0.828 -3.15 ---,, " " ~ ' ',,.v N>' N N -",' " " ._. ... " N N N N h >,- 3 .9 3 .42 1.53 -4.71 2.4 2 .14 0.932 -3.02 . .. .. ., .. - 7 .9 8 .92 3.25-12.7 Performance Evaluat ion Acceptable Acceptable Acceptable Acceptable __ ~~c_ep!~b!~ __ Accepta ble Acceptable Method Description EPA 8081A EPA 8081A EPA 8081A EPA 8081A EPA 8081A > ... " " .. V N N ., h """-' EPA 8081A EPA 8081A µQi~ ... __ ~ccep!able EPA 808 1A .. -. ¥ N N ,, A " " " ·h ¥ N ,. N N W " ... " " NN NN '" --,-N N > . . , N N -" " " " -, NN • .. ·-. . ' . .. --0050 4,4'-D DE µg/L 9.4 9.42 4.21 -12 .1 Acceptable EPA 8081A 0051 4,4'-D DT ~g/L . 9 .0 7 .74 2.89 -10 .9 Acceptable EPA 8081A -. . .. 0048 Dieldrin ~QI~. 12.2 11 .5 5.66 -15 .6 Accep!able EPA 8081A --. . ... .. ,. ___ ., . -.. ,,.,., . -. -. ..... " ' ¥ ,• N N .. 7540 Endrin µg/L 6 .0 4 .77 1.78-7.20 Acceptable EPA 8081A 7530 Endrin aldehyde µg/L 9.3 7 .29 2.03-11 .2 Ac cepta ble EPA 8081A 7535 Endrin ketone µg /~ 7.7 6 .01 3.30 -8 .71 Accep table EPA 8081A 7510 Endosulfan I µg/L 10.4 13.7 4.19 -20.0 Acceptable EPA 8081A 7515 Endosulfan II µg /L 14.7 16.6 5.02 -21 .9 Acceptable EPA 8081A 7520 Endosulfan sulfate µg/~ 11 .7 9 .12 3.43 -13.3 Accep!able EPA 8081A ·-A ,,A . . . . ... 0052 Heptachlor µg/L 3 .7 3 .35 1.09 -4.63 Acceptable EPA 8081A ... 0078 HepJach!o_r _epoxid e (b~ta) µ91~. 3.3 2 .85 1.37 -4.05 ~~-epta~le EPA 8081A ·-. -. ' . . .. . . . . .. -. 7810 Methoxychlor µg/L 14 .9 13.7 3.72 -21.5 Acceptable EPA 8081 A Oraanochlorine Pesticides 0047 Aldrin µQ/L 3 .0 3 .26 0.934 -4.51 Acceptable EPA 608 -.. --. . . . ... ... -7110 alpha-BH~ -µg /L 8 .6 8 .85 3.92 -12.0 Acceptable EPA 608 7115 beta-B HC µg/L 5.7 4 .65 1.90-6.43 Acceptable EPA608 .. 7105 delta-BHC µg/L 3 .5 2.74 0.874 -3.85 Acceptable EPA 608 7120 gamma-BH C(Lindane) µg /L 2.4 2.19 0.828-3.15 Acceptable EPA 608 7240 alpha-Chlordane µg /L 3 .9 3.42 1.53-4.71 Acceptable EPA 608 7245 gam,ma-C_hlordane µg/L 2.4 2 .14 0.932 - 3.02 Acceptable EPA 608 '. 0049 4,4'-D DD µg/L 7.9 8 .92 3.25 -12.7 Acceptab!e EPA 608 .. ... ... ··-0050 4,4'-DDE µg /L 9 .4 9.42 4 .21 -12.1 Acceptable EPA608 0051 4,4'-DDT . _yQI L 9 .0 7 .74 2.89 -10 .9 Ace:_e ptab_le EPA 608 ....... -,. N N N A A" " -N N N N . """"""""' ------. .. ""'" ----.... ,, ........... -.. . --. 0048 Dieldrin µg/L 12.2 11.5 5.66 -15.6 Acce ptable EPA 608 . . . .. 7540 Endrin µg/L 6.0 4 .77 1.78-7.20 Acceptable EPA 608 ....... 7530 E_n_d_ri ~ _a!~e_hy9e Y Q'~--. 9 .3 7.29 2.03 -11 .2 Acc_epta_bl~ E PA 608 .. . . ____ .... "¥," N N N" " ............... ,, A" 'll NNN h" .. .. .. " ..... .. .. . . .. 7535 Endrin ketone µg/L 7.7 6 .0 1 3.30 -8.71 Acceptable EPA 608 .. 7510 Endosulfan I µg /L 10.4 13 .7 4 .19-20 .0 Acceptable EPA 608 7515 Endosulfan II µg/L 14 .7 16.6 5.02 -21 .9 Acceptable EPA 608 . . . .• . 7520 Endosulfan sulfate µg /L 11 .7 9.12 3.43 -13 .3 Acceptable EPA 608 0052 Heptachlor µg /L 3 .7 3.35 1.09 -4 .63 Acceptable EPA 608 0078 Hepta.ch!o_r epoxide . (bet_a) µg/L 3 .3 2 .85 1.37 -4 .05 Acceptable EPA 608 .. -- 7810 Methoxychlor µg/L 14.9 13 .7 3.7 2-21 .5 Acceptable EPA608 Page 11 of 18 All analytes are inclu ded in ERA's A2LA accreditation . Lab Code: 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 ANnal. Analyte o . Chlordane I 0053 !Ch lordane , technical Chlordane Chlorinated Acid Herbicides 8505 Acifluorfen --· . 8530 Benta zo n ... A ,-A A A • ... .. . . 8540 Chloramben 8545 .. . . ••ttA A 2,~·!J. -.•.•.... .,. " N N N -~ -,. • " ll N N N A W -,. -,. -,. 8560 2 ,4-DB . . . 8550 Dacthal diacid (DCPA) 8555 Dalapon .. A .,• 8595 Dicamba 8600 3,5-D ic hlorobenzoic acid - 8605 Dic ~l'?rprop .. 8620 Dinoseb . . 7775 MCPA . . . . . . .. 7780 MCPP ' N -' .. -,. .. .. NN .... , . -......... ----V N N N A A ... 6500 4~Nitropheno l 6605 Pentachlor?phenol -.. 8645 Picloram .. ... ··-.. ....... _ ...................... . --- 8655 2,4 ,5-T 8650 2,4 ,5-TP (Silvex) WP-144 Final Complete Report EPA ID : ERA Laboratory Code: TX01484 A116001 03/22/07 Report Issued : Study Dates: 01/15/07 -03/01/07 Units Reported Assigned Acceptance Performance Method Description Value Value Limits Evaluation µgll 11.6 14 .0 5.25-20 .2 Acceptab le EPA8081A µgll 11 .6 14 .0 5.25 -20 .2 Acce ptable EPA608 µgll 20.5 21 .7 2.17 -39 .3 Acceptabl e EPA8081A µgll 20.5 2 1.7 2.17 -39 .3 Accepta ble EPA 608 ~gll 0.00 Not Reported .. µgj~ 9.69 0.969 -18 .9 Not Re[?orted . . . . . ... µQIL 0.00 Not Reported • • -~QI~ .. -4 .9 6 .96 0.696-11 .2 •• ll~c_ep!~bl E: • EPA 8151A --""'"""" 'A A""""• ''"NA. . .. µgll 7 .6 8.18 0.818 -15 .7 llcceptable EPA8151A µgll 2 .82 0.419 -4.89 Not Reported µgll < 1.0 0 .00 Acceptable EPA 8151A . . . . . . µgl l 2.0 2 .65 0.265 · 4 .06 llcceptable EPA 8151A µgll 9.48 2.82 -14.0 Not Reported -~gl~ < 1.0 0.00 Acceptable EPA8151A .. . ... . . µg_lL 1 .5 3.80 0.380 -5.96 Acceptable EPA8151A ... ~gll < 50 0.00 . llcceptab_lE: EPA8151A .. .. . . .. -~QI~. < 50 12 .8 0.00 -34.7 _N_oJ ~~~E;~t~?l_e . EPA8151A . ' ---. -.. N A A --. ..... .. . . .. . . ., .. µgll < 1.0 0.00 Acceptable EPA 8151A µg l~. < 0 .05 0.00 Acceptable EPA8151A .. . .. ~gl~---0.20 0.00 NoJ ~~cf:l~ta?l_e . EPA 8 151A ·-· ' ... --• y .... -• ... __ ,_ . . ,., .. --· . µgll 4.0 4.72 0.472 -7.08 Acceptable EPA8151A µgll 4 .1 4.47 0.541 -6 .62 Acceptable EPA8151A Page 12 of 18 All analytes are included in ERA's A2LA accreditation. Lab Code: 1539-01 Tamara Welch Qual ity Assurance Officer Accutest G u lf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 ANna l. Ana lyte o . Base/Neu trals 5500 Ac_enaphthe~e '. 5505 Ac!'l~~p~t~yl~~f:l . _ ._, -,._ .. --N N N ff N ----~ ff N ,, ' 5145 2-Ami no-~ -rriethylbenzen!'l (o :tolu~d in e) '' 5545 Aniline . ' '. y y ' -,, ' 5555 Anthrace ne ----. . , Y N N N .,_,. .... -..._ N Y "'N N 'N -..._ .,,,,,.,,.,,.,,,.,_ ..... , ,. """'"' 5595 Be nzidine 5575 Benzo(a)anth racene 5585 Benz<;J (b )fluora nthe~e ,., 5600 Benzo{k)fluoranthene 55 90 Benzo(g ,h ,i)perylene 5580 Be_n~<;1(a)eyr~~e .. ----'" 'ON ----... N N N 5630 Benzyl alco hol 5660 4-Bro_m~p_henyl-phe_nylether . 5670 Butyl~e~z_Yl p_hth~lat!'l ---. ... . -.. 5680 Carb azo le 5745 4-Chloroaniline -•• ,, N N • -' . -' .. 5760 bis(2-Chloroet hoxy)methane .. 5765 bis(2-Chloroethyl)ether 57 80 bis (2 -Chloroisopropyl)ether 579 0 1-Chloronaphthalene 57 95 2-Chloronaphthalene 582 5 4-Chl_?~op_h!'lnyl -p~enylether -- 5855 Chrysene 5895 Dibenz(a ,h)an th racene WP-144 Final Complete Report Uni ts µg/L -~QI~ . - µg/L '. ~g/~ -. -~QI~ •.. µg/L µg/L . µg_i ~ µg /L µg/L -yg_l L .. µg/L µg/~ µg/L __ _µg/L ~QI~ .. µg/L µg/L µg /L µg/L µg/L -µQ i~ µg/L µg/L EPAID: ERA Labo ratory Code : Report Issued : TX01484 A116001 03/22/07 Study Dates: 01/15/07 -03/01/07 Repo rt ed As si gned Acce ptan ce Va lu e Va lue Limits <5 0.00 16 20 .1 7.09 -26.4 ' --"' ,, y N N .v N N -< ----YNHN 128 25.3 -172 <5 0.00 " 20 .5 28 .2 12.4 -37 .0 , N N N ~ • -.. "' ,. ff N N .•.• , N ..._ Y. -y y N N N • -' < 20 0.00 14 15 .9 6 .67 -21 .0 18.5 23 .9 7.43 -34 .0 - <5 0.00 <5 0.00 19.5 23 .9 7.56 -33 .0 --'. -,_ - <5 0 .00 31 .8 38 .5 13 .8 -53 .2 101 149 30.5 -210 .. '_, . 45.8 55.5 32.0 -80 .2 <5 0.00 --'' .. 42.3 64 .0 25 . 1 -76 .9 13.9 18 .5 6.90 -26.9 59 .6 80 .2 20 .6 -99.2 0 .00 <5 0 .00 68 .9 92 .2 34 .7 -115 -- 13.2 17.3 7 .98 -25 .9 23.9 28 .5 7.42 -42 .3 Performance Evalua ti on Acceptable __ ~cc_eP!<:b_lE: __ t:J()t Report1:d ... ~cceptable __ ~~c_eP!<:ble ... Acceptable Acceptab le Acceptab le Acceptable Acceptable • ~cc_ep!ab lE: . _ Acceptab le . Acceptable Me t hod De sc r iption EPA 8270C EPA 8270C -y N N ff - EPA8270C EPA 8270C Y N N .Y • -.... - EPA 8270C EPA8270C EPA 82 70 C EPA 8270C EPA8270C EPA 8270C EPA8270C EPA8270C EPA 8270C ~~cep!a.ble '' Acceptab le EPA8270C Accepta bl e EPA 8270C ~cceptable EPA8270C Acceptab le EPA8270C Acceptable EPA8270C Not Reported Acceptable EPA 8270C Acceptable EPA 8270C Acceptable EPA 8270C Acceptable EPA8270C 5905 Dibenzofuran ... -~QI~ 9 1.2 121 42 .0-149 . _ .i:,ccep!a_blE: . EPA 82 70C -----y ----............. ---..... ------·. -.. ,._..._NY NN N N • ..._ ,._ ,._ ,._ Y. ~ N•• N •..• ..._,._ .. <,.y ,. 5925 Di :n-~uty lph~ha l~tEl ~g/~ 78 .4 97 .6 32.0 -128 Accepta_ble EP A 8270C -' . ' .. -. . -' - 4610 1,2-D ichlorobenzene µg/L 42 .2 64.1 6 .87 -79 .0 Acceptab le EPA 8270C , NY Y. Y. •• -· y, ff Y • u y .,,,. ' -. ' . ' -.. ' 46 15 1,3-D ichlorobenzene µg/L 31 .8 48.6 6 .58 -58 .6 Accep!ab}f: __ . EPA 8270C .. ··-YNNN •· • ..._..,,._ . -,,., ... .. ~ N N N N"' ..._ ----... ...... y y -,._,._ -...v N .. ' -. 4620 1 ,4-Dichlorobenzene µg/L 86.3 -128 12.8 -151 Acceptab le EP A 8270C 5945 3 ,3'-Dichlorobenzidine µg/L < 10 0.00 Accepta bl e EPA8270C 6070 Diethylphthalate µg/L <5 0.00 . ' Accept ab le EPA 8270C 6135 Dimethylphthalate µg/L <5 0.00 Acceptab le EPA 8270C Page 13 of 18 All ana lytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 WP-144 Final Complete Report Tamara Welch EPA ID: TX01484 Quality Assurance Officer ERA Laboratory Code: A116001 Accutest Gulf Coast Report Issued: 03/22/07 10165 Harwin Dr Study Dates: 01/15/07 · 03/01/07 Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte Units Reported Assigned Acceptance Performance Method Description No. Value Value Limits Evaluation Base/Neutrals Continued 6185 2,4-Dinitrotoluene µgt~ 39.3 49.4 17.0-64.1 Acc_eptable EPA 8270C , •• y ', 6190 2 ,6-Dinitrotoluene • _µQI~. 71.8 90.6 37.3-114 ... A,c_c_eptable EPA 8270C ¥ N N N N ,-V. V. " ¥ p N ll N N V, v, • v, " N N ·-y. Y, v, y ,, .·, ... . . 6200 Di-n-octrlp~thalate µg/L 59.2 103 22 .5 -152 Acceptable EPA 8270C 6255 b!~(?-Eth~l~e_xyl)phthalat~ . µg/~ 51.9 68 .6 20.6 -96.5 . i:-cceptable EPA 8270C ... 6265 Fluoranthene •.• ~QI~ •.• 30.2 40 .3 18.9 -52.4 __ i:-~c_ep!a_b}e EPA8270C S v,v, v,y N h N N N N N a "V. V, -N " N N " " 'N V. V, " V, Y N N N """"'"" ""' ...... ,..,..,.. ... _ """" y -""""" ---· ....... """ "'· " ___ ... _, 6270 Fluorene µg/L 98.4 131 57.8 -154 Acceptable EPA8270C 6275 Hexachlorobenzene ... _µg/L .. <5 0.00 .. i:-c_c_ep!able_ EPA 8270C 4835 Hexachlorobutadiene . ••• ~QI~. <5 0.00 _ • i:-cc_ep!a_b}e_ •.. EPA 8270C , Nn p-, "'"" "·""""""'"··""'""•" """"" ....... ,.." ... ......... ·'"" .. 6285 He xach lorocyclopentadiene µg/L <5 0.00 Acceptable EPA8270C 4840 Hexachloroethane µg/L <5 0.00 Acceptable EPA 8270C 6315 lnde_noJ1 ,2 13-cd.)pyr_e_ne ~QI~ .... 25.4 30.5 4.47-44.4 Accepta_b_le EPA 8270C 6320 lsophorone µg/L 37.8 53.1 21.5 -69.4 Acceptable EPA 8270C 6385 2-Met_hylnaphthalene µg/L 28.2 40.2 5.86 -54.1 Acceptab le EPA 8270C 5005 Nap_hthale_~e µg/L 34.3 43.6 13.6 -54.9 Acceptable EPA 8270C 6460 2-Nitroaniline µg/L <5 0 .00 Acceptable EPA 8270C 6465 3-Nitroaniline µg /~---<5 0.00 Acc_eptable EPA 8270C """ • y YN ,. 6470 4-Nitroaniline µg/L <5 0.00 Accep!a ble EPA 8270C .. . .. 5015 Nitrobenzene µg/L 49.5 63.5 20.3 -78 .7 Acceptable EPA8270C ..... 6525 N-N)trosodiethylamin_e . ~g/L 72 97.3 19.8 -107 . A,cc_epta_ble EPA 8270C .. 6530 N-Nitrosodimethtl;;imine_ µg/L 58 .5 109 10.9 -129 i:-cceptable EPA8270C 6535 N-Nitrosodiphenylamine .. µg/L <5 0.00 Acceptable EPA 8270C 6545 N-Nitr~so:ci.i-_n-er.opyla~ine_ .. -~Q'~-. <5 0.00 A,ccep!a_b]e EPA 8270C 6590 Pentachlorobenzene . ~Q/L 45.5 58.8 11 .6 -78 .8 Acceptable EPA 8270C 6615 Phenanthrene µg/L 97 116 53 .2-139 Acceptable EPA 8270C 6665 P_yre_ne_ .. _ • _ ... .YQ'~-<5 0 .00 Accep!a_ble_ EPA 8270C 5095 Pyridine µ9-:IL __ <5 0.00 Acceptable EPA 8270C . 6715 1 !2 ,1,_5-T ~t~achlorobe~z_e!1~. µ9-:/L <5 0.00 Acceptable EPA 8270C .. 5155 1,2,4-Trichlorobenzene µg/L <5 0 .00 Acceptable EPA 8270C Page 14 of 18 All analytes are included in ERA's A2LA accreditation. Lab Code: 1539-01 Tamara Welch Qual ity Assurance Officer Accutest Gu lf Coast 10165 Harw in Dr Suite 150 Houston , TX 77036 713-271-4700 ANna l. A nalyte o. Base/Neutrals 5500 Acenaphthime 5505 J\cenapht~ylene ---. .. . ·- 5145 2-Amino-1-methylbenze_ne (o-toluidine) . . 5545 An il ine 5555 Anthracene ' .... -" y .. ,. N " ' A " y .... ,.,,. " v ... " Y N N H N N" .,._ .,._ , Y N ll ll 5595 Benzidine 5575 Benzo (a)c1nt~racen~. . . . . .. -. . 5585 Be_nz?(b )fh-!o!c111t~7111: ___ ·-y -" # N ~ .. " ' 5600 Benzo(k)fluora nthe ne 5590 Benzo(g,~,i)perylene y.,' 5580 B.e_n~o(a)p~r7ri~ .... _ .. . . .. . ........ .... .... ,. .. 5630 Benzyl alcoho l 5660 4-Bromophenyl-phenylether 5670 Butylbenzylphthalate 5680 Carbazole 5745 4-Ch loroani li ne 5760 bis(2-Chl~roethoxy)mi:thane 5765 bis(2-Chloroethyl)ether 5780 bis(2-_Chlor?isop~~pyl)~ther . 5790 1-S:~IO(Ona phthali:n_e_ . _ ' • -N 5795 2~Ch loronaphthalene 5825 4:S:hlO(OP_h_e~yl:P.~e_nJ!e_t~er ... -.. AY. ""' ""'" ··- 5855 Chrysene 5895 Dibenz(a ,h)an thracene 5905 Dibenzofuran . 5925 Di-n-b~ty lphthalate 4610 1,2-Dichlorobenzene . 4615 1,3-Dichlorobenzene ,,.._,, ..... .. ... ,v ... "'. . . .. . .. 4620 1,4-Dichlorobenzene .. . . 5945 3,3'-Di chlorobenzidine .. .. . ••• y' • --.. 6070 Dif:thy~htha!at~. ......... . -. . . .. . .. 6135 Dimeth ylphtha late WP-144 Final Complete Report EPA ID : ERA Laboratory Code : Report Issued: TX01484 A116001 03/22/07 Study Dates : 01 /15 /07 -03/0 1/07 Units Reported A ssig ned Acce pta nce Va lu e Val ue Li mits µg/L <5 0 .00 µ!l.'~-.. 16 20.1 7 .09-26.4 . . .. ... '"· .... , ,.. " " -" . . - ~g/~ 128 25 .3 -172 µg/L <5 0.00 ... J!!l.'~-·-20.5 28 .2 12.4 -37 .0 -.. •·"""' .. ...... .... .... .. . µg/L < 20 0 .00 µg/~ 14 15 .9 6.67 -21 .0 . . .. . . .. -~!l_i l 18.5 23 .9 7.43 -34.0 -.. . .. -.. -. . -· ... µg/L <5 0 .00 µg/L <5 0.00 . .. Y!l.'~ 19 .5 23 .9 7.56 -33 .0 ' H N --" ... .. N N NA" """"' .. µg/L <5 0 .00 µg/L 31.8 38 .5 13 .8 -53.2 .. µg/L 101 149 30 .5 -210 .. µg/L 45 .8 55.5 32.0-80.2 µg/L <5 0 .00 ... µg/L 42 .3 64 .0 25.1 -76 .9 µg/L 13.9 18 .5 6 .90-26.9 µg/L __ 5 9.6 80.2 20 .6 -99 .2 µg/L 0.00 . .. -· ... ... µg/L _ <5 0 .00 .Y!l.'~ 68 .9 92.2 34.7-115 ·-' -...... . .. -· ---............ ~g/L 13 .2 17 .3 7 .98-25 .9 ... µg/L 23.9 28 .5 7.42 -42 .3 µgjl 9 1.2 121 42 .0 -149 -... - µg/L 7 8.4 97 .6 32.0 -128 ~g/L 42 .2 64.1 6 .87 -79.0 •. Y!l.'~---31.8 48 .6 6 .58 -58.6 . . . . .. .. .. ... -~g/L 86 .3 128 12 .8 -151 .. ~g/L < 10 0.00 ~!l.'~ •.. <5 0.00 ·-.. ....... ... . . µg/L <5 0.00 Page 15 of 18 . Perfo rma n ce Eva lua ti on Accep!able Accep)able '' .. Not Rep<?rted Acceptable . .. A~c.ep!a_b~f: Acceptable .. Accepta_ble .. . . A~c_eptable - Acceptable Acceptable .. .• i:,cc_ep!ab_le .. Acceptable Acceptable Acc_eptable Acceptable Acceptable Acceptable Acceptable Acceptable N?~ Reported Acceptab le • _ i:,ccep!a_ble . . Acc_eptable Acceptable .. __ i:,cc_epta_b_le Acc_e_pta_ble Acceptable Accepta_ble . Acceptable Acceptab le Acceptable Acceptable Method Descripti on EPA 625 EPA 625 EPA 625 EPA625 .. EPA 625 EPA 625 EPA625 EPA625 EPA 625 EPA625 . ... NNNN a""" EPA625 EPA 625 EPA625 EPA 625 EPA625 EPA 625 EPA 625 EPA 625 EPA625 EPA 625 . EPA625 EPA625 EPA625 EPA625 EPA 625 EPA625 EPA625 EPA 625 EPA625 EPA 625 All analytes are included in E RA's A2LA accreditation . Lab Code : 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 Anal. Analyte No . Base/Neutrals {Continued) 6185 2,4-Dinitrotol uen e • '" ¥ a V •• "N v,• • 6190 2,6-Dinitrotoluene ¥ A" # -.... " y N N • -" .. " ~ N N ... A· ... 6200 Di-n-octylphthalate 6255 bis(2-Ethylhexyl)phthalate 6265 Fluoranthene -.. ·-•A·A V VNN 6270 Fluorene 6275 Hexachlorobenzene 4835 Hexach lo ro butadiene ... ",.,,._ -· N ,. ,, " -" " ¥," # N N N # 6285 Hexachlorocyclopentadiene 4840 Hexachloroe thane A"., y . -· . -- ""·" - --y """ . . -.. .. -" .. . . 6315 l~~E:_n_oJ ! ,?~3:~~)ptr_e.!1~ . .. """" "" -V 6320 lsophorone 6385 2-~et_hylnap~tha!ene ... - 5005 Napht~alE:ne .. .. 6460 2-Nitroaniline 6465 3-Nitroan ilin e 6470 4-Nitroaniline 5015 Nitrobenzene 6525 N-Nitrosodiethylami_ne 6530 N-Ni trosodimethyl~m!ne ... .. 6535 N-Nitrosodiphenylamine 6545 N-~itr~s_o:~i-_n:r:_>r_optl_a~i ~E: . ___ ,,..,,,. .... v N N N A • " .. " 6590 Pentachlorobenzene .. . .. ... 6615 Phenanthrene 6665 . _Py!e~E:_ --. . --.. " . -"" ...... . . -· . .. 5095 Pyridine . ' - 6715 1,2 ,4 ,5-Tetrachlorobenzene 5155 1,2 ,4-Tri c hlorobenzene WP-144 Final Complete Report EPA ID: ERA Laboratory Code: Report Issued: Study Dates: TX01484 A116001 03/22/07 01/15/07 -03/01 /07 Units Reported Assigned Acceptance Value Value Limits Performance Evaluation Method Description µg/L 39.3 49 .4 17 .0 -64.1 Acceptable EPA 625 ·--•• "" y .. µQI~ ... 71.8 90 .6 37 .3-114 Ae:cep!ab le EPA625 --• .. N A" ·N • -.. --.. "" """' --. .. µg/L 59.2 103 22 .5 -152 Acceptable EPA625 µg/L 51.9 68.6 20 .6-96 .5 Acceptable EPA625 -•. y .. ". -~!l'~ 30 .2 40.3 18 .9 -52.4 Ae:c_ep!~ble EPA625 ,,.,, " .. .. . . .. , . " --___ ,.,,.,, .v. "' "'" .. -- µg/L 98.4 131 57 .8-154 Acceptable EPA625 µg/L <5 0.00 Acceptable EPA 625 -~g/~. <5 0 .00 Acceptable EPA625 -. "'" ··-"""·"" '"·""" . .... µg/L <5 0 .00 Acceptable EPA 625 µg/L <5 0 .00 Acceptable EPA 625 ... -. YQ'~-.... 25.4 30 .5 4.47 -44.4 . -~cc_ep!ab_l~ .• EPA625 N # A " -A " " " .. ,.,, -· '""""" NN N, • ... .. µg/L 37 .8 53 .1 21 .5 -69.4 Acceptable EPA 625 ,. µg/L 28.2 40.2 5.86 -54 . 1 Acceptable EPA 625 . .. '"., .. ~g/L 34 .3 43.6 13 .6 -54 .9 Acceptable EPA625 .. . . -'. ·--.---· µg/L <5 0.00 Acceptable EPA625 µg/L <5 0.00 Acceptable EPA625 µ!l/L <5 0 .00 Acceptable EPA 625 µg/L 49 .5 63 .5 20 .3 -78 .7 Acceptable EPA 625 µg/~ 72 97.3 19 .8 -107 Acceptable EPA625 µg/L 58 .5 109 10.9 -129 Acc_eptable EPA 625 . . . . µg/L <5 0 .00 Acceptable EPA625 µQI~ -.. <5 0.00 Acceptable EPA 625 . ·-" " V y , V ", .. --· ----. ~g/L 45 .5 58 .8 11 .6 -78 .8 Acceptable EPA 625 .. µg/L 97 11 6 53.2 -139 Acceptable EPA 625 .. )!Qi~ <5 0 .00 Acceptable EPA 625 . . .. .. '. ~g/L <5 0 .00 Acceptable EPA 625 yg/L <5 0 .00 Acceptable EPA 625 .. µg/L <5 0 .00 Acceptable EPA625 Page 16 of 18 All analytes are included in ERA's A2LA accreditation. Lab Code : 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 Ana l. Analyte No. Acids 5610 Benzoic acid -··. y ._ • . . . •• , --y .. ·-. 5700 4:S:~l_o :~-~:m~thylp~l:~<?1 .•. __ .. --h . _,.._,,,_ . 5800 2-C~lorop_he~ol .. . . . 6000 2,4-Dich)orol)~en_ol 6005 2:6-l)!ch!C?r?p~~n_o_l _ •. --N A y --• • -N N ' 6130 2,4-Dimethylph enol 6360 4 ,6-Din itro-2 -m ethy lphenol 6175 2 .~-,0in_it r9~he_no! .. . ... -. --,, - 6400 2-Methylphenol 6410 4-Methylphenol . - 6490 WP-144 Final Complete Report Un its . ~Q_/L . . .. ~Q_/L -. µ\fl .... ~glL . . µQI~ ...•. µgll µgll ••• ~QI~ µgll ~gll EPA ID: ERA Laboratory Code: Report Issued: TX01484 A116001 03/22/07 Study Dates: 01/15/07 -03/01/07 Reported Assigned Acceptance Value Value Limits < 10 0 .00 . .. 97 .3 128 50 .0 -164 •u N . .. ' ---. 111 158 44 .6 -198 98 .7 131 42.6 -161 175 61.3-216 ,V NA A'> ,. •. , . ·---' 53 .4 68.4 13.0 -90 .7 104 130 44 .4 -184 .. 80.4 120 12 .0 -169 .. ... -------·· ., --. --" 59 74.1 14 .0 -92 .7 83 .5 109 10.9-141 117 154 35 .0 -202 Performance Evaluation Acceptable Accepta_ble Acceptable Acceptable , .. , . No! Rep<?rtE:d Acceptable . Acceptab)e . . •. ~e:cep!<:bl~ _ • Acceptable Acceptab_le Method Descr iption EPA 8270C EPA 8270C EPA 8270C EPA8270C .. EPA 8270C EPA 8270C EPA 8270C -··-·· -.. . EPA8270C EPA8270C EPA 8270C -----2:~iJr_op h~~~I -.• . ----... . y y N N N ' ---µg_l~ . --·· -... .. ... .. Acc_eptable . 6500 4-Nitrophenol µg/L < 25 116 11 .6 -157 Not Acceptable EPA8270C 6605 P_entac_hlor?pheno} ~gl l 42.8 74.5 17 .3 • 103 Acceptable EPA8270C -. . . ... .. -· .. 6625 Phenol µgll 41.4 151 15 .1-202 Acceptable EPA 8270C . --. . .. .. 6735 2,3 ,4,6-Tetrachlornphenol µgll 30.6 46 .7 4 .67 -63 .8 Acceptable EPA 8270C . 6835 2,4. 5: T richlo_ro~hen_ol µQIL 57.7 79 .1 29 .1 -103 Acceptab.le EPA8270C .. . .. -.. 6840 2,4 ,6-Trichlorophenol µgll 98.8 130 41.6 -162 Acceptable EPA8270C Acids 5610 Benzoic acid µg/L < 10 0 .00 Acceptable EPA 625 ... . . 5700 4-C~lo'.~-3:met~ylph1:nol µQI L 97 .3 128 50.0 -164 Acceptab!E: EPA 625 ... . . ,. ----. --. .. . .. ,.,, .. . .. .. -. 5800 2-Chlorophenol µgll 111 158 44 .6 -198 Acceptable EPA 625 6000 2,4-D ic.hlorophenol µgll 98 .7 131 42 .6 • 161 Acceptable EPA625 . .. ... 6005 2,~-l)ichl(!r?phenol µgll 175 61.3-216 Not Reported .. _, . -.. 6130 2,4-Dimethylphenol µgll 53.4 68.4 13.0 -90 .7 Acceptable EPA 625 -. ... 6360 4,~-Din_itr~:2~methylphenol. . µQIL . 104 130 44.4 -184 Acceptable EPA 625 .. . . ,. . . ,, -. 6175 2,4-Dinit_ro~~e_nol .. ~gll 80.4 120 12 .0 -169 Acceptable EPA 625 . ··-. . .. .. .. . , 6400 2-M ethylphenol µgll 59 74.1 14.0-92 .7 Acceptable EPA 625 6410 4-Methylp_h_enol µgll 83 .5 109 10 .9 -141 Acc_eptable EPA 625 .. 6490 2-Nitrophenol µgll 117 154 35 .0-202 Acceptable EPA 625 . 6500 4-Nitrophenol µgll < 25 116 11 .6 -157 Not Acceptable EPA 625 6605 Pentachlorophenol ~gll 42.8 74.5 17.3 -103 Acc_ep!abl~ EPA625 . --.. . ·---. 66 2 5 Phenol µgll 41 .4 151 15 .1-202 Acceptable EPA625 6735 2 ,3,4,6-Tetrachlorophenol µgll 30.6 46 .7 4 .67 -63 .8 Acceptable EPA 625 .. 6835 2 .~,?-.Tri_c~lo:o~h_en_o( ..• -~QI L 57 .7 79.1 29 .1 -103 ~cceptable EPA 625 .. . ,,_,,_ ··-·"·""" ... .. .. .. .. -. . .. . 6840 2,4, 6-Trichlorophenol µgll 98 .8 130 41 .6-162 Acceptable EPA 625 Gasoline Range Organics (GRO) in Water 9408 G':solin_e R_a~ge Organics (GRO ) µgll 3170 2480 963 -4380 Acceptable EPA8015B 4375 Benzene in GRO µg/L 15.6 6 .73 -26 .2 Not Reported 4765 Ethylbenzene in GRO µgll 68.7 39 .2-96.0 Not Reported 5140 Toluene in GRO µgl ~ 194 103 -259 Not Reeorted -. .. --·. -· ····· ... ... •. "A ··-.. . A A A --- 5260 Xylenes , total in GRO µgll 276 157 -373 Not Reported Page 17 of 18 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 anics DRO in Water 9369 Diesel Range Organics (ORO) BTEX & MTBE in Water 4375 Benzene 5000 tert-Butyl methyl ether (MTBE) .. . _4_7_6_5_ . _Et~}'.1~~~2:_e_n~. . • •••... _ •••••. _ ••• 5140 Toluene > ---= 0 > S N ll h O • > 5260 Xylenes, total BTEX & MTBE in Water 4375 Benzene 5000 tert-Butyl methyl ether (MTBE) 4765 E_thylbenzene 5140 Toluene 5260 Xylenes , total Texas Low-Level Fuels TPH in Water 2050 Total Petroleum Hydrocarbons Texas Hi h-Level Fuels TPH in Water 2050 Total Petroleum Hydrocarbons . . . WP-144 Final Complete Report EPA ID: ERA Laboratory Code: TX01484 A116001 03/22/07 Report Issued: Study Dates: 01/15/07 -03/01 /07 Units Reported Assigned Acceptance Performance Method Description Value Value Limits Evaluation µg/L 1910 3200 781 -4130 Acceptable EPA8015B -~g/~-69.202 74 .1 53 .9 -93.7 Acceptable EPA 80218 ... -ll •• - .. _µg/L 51 .021 55 .3 34.8 -78 .0 Acceptable EPA 80218 .. -~!!1~ -. -16 .276 16.3 10.9 -21 .5 •. i:-<:c_ep)a_b_lE: •• EPA8021B ·---~N¥Nll' N ,-----ll N hNllNNll ____ vv, "ll-----ll ll ~ , µg/~ 64.553 66.0 45 .8 -82 .6 Acc_ep!a_ble EPA8021B •llllo> 0 --... µg/L 109.542 112 63 .9-151 Acceptable EPA 80218 µg /L 69.202 74 .1 53 .9 -93.7 Acceptable EPA 602 µg/L 51 .021 55 .3 34 .8 -78 .0 Acceptable EPA602 µ9,/L 16.276 16.3 10.9-21 .5 Accep!able EPA602 .. µg/L 64 .553 66 .0 45 .8 -82 .6 Acceptable EPA 602 µg/L 109.542 112 63 .9-151 Acceptable EPA 602 mg/L 5 .76 6.59 0.659 -9 .69 Acceptable TNRCC 1005 mg/L 56.3 63 .1 6 .31 -90 .8 Acceptable TNRCC 1005 Page 18 of 18 All analyte s are included in ERA's A2LA accreditation . Lab Code : 1539-01 -~!,~ ENVIRONMENTAL Vi1 RESOURCE ASSOCIATES ® Study: WP-138 ERA Laboratory Code: A 1160-01 Laboratory Name: Accutest Gulf Coast Report Type: Complete Report Method: Method A Page 2 of 26 ~1,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. pH 0019 pH Hardness 0072 Non-Filterable Residue (TSS) --------------------- -- 0023 Calcium -- -- ----------------- ------ - 0024 Magnesium ----------------------- 1550 Calcium Hardness (CaC03) ----------------------- 0022 Total Hardness (CaC03) Demand 0038 BOD ----. --.. ----------------·- 0102 CBO D -- ------------------------- 0036 COD ---------------------------- 0037 TO C Simple Nutrients 0031 Ammonia as N --------------------------- 0032 Nitrate as N ---------------------------- 1820 Nitrate + Nitrite as N -- -------------------------- 0033 Ortho-phosphate as P Complex Nutrients 0034 ::r~t~l_ l9~l~a_h! ~i!r~~e_n _________ . 0035 Total phosphorus as P Total Cyanide 0071 Cyanide , total Total Phenolics (4-AAP) 0097 Phenolics , total Oil & Grease 0104 Oil & Grease (Gravimetric) ------------------------ 1860 Oil & Grease (Infrared) Total Residual Chlorine 0098 Total Residual Chlorine WP-138 Final Complete Report Units Reported Value s.u. 6 .65 mg/L 35 -------------- mg/L 42.198 -------------- mg/L 7.023 -------------- mg /L 112 -------------- mg /L 120 .0 mg /L 134 -------------- mg/L 100 -------------- mg /L 143 -------------- mg/L 61.3 mg /L 12 .1 -------------- mg /L 20 .7 -------------- mg /L 20 .7 -------------- mg /L 4.67 mg /L 23 .5 -------------- mg/L 2 .6 mg /L 0.378 mg /L 0 .2760 mg/L 50 .05 EPAID: ERA Laboratory Code: TX01484 A1160-01 Report Issued: 09/21/06 07/17/06 -08/31/06 Study Dates: Assigned Acceptance Warning Performance Value Limits Limits Evaluation 6 .70 6 .50 - 6 .90 Acceptable 76.3 62 .0 -85 .2 65 .9 -81 .3 Not Acceptable ------------------------------------ 41 .5 37 .0 -47 .2 38 .7 -45 .5 Acceptable ----------------------------------- 6 .73 5.69 - 7 .70 6.02 - 7 .36 Acceptable ----------------------------------- 104 92 .7-118 _ Acceptable _ ------------------------- 131 116-150 121 -144 Check for Error 102 51 .5-152 68 .3 -135 Acceptable -------------------------------- 87 .6 39.3 - 136 55.4 -120 Acceptable ---------------- ------------------- 164 126-187 136 -177 Acceptable ----------------------------------- 64 .9 54.2 -74 .7 57 .6-71 .3 Acceptable 13 .1 9.74 -16 .3 10 .8 -15 .2 Acceptable ----------------------------------- 22.3 17.4 -26.9 19.0 -25 .3 Acceptable ----------------------------------- 22 .3 18 .2 -25 .9 Acceptable ------------------------------------ 4.73 3.91 -5.59 4 .19 - 5 .31 Acceptable 25.4 16 .7 -32 .6 19 .4 -30.0 Acceptable ----------------------------------- 2 .59 2.09 - 3 .14 2 .27 - 2 .97 Acceptable 0.370 0.200 -0.545 0 .258 -0.488 Acceptable 0.383 0 .205 - 0.561 0 .264 -0 .501 Acceptable 65.0 43.8 -77.6 49.4 -71 .9 Acceptable ------------------------------------------------- mg/L 80.0 55 .5 -94 .1 mg /L 0 .90 0 .937 0.676 - 1.17 0.758 -1 .09 Acceptable Method Description EPA 9040B EPA 160 .2 ------------- EPA 6010B ------------- EPA 6010B ------------- EPA 130.2 ------------- EPA 130.2 EPA405.1 - - .. - - SM 5210 B ------------- EPA410.4 ------------- EPA 415.1 EPA 350 .1 ------------- EPA 353 .2 ------------- EPA 353 .2 ------------- EPA 365 .2 EPA 35 1.2 ---------·---- EPA 365 .2 epa 335 .3 EPA420.2 epa 1664 ------------- EPA 330 .5 All analytes are included in ERA 's A2LA accred itation . Lab Code : 1539-01 Page 3 of 26 I i,~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Trace Metals WP-138 Final Complete Report EPAID: ERA Laboratory Code: TX01484 A1160-01 09/21/06 Report Issued: Study Dates: Units Reported Assigned Acceptance Value Value Limits 07/17/06 -08/31/06 Warning Limits Performance Evaluation Method Description 0001 Aluminum µg/L 380.65 300 219 -385 246 -357 Check for Error EPA 601 OB ---·-------------·-----------· ------------------------------------------------------------ -~~1~ _ !'-~~n:,o_ny _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ':'_9~L-___ 3~~-~6-____ 1J~ __ . _ } ~~-:_ ~4_0 ____ !~7--_23! ____ A~~_P!a_b~e _ _ _ ~PA 601 OB 0002 Arsenic ------ -- - -------- - ---------- - __ ':'_9~L-___ ~~~-~1-____ BJ? __ . _ !~~-:_ ~7_8 _ _ _ ?5_0_-_9}~ ____ A_C~_P!a_b~e-____ ~~A 601 OB 1015 Barium µg/L 2095 .3 2020 1750 -2280 Acceptable EPA6010B --------------------------- 0003 Beryllium µg/L 742.78 726 618 -820 652 -786 Acceptable EPA 601 OB -------------------------------------------------------------------- 1025 Boron µg/L 1165.4 879 ---------------------_ ?~8--_1 _o~~ _ _ ________ Not Acceptable ___ ~~~ ~~1_o~ __ _ 0004 Cadmium µg/L 568.48 581 496 -660 523 -632 Acceptable EPA 601 OB ------------------------------------------0006 Chromium µg/L 660.09 663 578 -750 606 -721 Acceptable EPA 601 OB ------------------------------------------------------------------------------------------- 0005 Cobalt µg/L 457.61 446 391 -500 410 -482 Acceptable EPA 6010B -------------------------------- 0007 Copper µg/L 707.99 703 633 -773 661 -749 Acceptable EPA 6010B ------------------------------------------------------------------------------------------ 0008 Iron µg/L 890.39 849 749 -960 785 -925 Acceptable EPA 6010B ------------------------------------------------------------------------------------------- 0012 Lead µg/L 772.06 760 665 -852 696 -821 Acceptable EPA 6010B ---------------------------------------- 0010 Manganese µg/L 508.46 488 437 -542 455 -525 Acceptable EPA 601 OB -----------------------------------------------------------______________ ,. ________ _ 0074 Molybdenum µg/L 579.11 566 481 -645 509 -618 Acceptable EPA 6010B --------------------------------------------------------------------------------- 0011 Nickel __ ':'_9~L-___ J~~-~1-____ 9~~ __ . _ ~6_6_-_1g?~ ___ 9_0~ ~ ~~4_0 ____ A_c~e_P!a_b~e _____ ~~~ ~~1g~ __ _ 0013 Selenium ----------------------------0017 Silver 0075 Strontium ---------------------------- 0018 Thallium 0014 Vanadium 0015 Zinc Mercury 0009 Mercury Minerals µg/L 1047.3 1020 --------------------- µg/L 107.16 106 ---------------------µg/L 57.8 60.4 --------------------- µg/L 232.97 226 µg/L µg/L µg/L 234.46 1178 .7 27.5 228 1120 26.4 .. ~~27 _ !\~k~l~n!t~ ~~ ~~~~3-_____________ n:19!~ _____ 5_:i :33 ____ _:i~-! __ 0028 Chloride mg/L 81 92.2 811 -1180 872 -1120 Acceptable EPA 6010B ------------------------------------------90.4-122 49 .8 -70.9 ---------165-284 199 -256 963 -1280 16.2 -35.6 _ ~5~6--_ 1_1.? ____ A_c~_P!a_b~e _____ ~~~ ~~1_o~ __ _ 53 .3 -67.4 Acceptable EPA 6010B -------------------------------- 185 -264 Acceptable EPA 6010B -------------------------------- _ ~~9_-_2_:i~ ___ Acceptable _____ ~~~ ~~1_o~ __ _ 1020 -1230 Acceptable EPA 6010B 19 .5 -32.3 Acceptable EPA 7470A 40 .2 -53.6 42 .5 -51.4 Not Acceptable EPA 310 .1 EPA 325 .3 -------------- ------- ------- --· - 79.1 -105 83 .5 -101 Check for Error _ ~~2_o _ ~.?~~u~~v~t~ ~t_2_5:~ _ _ _ _ _ _ _ _ _ _ _µ~~o~/~n:1 ___ ~~3-_____ 4_:i~ ____ ~~ ~ ~ ~0_5 ____ ~~7--_4~~ ____ A~:e_P!a_b~e-____ ~~~ }~~-! _ _ 0029 Fluoride mg/L 3.56 3.52 2.96 -4.09 3.15 -3.91 Acceptable EPA 340.2 -------------------------------------------------------------------------------------------- 0026 Potassium mg/L 25.616 23.4 19.3 -27.9 20.7 -26 .5 Acceptable EPA 6010B -------------------------------------------------------------------------------------------- 0025 Sodium ---------------------------- 0030 Sulfate 0021 Total Dissolved Solids at 1so·c 1950 Total Solids at 105 °C Hexavalent Chromium 1045 Hexavalent Chromium mg/L 79.86 80.4 --------------------- mg/L 53.49 19.8 mg/L mg/L µg/L 260 225 513 285 305 537 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Page 4 of 26 68.3 -92.1 15.4 -23.7 213-357 264-342 437 -632 72.2 -88 .2 Acceptable EPA 6010B ------------------------------- 16.8 -22.4 Not Acceptable EPA 375.2 -------------------------------- 237 -333 Acceptable EPA 160.1 -------------------------------- Not Acceptable EPA 160.3 Acceptable EPA 7196A I i,\. ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Nitrite 1840 Nitrite as N Turbidity 2055 Turb idity Tin and Titanium 1175 Tin - - --------------------------- 0076 Titanium Units Reported Value mg/L 1 .56 NTU 7 .62 µg /L 3 154 -------------- µg /L 257 .81 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Assigned Acceptance Warning Performance Method Value Limits Limits Evaluation Description 1 .59 1.32-1 .86 Acceptable EPA 353 .2 6 .99 5.84 -8 .00 Acceptable EPA 180 .1 3200 2520 -3900 Acceptable EPA 6010B -----------------------------------------·-------- 249 214 -280 225 -269 Acceptable EPA 6010B Page 5 of 26 I /;\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271--4700 Anal. Analyte No . Volatiles 4315 Acetone 4320 Acetonitrile ---------------------------- 4340 Acrylqnitrile 4325 Acrolein 0065 Benzene 0060 Bromodichloromethane 0062 Bromoform . 4950 Bromomethane 4410 2-Butanone (MEK) ----------------------------· 5000 tert-Butyl methyl ether (M TBE) ---------------------------- 4450 Carbon disulfide 0058 Carbon tetrachloride 0064 Chlorobenzene 0061 Chlorodibromomethane ---------------------------- 4485 Chloroethane 4500 2-Chloroethylvinylether ---------------------------- 0055 Chloroform WP-138 Final Complete Report EPAID: TX01484 A1160-01 ERA Laboratory Code: Report Issued: 09/21/06 07/17/06 -08/31/06 Study Dates: Units Reported Assigned Acceptance Warning Limits Performance Evaluation Method Description Value Value Limits µg /L µg/L µg/L µg /L < 50 < 10 < 10 < 10 0.00 0.00 0.00 0.00 µg/L 46 .9 46.4 --------------------- µg/L 40.3 37.1 µg/L 17 .7 14 .7 --------·-·------------ µg/L < 2 0.00 µg/L < 10 0.00 --------------------- µg/L < 2 0.00 µg/L µg/L <2 77.5 0 .00 74.7 µg /L 104 97 .8 --------------------- µg/L 92.8 81.2 µg/L µg /L µg/L <2 < 10 24.6 0.00 0.00 23.0 33.3 -59.2 26.0-50 .0 8.15 -19.6 40.7 -102 Acceptable EPA 82608 Acceptable EPA 82608 -------------------------------- Acceptable EPA 82608 -------------------------------- Acceptable EPA 82608 -------------------------------- 37.6 -54.9 Acceptable EPA 82608 -------------------------------- 30.0 -46.0 Acceptable EPA 8260B -------------------------------- 10.1 -17 .7 Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B --------------------··----------- Acceptable EPA 8260B ----- - ----- - -------- ---------- --- Acceptable EPA 8260B Acceptable EPA 8260B ------ ----- ------------· --- ------- 50 .9 -91.6 Acceptable EPA 8260B --- ----- --- - - ---------·--- -------- 70 .6-122 79.2-114 Acceptable EPA 8260B ------------------------------------------ 55.7 -108 64.4 -99.2 Acceptable EPA 8260B ----------------------------------------- Acceptable EPA 82608 ----------------------------------------- Acceptable EPA 82608 15.8 -30.6 18.3-28.1 Acceptable EPA 826 08 ------------------------------------------------------------------------------------------4960 Chloromethane µg /L <2 0.00 4570 1,2-Dibromo-3-chloropropane (DBCP) µg /L < 2 0.00 ---------------- --- - - - - ---- - - ------ --- ---- ------- --- 4585 1,2-Dibromoethane (EDB) --------· - ---- ----- - - --------- 4595 Dibromomethane 0094 1,2-Dichlorobenzene µg/L 32.5 28.9 µg /L <2 0.00 µg/L 49.2 52 .8 Acceptable EPA 8260B ------------------------------------------ Acceptable EPA 8260B -------------------------------------------- 19 .8 -39 .9 Acceptable EPA 8260B ------------------------------------------ Acceptable EPA 8260B ----------------------------------------- 36 .5 -68.7 41.9-63.3 EPA 8260B 0096 1,3-Dichlorobenzene 0095 1,4-Dichlorobenzene 4625 Dichlorodifluoromethane Acceptable -- - --------------------------------·----------- ---- - ------- --·-- ---- - ---------------------------- 4630 1, 1-Dichloroethane 0054 1,2-Dichloroethane µg/L 53 .2 49 .7 --------------------- µg/L 92.9 94.0 µg/L µg/L µg/L <2 <2 58 .8 0.00 0 .00 53.2 33.4 -63 .5 38.4 -58.5 Acceptable EPA 8260B 63 .9-117 72 .8-108 Acceptable EPA 8260B -------------------------- ------- -------· -- Acceptable EPA 8260B ----------------------------------------- Acceptable EPA 8260B 36.9 -70.2 42 .5 -64 .6 Acceptable EPA 8260B --------------------------------------------------------------- Acceptable EPA 8260B ------------------------------------------ _ ~~4!i _ _9 i:>-_1 :2.::~i~h~~r?e_t~y~e_n~ _ _ _ _ _ _ _ _ _ _ ~g~L-____ ~2_:~ ____ .?~-~ __ 45 .8 -83.8 Acceptable EPA 8260B _ ~~O~ _ !r~12s~1_.~-~~c~l9~o~~htle_12e_ _ _ _ _ _ _ _ _ ~g~L-____ ~~~ ____ .4~.9 _ _ _ ~8_: ~-:. ~7~~ _____________ A_c~ep!a_b~e _____ ~~~ ~~6~~ __ _ _ ~~5!i _ ~ c2:~i~h~o_r?P!?P_a11e_ ______ .. ___ . __ ~g~L-____ ~~-1_ _____ 8?-~ __ . _ ?~-~ = ! 1_ 2_ _ _ __________ A.9~p!a_b~e-____ ~~~ ~~6~~ __ _ 4680 cis-1 ,3-Dich loropropylene -------- - ------· ------- -------<2 µg /L 0.00 Acceptable EPA 8260B ----------------------------- - ------------------- ------· -------- -·-- _ ~~8!i _ !r~12s :1_,~-~~c~l9~op~op~le_n_e ______ . __ ~g~L-_____ <_2 _____ ~:09 __ . 0066 Ethylbenzene ---------------------------- Acceptable EPA 8260B -----·------------·------------------- µg /L 51 .8 52 .2 --------------------- µg/L < 2 0 .00 ---------------------- µg /L 107 86 .8 35.9 -66 .5 41 .0 -61.4 Acceptable EPA 8260B ----------- ----- ---·----· -- --·-------------- - Acceptable EPA 8260B -------------------·-------------------- 43.7 -127 Acceptable EPA 82608 4835 He xachlorob utadiene ---------------------------- 4860 2-Hexanone -------------------------------------------- 96 .7 µg /L 94.0 57.7-130 69 .8 -118 Acceptable EPA 8260B ----------· ----------------- --- ----------- ------- ----· ---- - ----- All analytes are included in ERA 's A2LA accredi tation . Lab Code: 1539--01 Page 6 of 26 I i,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® WP-138 Final Complete Report Tamara Welch EPA ID: TX01484 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Units Reported Assigned Acceptance Warning Limits Performance Evaluation Method Description Value Value Limits Volatiles (Cont.) 4995 4-Methyl-2-pentanone (MIBK) ---------------------------- 5005 Naphthalene ---------------------------- 5100 Styrene ---------------------------- 5105 1, 1, 1,2-Tetrachloroethane 5110 1, 1,2,2-Tetrachloroethane 0059 Tetrachloroethylene ---------------------------- 0067 Toluene 5155 1,2,4-Trichlorobenzene ---------------------------- 0056 1, 1, 1-Trichloroethane µg/L 129 102 µg/L 39.8 43 .9 --------------------- µg/L < 2 0 .00 µg /L µg/L µg/L µg /L µg/L <2 <2 83 .1 49 .1 79.1 0.00 0 .00 83.0 48 .9 91 .4 µg /L 56 .3 57.3 -------------------------------------------------- 5165 1, 1,2-Trichloroethane µg/L 87 .2 75.0 _ ~0_5_! _ .:r ~~h~o_r~e~h_y~e~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~g~L-____ ~~~ ____ .?~·_:1 __ 5175 Trichlorofluoromethane µg /L 46.4 43.3 ----------------·--------------------------------- 5180 1,2 ,3-Trichloropropane µg /L < 2 0.00 ----------------------------· --------------------- _ ~~2_? _ V~nyl_a_c~t~~ _ _ _ _ __________ . __ ~g~L-____ ~ ~ ~ _____ 0~09 __ 5235 Vinyl chloride µg /L <2 0 .00 ---------------------------- 5260 Xylenes , total µg /L <6 0.00 All anal ytes are included in ERA 's A2LA accreditation . Lab Code : 1539-01 Page 7 of 26 49 .1 -151 --------- 13.7 -55.3 47 .0 -108 34.0 -61.5 Acceptable EPA 8260B ------------------------------ Acceptable EPA 8260B ---------------------------- Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B --------------------------------57 .2 -98.1 Acceptable EF!A 8260B -------------------------------- 38 .5 -56 .9 Acceptable EPA 8260B -------------------------------- 19 .8 -110 Acceptable EPA 8260B ----------------------------------------- _ ~5_: ~:. ~5~5-___ 4_2~4_-_6~~8-___ A_c~_p!a_b~e-____ ~~~ ~~6~~ __ _ 52 .0 -97 .3 Acceptable EPA 8260B ------------------------------------------ 46.5 -95 .2 17 .3 -69.3 54 .6 -87 .1 Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B --------------------------------Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B -------------------------------- Acceptable EPA 8260B I 11"!& ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Value Value Limits Warning Limits Performance Evaluation Method Description PCBs in Water (Standard #1) 0040 Aroclor 1016 8885 Aroclor 1221 004 2 Aroclor 1232 0040 Aroclor 1242 0044 Aroclor 1248 ---------------------------- 0045 Aroclor 1254 µg/L µg /L µg/L µg /L µg/L < 0 .5 < 0.5 < 0.5 < 0 .5 < 0 .5 0.00 0 .00 0 .00 0 .00 0.00 µg /L < 0.5 0 .00 Acceptable EPA 8082 -------------------------------- Acceptable EPA 8082 -------------------------------- Acceptable EPA 8082 -------------------------------- Acceptable EPA 8082 ------------------------------ Acceptable EPA 8082 ------------------------------- ------------------------------- 0046 Aroclor 1260 µg/L 3.40 4 .54 2.45 -5.92 3 .03 -5.35 Acceptable EPA 8082 PCBs In Water (Standard #2) 0040 Aroclor 1016 µg/L < 0 .50 0 .00 Acceptable EPA 608 ------------------------------------------------------------------------------------------ 8885 Aroclor 1221 µg /L < 0.50 0.00 Acceptable EPA 608 ------------------------------------------------------------------------------------------- 0042 Aroclor 1232 0040 Aroclor 1242 0044 Aroclor 1248 µg /L < 0 .50 0.00 --------------------- µg /L 2.40 0 .00 µg /L < 0 .50 3 .18 Acceptable EPA608 Not Acceptable EPA 608 ------------------------------------------ 1.31 -4 .44 1.83 -3 .92 Not Acceptable EPA 608 --· - - ----·----- ----------------- - - --- - - - - --- --· -·-- ----- - -- -- - - - --- - - - - ---------- ---- - - ---- --- - -- 0045 Aroclor 1254 0046 Aroclor 1260 PCBs in Oil (Standard #1) 0099 Aroclor 1016/1242 0100 Aroclor 1254 µg /L µg /L mg/kg < 0 .50 < 0.50 25 .5 0.00 0.00 31.1 mg/kg < 0 .50 0.00 -------------------------------------------------- 0101 Aroclo r 1260 mg/kg < 0 .50 0 .00 PCBs In Oil (Standard #2) 0099 Aroclor 1016/1242 mg/kg < 0.50 0 .00 0100 Aroclor 1254 mg/kg < 0 .50 0 .00 --------------------- 0101 Aroclor 1260 mg /kg 2 .930 23 .1 All an alytes are included in ERA 's A2LA acc reditation . Lab Code : 1539-01 Page 8 of 26 Acceptable EPA 608 -------------------------------- Acceptable EPA 608 5.07 -43.1 _1_1:4_-_3~~8-___ A~~_P!a_b~e ______ Ef'!',_8p ~~ __ _ Acceptable EPA 8082 ------------------------------- Acceptable EPA 8082 ___________ A~~ey!a_b~e ______ Ef'!',_8p~~ __ _ Acceptable EPA 8082 -------------------------------- 4 .32 -32 .9 9.08 -28 .1 Not Acceptable EPA 8082 ,;,~ ENVIRONMENTAL V{j1 RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Organochlorine Pesticides WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Value Value Limits Warning Limits Performance Method Evaluation Description 004 7 Aldrin µg/L 1.4 1.13 0.343 -1.59 0.552 -1.38 Check for Error EPA 8081A ------------------------------------------------------------------------------------------ 7110 alpha-BHC µg /L 5 . 7 7.45 3.24 -10 .2 Acceptable EPA 8081A --------------------------------------------------------------------------------------------- 7115 beta -BHC µg/L 7.4 6 .87 2.84 - 9 .37 Acceptable EPA 8081A 7105 delta-BHC µg/L 10.9 13.4 --------------------- -:~2~ _ il~f:1~~-_!3~S:_(~i~~a_n~)_ _ _ _ _ _ _ _ _ _ _ l:g~L-_____ 1_'.I ______ 1~.~ __ _ :~4~ _ ~lp~~-S:~19f9 ~~e ________________ l:g~L-_____ ~ _____ _!3 :3~ __ 7245 gamma-Chlordane µg/L 6 7 .22 ------------------------------------------------- 0049 4,4'-DDD 0050 4 ,4'-DDE 0051 4 ,4'-DDT 0048 Dieldrin 7540 Endrin ---------------------------- 7530 Endrin aldehyde ---------------------------- µg /L 8 .1 8.3 7 µg/L 6.2 5 .21 µg/L 4.7 3 .87 ---------------------µg /L 9.3 8 .67 µg /L 4.7 3 .82 --------------------- µg /L 6 .9 6 .69 5 .15 -18.7 ---------5.81 -19.1 3 .73-11.1 --------- 2 .95 - 9 .78 3 .06-11 .9 2 .30 -6.79 -------------------------------- Acceptable EPA 8081A -------------------------------- Acceptable EPA 8081A -------------------------------- Acceptable EPA 8081A ------------------------------- Acceptable EPA 8081A 4 .53 -10.4 Acceptable EPA 8081A -------------------------------- 3 .05 - 6 .04 Check for Error EPA 8081A 1.45 -5 .57 2 .14 -4.89 Acceptable EPA 8081 A ------------------------------------------ 4 .25 -11 .8 5 .51 -10 .5 Acceptable EPA 8081A ----------------------------------------- 1.46 - 5 .80 Acceptable EPA 8081A -----------------------------------·------ 1.83 -10 .3 Acceptable EPA 8081 A ------------------------------------------ 7535 Endrin ketone -_l:g~L-___ _!i :6 ______ 5J~ ___ ~-~~-::_ ~-~~ ____________ A_9~e_p!a_b~e-____ ~~~ ~~8_1~ __ _ 751 O Endosulfan I _ _ l:g~L-____ _'.IJ _____ _?:93 __ . _ !-~~-::_ ~-~~ ____________ Accep table ____ ~~~ ~~8_1~ __ _ 7515 Endosulfan II µg /L 12 .4 13.1 4.03 -17 .4 Acceptable EPA 8081A 75 20 Endosulfan sulfate µg /L 10 .6 10 .2 3.85 -14 .9 Acceptable EPA 8081A ------------------------------------------ 1.14 -3.44 1.53 -3 .06 Check for Error EPA 8081 A ------------------------------------------_ ~~7_!3 _ ~:~t~ch~o_r :~~x~d: _(~eyy .. _____ _ µg/L 1.2 2.41 --------------------- 7810 Methoxychlor µg/L 5.5 4 .68 1.16-7 .58 Acceptable EPA 8081A Chlordane 0053 Chlordane, technical µg/L 20.0 20.4 7 .66 -29.4 11.3 -25 .8 Acceptable EPA 8081A Toxaphene 8250 Toxaphene µg/L 18 .9 39 .0 3 .90-70 .6 Acceptable EPA 8081A Chlorinated Acid Herbicides 8505 Acifluorfen µg /L 4.95 0.648 - 7 .38 --------------------- 8530 Bentazon µg /L 0.00 ---------------------------- 8540 Chloramben µg /L 6.17 0 .617 -9.75 ---·--- --- - ---------------- - - 8545 2 ,4-D µg /L 4 .300 7.18 0 .718-11 .6 Acceptable EPA8151 -------------------------------------------------------------- 8560 2 ,4-DB µg/L 2.100 3.70 8550 Dacthal diacid (DCPA) µg/L 0.00 ---------------------------- 8555 Dalapon µg /L 4.900 9.3 4 0 .934-14 .5 Acceptable EPA 8151 ------------------------------------------------------· ----- - - --- -- - --- - ------· --------- ----- 8595 Dicamba µg /L 1.100 2.24 0 .224 -3.48 Acceptable EPA 8151 ------------------------------ 8600 3 ,5-Dichlorobenzoic acid µg /L 3.26 1.26 - 4 .56 ---------------------------- 8605 Dichlorprop µg/L 2.600 3.45 0.345 - 5 .07 Acceptable EPA 8151 -------------------------------------------------· ----------------------------- All ana lytes are included in ERA 's A2l.A acc reditation . Lab Code : 1539-0 1 Page 9 of 26 I i,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Value Value Limits Warning Limits Performance Evaluation Method Description Chlorinated Acid Herbicides (Cont.) 8620 Dinoseb ---------------------------- 7775 MCPA ---------------------------- 7780 MCPP 6500 4-N itrophenol ---------------------------- 6605 Pentachlorophenol ---------------------------- 8645 Picloram ---------------------------- 8655 2 ,4 ,5-T 8650 2 ,4 ,5-TP (Silvex) µg /L < 0.200 0.00 Acceptable EPA 8151 ----------------------------------------------------------------µg/L < 50 .0 0 .00 Acceptable EPA 8151 ------------------------------______________________ .. ________ _ µg/L < 50.0 0.00 Acceptable EPA 8151 ------------------------------------------ µg/L 5.30 9.36 0.936 -15 .2 Acceptable EPA 8151 -------------------------------- µg/L < 0.05 0.00 ---------------------_ _ _ _ _ _ _ _ _ _ __________ A~~e_p!a_b~e-_____ E£'~-8~~~ __ _ µg /L 1.10 2 .20 0.220 -3.43 Acceptable EPA 8151 ---------------------------------------------------------------- µg/L µg /L 2 .60 2.90 5.24 5 .96 0 .524 -7 .81 Acceptable EPA 8151 ------------------------------------------ 0.837 -8.71 Acceptable EPA 8151 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Page 10 of 26 1 /t\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Base/Neutrals 5500 Acenaphthene ----------------------------_ 5505 _ Acenaphthylene ____________ _ _ 5145 _ 2-Amino-1-methylbenzene _____ _ 5545 Aniline 5555 Anthracene 5595 Benzidine 5575 Benzo (a)anth racene ----------------------------5585 Benzo(b)fluoranthene ---------------------------- WP-138 Final Complete Report EPAID: ERA Laboratory Code: TX01484 A1160-01 09/21/06 Report Issued: Study Dates: Units Reported Assigned Acceptance Value Value Limits µg/L 34.8 49 .8 --------------------- µg/L 25.2 31.3 ---------------------µg/L µg /L <5 0.00 0.00 20 .7 -60 .6 11.7-39.7 07/17/06 -08/31/06 Warning Limits Performance Evaluation Method Description Acceptable EPA 8270C --------------------------------Acceptable EPA 8270C -------------------------------- EPA 8270C Acceptable -------------------------------------------------------------- __ 1:1_g~L-____ ~~-~ ____ _:3~-3 __ . _ !6.:~-:_ ~9~2-_ _ __________ A_c~e_p!a_b~e-____ ~~~ ~~7_9 ~ __ _ µg /L < 25 0.00 Acceptable EPA 8270C --------------------------------------------------------------µg /L 60.4 79 .7 36.1 -101 Acceptable EPA 8270C __ 1:1_g~L-____ ~~-~ ____ ~ ~ ·¥ __ . _ ! ~ ~ -:_ ~7~~ _ _ __________ A_c~_p!a_b~e _____ ~~ ~ ~~7.9~ __ _ µg /L 31.8 45 .9 10 .7 -68 .8 Acceptable EPA 8270C _ ~~9.9 _ ~:~z_oi g~~·il p_ery~e_n: _____________ 1:1_g~L-____ ! ~-~ _____ 2~-~ __ -------------------------------------------------------------- 4.90-36 .8 Acceptable EPA 8270C _ ~~8.9 _ ~:~z_o !a)~Y!e_n~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ l:1_9~L-_____ <_5 ______ 0:0.9 __ Acceptable EPA 8270C -------------------------------- -~~3.9 _ ~:~ZJ ~ a_l~o_h~I -- - --- ------- ---_ 1:1_9:L_ ----_<_5_ ----.9 ~09 --. -----.. ---Acceptable EPA 8270C --------------------------------5660 4-Bromophenyl-phenylether ---------------------------- 5670 Butylbenzylphthalate ---------------------------- 5680 Carbazole 5745 4-Chloroaniline 5760 bis(2-Chloroethoxy)methane --------------------------- -5765 _ bis(2-Chloroethyl)ether _______ _ 5780 bis(2-Chloroisopropyl)ether ---------------------------- 5790 1-Chloronaphthalene ----------------------------5795 2-Chloronaphthalene ---------------------------- 5825 4-Chlorophenyl-phenylether ---------------------------- 5855 Chrysene --------------------------- µg /L <5 0.00 Acceptable EPA 8270C -------------------------------- µg/L < 5 0.00 ---------------------Acceptable EPA 8270C --------------------------------µg/L < 5 0.00 --------------------- µg/L < 5 0.00 Acceptable EPA 8270C ------------------------------------------µg /L 76 .7 114 --------------------- µg /L 110 171 ---------------------µg/L < 5 0.00 µg/L µg/L 95.9 0.00 146 45.1 -135 --------- 45.0 -206 45 .0 -176 µg /L 72 .5 97.5 36 .6 -122 ------------------------------- µg /L 60 .9 79 .7 31.6 -104 Acceptable EPA 8270C -------------------------------- Acceptable EPA 8270C -------------------------------- Acceptable EPA 8270C -------------------------------- Acceptable EPA 8270C --------------------------------- Acceptable EPA 8270C ----- - --- ------· ----- ----------- -- _ ~~9_:i _ ?!b~~':.(~.~)_'.3~t~~a ~1:n_e ____________ l:1_9~L-_____ <_5 _____ .9 ~0.9 _ _ _ ____________________ A_c~ip!a_b~e-____ ~~~ ~~7.9~ __ _ 5905 Dibenzofuran µg /L 58.4 82 .8 29 .3 -104 Acceptable EPA 8270C - --------- --------------------- ---------------------- - - --- ----- - --- ----- ------ --------.. - --- _ ~~2_:i _ ?!-~-~~ttlp~t~~l~tt: ____ ·-_ _ _ _ _ _ _ _ l:1_9~L-____ ~~-~ _____ 1_9~ ____ ~~-~: !~1-_ _ __________ A~~_p!a_b~e-____ ~~~ ~~7_9~ __ _ 4610 1,2-Dichlorobenzene µg/L < 5 0.00 Acceptable EPA 8270C --------------- ------ ------------ ------ --------- --·-- - - ---- - ---- - --------- - --- - ---- --------- 4615 1,3-Dichlorobenzene µg/L < 5 0.00 Acceptable EPA 8270C -------------------------------------------------------------------------------------------4620 1,4-Dichlorobenzene 5945 3 ,3'-Dichlorobenzidine ---------------------------- -~~7.9 _ ?!e~h_y!_p~l_!l~l~~e ____________ _ 6135 Dimethylphthalate ---------------------------- 6185 2.4-Dinitrotoluene µg/L 35.4 87.2 8.72 -105 Acceptable EPA 8270C --------------------------------------------------------------- µg/L < 10 0.00 Acceptable EPA 8270C --------------------------------------------------------------- µg/L 108 141 26 .6-191 Acceptable EPA 8270C --------------------------------------------------------------- µg /L 87 .2 124 12.4 -179 Acceptable EPA 8270C µg/L 40.6-135 ------------------------------------------------------··------ 90 109 6190 2 ,6-Dinitrotoluene µg /L 129 169 71 .1-211 27.7 -207 _ _ ________ A~~_pta_b~e __ _ _ _ ________ A_c:e_pta_b~e __ Acceptable EPA 8270C EPA 8270C EPA 8270C ------------------------------------------------- -~~09 __ Di-~-_o :ttlp~t~a~~tt: ___________ . __ l:1_9~L-____ ~~-!-____ 1~!-_ 6265 Fluoranthene _ ~2_5_:i _ ~i_s(2=~t~y_lh_e~~l)_P~~h~l~t~ _ _ _ ___ . __ l:1_9~L-____ ~~-! _____ 1_2~ __ . _ ~~-~: ! ~1 -_____________ A_c~_p!a_b~e-____ ~~~ ~2_7_9S: __ _ µg /L 48 .3 62.2 28 .2 -77.4 Acceptable EPA 8270C -----------------------------------------------------------~-------------------------------- All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Page 11 of 26 I,;~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® WP-138 Final Complete Report Tamara Welch EPA ID: Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr ERA Laboratory Code: TX01484 A1160-01 Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Base/Neutrals (Cont.) 6270 Fluorene 6275 Hexachlorobenzene 4835 Hexachlorobutadiene 6285 Hexachlorocyclopentadiene ---------------------------- 4840 Hexachloroethane _ 6315 _ lndeno(1 ,2,3-cd)pyrene _______ _ 6320 lsophorone ---------------------------- Report Issued: Study Dates: Units Reported Assigned Acceptance Value Value Limits µg /L µg/L 123 .0 58 .2 157 84.6 µg /L 49 .3 111 --------------------- µg/L < 5 0 .00 µg /L 26.9 65.5 µg/L 30.5 44.5 --------------------- µg/L < 5 0.00 70.0 -183 36.6-104 12 .9 -132 6 .66 -78.4 9.40 -60.9 09/21/06 07/17/06 -08/31/06 Warning Limits Performance Method Evaluation Description Acceptable EPA 8270C ---------- - - - ----- - - ----·-- - --- -- Acceptable EPA 8270C -------------------------------- Acceptable EPA 8270C -------------------------------- Acceptable EPA 8270C --------------------------------Acceptable EPA 8270C -------------------------------- ___________ A_c~_p!a_b~e _____ ~~~ ~~7_D~ __ _ Acceptable EPA 8270C -------------------------------- -~~8_? _ 3°::_~e!~!.'1~e~t~a~e_n~ _____________ ~g:L _____ ~~~ _____ 5?-~ __ 9 .90 -72.4 Acceptable EPA 8270C _ ~~0_? _ !'l~e~t~a~e_n~ __________________ ~9:l _____ ?~-~ _____ 1~?-_ 6460 2-Nitroaniline µg/L < 5 0.00 µg/L µg/L <5 <5 0.00 0.00 ----------------------------------------- 33.1 -150 Acceptable EPA 8270C ---------r -------------------------------- Acceptable EPA 8270C ----------------------------------------- ___________ A_c~e_p!a_b~e-____ ~~~ ~~7_D~ __ _ ___________ A_c~e_p!a~~e-____ ~~~ ~~7_D~ __ 6465 3-Nitroaniline 6470 4-Nitroaniline 5015 Nitrobenzene µg/L 82.8 116 36 .1 -141 Acceptable EPA 8270C ---------------------· ----------------------------------------- µg/L < 5 0 .00 ___________ A_c~EP!a_b~e _____ ~~~ ~~7_D~ __ _ 6530 N-Nitrosodimethylamine µg /L 54.1 101 10 .1 -120 Acceptable EPA 8270C -------------------------------------------------------------------------------------------- -~~3_5 _ !'J=f\J_i~<:S_?~ie~e_n~l~f!i~n~ ___________ ~g:L ______ <_5 _____ _D ~09 __ Acceptable EPA 8270C _ ~~4_5 _ !'J=f':J.i~<:S_?::_d~-~-p~op~l~r,:ii~~ ______ . __ ~g:L ______ <_5 ______ 0~09 __ ___________ A_c~e_p!a_b~e-____ ~~~ ~~7_D~ __ _ 6590 Pentachlorobenzene µg/L <5 0.0 0 Acceptable EPA 8270C ------------------------------------------------------------ 6615 Phenanthrene µg/L <5 0 .00 Acceptable EPA 8270C -------------------------------- _ 6665 _ Pyrene _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~g:L _____ ~7_.! ____ ~~-~ __ . _ !4_.~::. ~5~(!_ _____________ A_c~_p!a_b~e _____ ~~~ ~~7_D~ __ _ _ 5095 _Pyridine__________________ _ _ ~g!.L ______ <_5 _____ _o ~o9 _ _ _ _ _ _ _ _ _ _ _ _ __________ A_c~e_p!a_b~e-____ ~~~ ~~7_D~ __ _ 6715 1,2 ,4 , 5-Tetrachlorobenzene 5155 1,2 ,4-Trichlorobenzene µg/L µg/L <5 63 .5 0.00 120 All analytes are in clu ded in ERA 's A2LA accreditation . Lab Code : 1539-01 Page 12 of 26 Acceptable EPA 8270C --------------------------------26 .8-142 Acceptable EPA 8270C ~1.~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Acids 5610 Benzoic acid -----------------------------~~09 _ 4-Chloro-3-methylphenol ______ _ _ ~~09 _ 2-Chlorophenol ____________ _ _ ~~09 _ 3 :_4:~i~h~o_r~p_h:~O~ __________ _ 6005 2 ,6-Dichlorophenol ----- - ---------- - - ---- - -- - - - -- _ ~1_39 _ 3 :_4:~i~:t~~leh_e~~I -_________ _ _ ~3_69 _ ~:_6:~i~i~~-~-~!!!hJlp~E:_n_?~ _____ _ _ ~175 _ 2 ,4-Dinitrophenol ___________ _ _ ~~09 _ 3 :_~e!hJ!_P~:~O~ ____________ _ _ 641 O _ 4-Methylphenol ____________ _ _ 6490 _ 2-Nitrophenol _____________ _ WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A1160-01 09/21/06 07/17/06 -08/31/06 Report Issued: Study Dates: Units Reported Assigned Acceptance Value Value Limits Warning Limits Performance Evaluation Method Description µg/L < 50 0.00 _____________________ A~~ey!a_b~e _____ ~~ ~ ~~79!? __ _ __ l-!_9~L-____ ?9_.~ _____ 19? __ . _ ~!-~: !3_8 _____________ A~~_p!a_b ~e-____ ~~~ ~~79!? __ _ µg/L 60 .6 93 .8 27 .6-118 µg/L µg /L 38 .9 55 .8 105 _ !6_.~:. ~2_. 1_ _____________ A_c~_p!a_b~e _____ ~~~ ~~79!? __ _ 35.4-132 µg/L 50 .7 72 .7 14 .1 -96 .3 ------------------------------µg/L 117 128 43 .5-181 µg/L 117 144 µg/L 73 .1 107 µg/L 35.7 54 .5 --------------------- µg/L 92 .6 125 20.2 -132 5.45 -73.0 --------- 29 .8-163 ___________ A~~_p!a_b~e _____ ~~~ ~~79!? __ _ Acceptable EPA 8270C -------------------------------- ___________ A_c~_p!a_b~e _____ ~~~ ~~79~ __ _ ___________ A~~_p!a_b~e _____ ~~ ~ ~~79!? __ _ ___________ A~~_p!a_b~e _____ ~~~ ~~79!? __ _ _ 6500 _ 4-Nitrophenol _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ l-!_9~L-____ ~2_.~ _____ 19~ __ 10.6-144 27 .2 -147 14 .5-194 _ _ _ _ _ _ _ _ _ _ Acceptable ____ ~~ ~ ~~79!? __ _ _ ~~O: _ ~:~t~<:_h~o_r~P~:~o~ ___________ . __ l-!_9~L-____ ?5_-~ _____ 19~ __ 6625 Phenol µg/L 48.1 145 --------------------- _ ~~3: _ 3 :_3:4~6_-!e_tr~~~l~r~~h!!~~I -_____ _ µg/L 35 .5 45.2 --------------------- _ ~~3: _ 3 :_4:5~ ,::r~c~l~r.?e~e_n~I -________ _ µg/L 45 .6 74 .3 6840 2,4 ,6-Trichlorophenol µg/L 60 .4 87 .3 All analytes are included in ERA 's A2LA accred itation . Lab Code : 1539-01 Page 13 of 26 --------- 4 .52 -61 .5 27.5 -97.2 27 .9-111 __________ Acceptable _____ ~~~ ~~79!? __ _ ___________ i\_c~_p!a_b~e _____ ~~~ ~~79!? __ _ _ _________ Acceptable ____ ~~~ ~~7_9!? __ _ _ __________ A_c~_p!a_b~e _____ ~~~ ~~7_9(? __ _ Acceptable EPA 8270C I i.~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® WP-138 Final Complete Report Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Units Reported Value EPAID: ERA Laboratory Code: TX01484 A1160-01 Report Issued: Study Dates: Assigned Acceptance Value Limits 09/21/06 07/17/06 -08/31/06 Warning Performance Limits Evaluation Gasoline Range Organics (GRO) in Water 9408 Gasoline Range Orgaincs (GRO) µg/L 2910 3150 1220 -5550 Acceptable - --- --------- - --------------------------------------------------------------- 4375 Benzene in GRO µg/L 19 .8 3 .16 -40.8 - ----------------------------------------------------------------------------- 4765 Ethylbenzene in GRO µg /L 87 .2 58.4 -116 ------------------------------------------------------------------------ 5140 Toluene in GRO µg/L 246 131-321 --- - ------------------------------------------------------------------------- 5260 Xylenes , total in GRO µg/L 351 228 -482 Diesel Range Organics (DRO) in Water 9369 Diesel Range Organics (ORO) µg /L 505 882 139 -1200 Acceptable BTEX & MTBE in Water 4375 Benzene µg/L 38.0 33.2 23.4 -42 .8 Acceptable -- - --------------------------------------------------------------------------5000 tert-Butyl methyl ether (MTBE) µg /L 68 .6 55 .3 34 .8-78 .0 Acceptable ---- -------------------------------------------------------------------------- 4765 Ethylbenzene µg/L 46.8 45 .3 31.1 -57 .8 Acceptable ------------------------------------------------------------------------- 5140 Toluene µg/L 22 .5 22 .1 15.4 -28 .3 Acceptable --- - ------------------------------------------------------------------------- 5260 Xylenes , total µg/L 77.0 73 .6 41.7 -100 Acceptable Texas Low-Level Fuels (TPH) in Water 2050 Total Petroleum Hydrocarbons mg /L 19 .65 6.12 0.612 -8 .94 Not Acceptable Texas High-Level Fuels (TPH) in Water 2050 Total Petroleum Hydrocarbons mg /L 81 .3 88 .1 8.81 -127 Acceptable All analytes are included in ERA 's A2LA accred itation . Lab Code : 1539-01 Page 14 of 26 Method Description EPA 8015B ------------- ------------- -------------- -------------- EPA 8015B EPA 8021 B -------------EPA 8021 B ------------- EPA 8021 B ------------- EPA 8021 B ------------- EPA 8021 B TNRCC 1005 TNRCC 1005 . ,;,~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Study: WP-138 ERA Laboratory Code: A 1160-01 Laboratory Name: Accutest Gulf Coast Report Type: Complete Report Method: Method B Page 15 of 26 1 11\ ENVIRONMENTAL ·~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. pH 0019 pH Hardness 0023 Calcium 0024 Magnesium ---------------------------- 1550 Calcium Hardness (C aC03) -- ------- -------- ------- - --·- 0022 Total Hardness (CaC03) Demand 0038 BOD 0102 CBOD 0036 COD 0037 TOC Simple Nutrients 0031 Ammonia as N ---------------------------- 0032 Nitrate as N 1820 Nitrate + Nitrite as N 0033 Ortho-phosphate as P WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Value Value Limits S .U. 6.65 6.70 6 .50 -6 .90 mg /L 76 .3 62 .0 -85 .2 mg /L 42.198 41 .5 --------------------- mg /L 7.023 6.73 5.69 -7.70 --------- mg /L 104 92 .7-118 --------------------- mg /L 131 116-150 Warning Limits 65 .9 -81.3 Performance Method Evaluation Description Acceptable EPA 150 .1 6.02 -7 .36 Acceptable EPA 200 .7 -------------------------------- 121 -144 mg /L mg/L mg /L mg /L 134 100 102 87 .6 164 64 .9 51 .5 -152 68 .3 -135 Acceptable SM 521 O B ------------------------------------------39.3 -136 55.4-120 Acceptable EPA 405 .1 ------------------------------------------ mg/L mg/L 61.3 20 .7 13 .1 22 .3 126 -187 54 .2 -74.7 9 .74 -16 .3 --------- 17.4 -26 .9 mg /L 22 .3 18.2 · 25 .9 ---------------------· --------- mg/L 4.73 3.91 -5 .59 136 -177 57.6 -71 .3 10 .8-15 .2 Acceptable EPA 9060 19 .0 -25 .3 Acceptable SM 4500 N03-E -- ---- -- - ----- - - --------------- -- 4 .19 -5.31 All analytes are incl uded in ER A's A2LA acc reditation. Lab Code : 1539-01 Page 16 of 26 I ii~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Trace Metals 0001 Aluminum 0016 Antimony ---------------------------- 0002 Arsenic ---------------------------- 1015 Barium -----r ---------------------- -~~O} _ !3~ry~i~~ ________________ _ 1025 Boron 0004 Cadmium 0006 Chromium ---------------------------- 0005 Cobalt 0007 Copper ---------------------------- 0008 Iron --------------------------- 0012 Lead 0010 Manganese ---------------------------- -~~7~-~3ry~~~n~~--------------- 0011 Nickel 0013 Selenium WP-138 Final Complete Report EPAID: TX01484 A1160-01 ERA Laboratory Code: Report Issued: 09/21/06 07/17/06 -08/31/06 Study Dates: Units Reported Assigned Acceptance Warning Performance Method Value Value Limits Limits Evaluation Description µg /L 380 .65 300 219 -385 246 -357 Check for Error EPA 200 .7 --------------------- µg /L 201 .36 196 129 -240 147 -221 Acceptable EPA 200 .7 --------------------------------------------------------------- µg /L 855 .31 837 µg /L 2095.3 2020 --------------------- µg /L 742.78 726 µg /L 1165.4 879 µg /L 568 .48 581 704 -978 1750 -2280 618 -820 --------- 728 -1030 496 -660 _ ~5_0_-_9~~ ____ A_c~y!a_b~e-____ ~~~ 3~~-~ __ _ Acceptable EPA 200 .7 -------------------------------- 652 -786 Acceptable EPA 200 .7 ------------------------------·-- _________ ~9~ ~c9:p_t~b~e ____ ~~~ 3g~-~ __ _ 523 -632 Acceptable EPA 200 .7 --------------------------------------------------------------- µg /L 660.09 663 µg/L 457 .61 446 --------------------- µg/L 707. 99 703 µg/L 890.39 849 --------------------- µg /L 772 .06 760 --------------------- µg /L 508 .46 488 µg /L 579 .11 566 --------------------- µg /L 980.31 962 --------------------- µg /L 1047 .3 1020 578 -750 391 -500 633 -773 _ ~~6--_73! ____ A~~y !a_b~e-____ ~~~ 3 ~~-~ __ _ 410 -482 Acceptable EPA 200 .7 ----------- -- - ---- - ------ - ------ - 661 -749 Acceptable EPA 200 .7 749 -960 785 -925 Acceptable EPA 200 .7 ----------------------------------------- 665 -852 696 -821 Acceptable EPA 200 .7 ----------------------------------------- 437 -542 455 -525 Acceptable EPA 200 .7 ------------------------------------------ 481 -645 509 -618 Acceptable EPA 200 .7 ----------------------------------------- 866 -1070 904 -1040 Acceptable EPA 200.7 ----------------------------------------- 811 -1180 872 -1120 Acceptable EPA 200 .7 0017 Silver µg/L 107.16 106 90.4-122 _ ~5~6--_ 1_1? ____ A~~y!a_b~e _____ ~~~ 3~~-~ __ _ ----------------------------------------------------------- 0075 Strontium µg /L 57 .8 60 .4 49 .8 -70 .9 53 .3 -67 .4 Acceptable EPA 200 .7 -------------------------------- 0018 Thallium µg/L 232 .97 226 165 -284 185 -264 Acceptable EPA 200 .7 -------------------------------- 0014 Vanadium µg /L 234 .46 228 199 -256 209 -246 Acceptable EPA 200 .7 - -------- ---· --· ---· - --- - ------------------------- --- ------------------------------------------ 0015 Zinc µg /L 1178 . 7 1120 963 -1280 1020 -1230 Acceptable EPA 200 .7 Mercury 0009 Mercury µg /L 27 .5 26.4 16 .2 -35.6 19.5 -32 .3 Acceptable EPA 245 .1 Minerals _ 0027 _ Alkalinity as CaC03 _________ _ 40.2 -53.6 42 .5 -51 .4 mg /L 46.7 --------------------- 0028 Chloride mg /L 92.2 79 .1 -105 83 .5-101 0020 Conductivity at 25 °C µmhos/cm 458 411 -505 427 -489 ----------- -------· ----- ----- 0029 Fluoride mg /L 3.52 2 .96 -4.09 3.15 - 3.91 ---------------------------·-----------------------· -----·--------------------------- 0026 Potassium ----------------------- 0025 Sodium ----·--------------------- 0030 Sulfate 0021 Total Dissolved Solids at 180°C .. ".1 9!L ____ 2~-~!6 ____ 3~.~ __ . _ 19:~ ~ ~7:~ ___ 2_0~7_-_2?~5-___ Accey!a_ble __ . mg /L 79 .86 80.4 68 .3 - 92 .1 72 .2 -88 .2 Acceptable -----·-------------·----------· mg /L 19 .8 15.4 -23 .7 16 .8 -22 .4 EPA 200.7 EPA 200 .7 - ------~ - --- ---------------· --------- - ---- ------------ - ---- mg /L 285 213 -357 237 -333 - -------- ------ ---------------------------· ------- --- - ----· - - ----- - - --------------- --- --- - ------ 1950 Total Solids at 105°C mg /L 305 264 -342 Tin and Titanium All analytes are included in ERA 's A2LA accreditation . Lab Code : 1539-01 Page 17 of 26 #11\ ENVJRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Tin and Titanium (Cont.) 0076 Titanium Units Reported Value µg/L 257 .81 All ana lytes are included in ERA's A2LA accreditation. Lab Code : 1539-01 WP-138 Final Complete Report EPAID: ERA Laboratory Code: TX01484 A1160-01 09/21/06 Report Issued: Study Dates: 07/17/06 -08/31/06 Assigned Acceptance Warning Performance Value Limits Limits Evaluation 249 214 -280 225 -269 Acceptable Method Description EPA 200.7 Page 18 of 26 ,/,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Volatiles WP-138 Final Complete Report EPA ID: ERA Laboratory Code: TX01484 A1160 -01 09/21/06 Report Issued: Study Dates: Units Reported Assigned Acceptance Value Value Limits 07/17/06 -08/31/06 Warning Limits Performance Evaluation Method Description 4315 Acetone µg/L < 50.0 0.00 _____________________ A_c~ey!a_b~e ______ ~~A_ ~2_4 ___ _ -------------------------------------------------- 4320 Acetonitrile µg /L < 10.0 0 .00 ------------------------------------------------------------___________ A_c~e_P!a_b~e ______ ~~A_ ~2_4 ___ _ -~~4_D _ !'-_?')'l_?~i!.1'i~e_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~g~L-____ <_ 1_o:o _____ o:o_o __ _ _________ Acceptable ______ ~~A_ ~2.4 ___ _ 4325 Acrolein ---------------------------- 0065 Benzene 0060 Bromodichloromethane ---------------------------- 0062 Bromoform 4950 Bromomethane ---------------------------- -4410 _ 2-Butanone (MEK) __________ _ -~C!_O_D _ !e_rt:~U!Y~ !11~~ht1 _e!h_e~ t~T_B_E2 ---- 4450 Carbon disulfide 0058 Carbon tetrachloride 0064 Chlorobenzene 0061 Chlorodibromomethane ---------------------------- 4485 Chloroethane 0055 Chloroform 4960 Chloromethane ---------------------------- µg/L < 10.0 0 .00 --------------------- µg /L 46 .9 46.4 --------------------- µg/L 40.3 37.1 µg /L 17.4 14 .7 --------------------- µg /L < 2.00 0 .00 --------------------- µg /L < 10.0 0.00 -------------------- µg/L < 2.00 0 .00 µg/L < 2 .00 0 .00 --------------------- µg/L 77 .5 74.7 µg /L 104 97.8 --------------------- µg/L 92.8 81.2 --------------------- µg/L < 2.00 0.00 --------------------- µg/L < 10.0 0 .00 µg/L 24 .6 23 .0 --------------------- µg/L < 2.00 0 .00 33.3-59 .2 26.0-50.0 8.15-19.6 Acceptable EPA 624 -------------------------------- _3_? :6_-_5~~9-___ A_c~y!a_b~e-_____ ~~A_ ~2.4 ___ _ 30 .0 -46.0 Acceptable EPA 624 -------------------------------- 10.1 -17.7 Acceptable EPA 624 ------------------------------- _____________________ A_c:e_P!a_b~e ______ ~~ ~ ~2_4 _ _ __ _____________________ A_c~ey!a_b~e ______ ~~A_ ~2.4 ___ _ Acceptable EPA 624 ----------------------------------------- 40.7-102 70.6 -122 55.7 -108 ___________ A_c~ey!a_b~e ______ ~~ ~ ~2_4 ___ _ _5_0:9_-_9_:1 ~6-___ A~~ey!a_b~e ______ ~~A_ ~2.4 ___ _ 79.2 -114 Acceptable EPA 624 -·------ ---------------- - - ------- Acceptable EPA 624 ----------------------------------------- -_ _ _ _ _ _ _ _ _ __________ A_c~ey!a_b~e ______ ~~A_ ~2_4 ___ _ _ ! 5_:~-:_ ~o~~ ___ 1_8:3_-_2~~1-___ A_c~ey!a_b~e ______ ~~A_ ~2_4 ___ _ -~~7_D _ _:1 ._2:~i~r~~~-~-:_c~l~~op~op~n_e_(I?~~~) __ ~g~L-____ <_2~(!_0 _____ 0:09 __ _ _ _ _ _ _ _ _ _ _ __________ A_c~ey!a_b~e ______ ~~~ ~2_4_ _ _ _ ____________________ A_c~E:_P!a_b~e ______ ~~ ~ ~2_4 ___ _ µg/L 32.5 28 .9 19.8-39.9 4595 Dibromomethane µg/L < 2 .00 0.00 ---------------------------------------------------------- 0094 1,2-Dichlorobenzene µg/L 49.2 52.8 36.5 -68.7 ---------------------------------------------------------- 0096 1,3-Dichlorobenzene µg/L 53.2 49 .7 33.4 -63 .5 0095 1 ,4-Dichlorobenzene µg/L 92.9 94.0 63.9 -117 ---------------------------------------------------------- 4625 Dichlorodifluoromethane µg/L < 2.00 0 .0 0 ___________ A_c~y!a_b~e ______ ~~A_ ~2_4 ___ _ __________ Acceptable _____ -~~A_~2__4 ___ _ _4_1:9_-_6~~3-___ A_c~y!a_b~e ______ ~~A_ ~2_4 ___ _ _3_8:4_-_5~~5-___ A_c~y!a_b~e ______ ~~A_ ~2_4 ___ _ 72.8 -108 Acceptable EPA 624 -· ------------------------------- -- -------- - - --------· ------- -------------- ------------- ----- _ ~~4_D _ _:1 ,_1 =~i~h~o__r~e!~y~e!l~ _________ _ 4645 cis-1 ,2-Dichloroethylene ---------------------------- 4700 trans-1 ,2-Dichloroethylene ---------------------------- _ 4~3~ _ ~, 1:~i~h~o__r~e!~a!l ~ ______________ ~g:L _____ <_2:0_0 _____ 0:09 ________________________ A~~E:_P!a_b(e ______ E~~ 62_4 ___ _ _ g(!_5~ _ _:1 ,_2:~i~h~o__r~e!~a!l ~ ____ . _________ ~g~L-____ ~~.~ _____ 5~.3 _ _ _ ~6_:~ -_ ?_O~~ ___ 4_2:5_-_6~~6-___ A_c~y!a_b~e-_____ ~~~ ~2_4 ___ _ µg/L < 2 .00 0 .00 --------------------- µg/L 62.4 63 .1 _ ~~5~ _ _:1 ._2:~i~h~o__r~p__r~p_a_ll: _________ _ _ ~~8_D _ _9i~-:_ 1 :3_:~i~h~~r~~r~~y~e!l: ______ _ 4685 trans-1 ,3-Dichloropropylene ---------------------------- -g(!_6~ _ _!:!hJl_?~~Z:!~: _____________ _ _ _ _ _ _ _ _ _ _ _ __________ A~~ey!a_b~e ______ ~~ ~ ~2_4 ___ _ _ ~5_:~-:_ ~3~~ _____________ A_c~ey!a_b~e-_____ ~~~ ~2_4 ___ _ __ ~g:L _____ ~~.~ ____ .4~ 9 ____ ~8_.?_-:_ ~7~3-_ _ __________ A_c~y!a_b~e ____ .. _ ~~A_ ~2_4 _ -~g~L-____ ~~·! _____ 8~._:1 -___ ~~.g : !~2-_____________ A_c~:P!a_b~e _____ EPA 624 _ _ ~g~L-____ <_2~0_0 ____ _D :09 _ _ _ _ _ _ _ _ _ _ _ _ __________ A_c ~e_P!a_b~e-_____ ~~~ ~2_4 ___ _ _ _ ~g:L _____ <_2:C!_O ____ _D :O_D ________________________ A_c~ey!a_b~e-_____ ~~~ ~2_4 ___ _ __ ~g~L-____ ~~.~ _____ 5~.3 ____ ~5_:~-:_ ~6~~ ___ 4_\0_-_6_:1 ~4-___ A~~_P!a_b~e ______ ~~A_ ~2_4 ___ _ _ _ ~g~L-____ <_2~(!_0 ____ _D :O_D _ _ _ ____________________ A_c~ey!a_b~e ______ ~~A ~2.4 ___ _ _ 1~6_D _ 3 :H_e~~n_o_ll : _ _ _ _ _ _ _ ________ ~g~L-____ ~~7-____ ~~.~ _ _ _ ~~·?: !~7-_ _ __________ A_c~ey!a_b~e ______ ~~A_ ~2_4_ 0063 .. _M_eth_yl~~= ch}o__ri9: _ _ _ __________ ~g~L-____ ~~.?_ _____ 9~._o _ _ _ ~?.·? = !30 ____ ~9~8--_ 1_1~ ___ A_c~y!ab~e-_____ ~~~ ~2_4 __ _ 4835 Hexachlorobutadiene All analytes are included in ERA 's A2LA accreditation. Lab Code : 1539-01 Page 19 of 26 I i,~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Volatiles (Cont.) 4995 4-Methyl-2-pentanone (MIBK) ---------------------------- _ ~~0_? .. !l~e~t~a~E:_n~ ______________ _ _ ~ 1_ 0_9 _ 5>!Y~e_n~ _________________ _ 5105 1, 1, 1,2-Tetrachloroethane 511 O 1, 1,2 ,2-Tetrachloroethane 0059 Tetrachloroethylene ---------------------------- 0067 Toluene 5155 1,2,4-Trichlorobenzene ---------------------------- 0056 1, 1, 1-Trichloroethane 5165 1,1,2-Trichloroethane 0057 Trichloroethylene ---------------------------- 5175 Trichlorofluoromethane --~------------------------- WP-138 Final Complete Report EPAID: TX01484 A1160-01 09/21/06 ERA Laboratory Code: Report Issued: Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Warning Limits Performance Evaluation Method Description Value Value Limits µg/L 129 102 --------------------- µg/L 39.8 43.9 µg/L µg /L <2.00 < 2 .00 0.00 0.00 µg/L < 2.00 0.00 --------------------- µg /L 83 .1 83 .0 µg/L 49 .1 48 .9 -- - ------------------ µg /L 79.1 91 .4 -------------------- µg /L 56.3 57.3 49.1-151 Acceptable EPA 624 13.7 -55.3 Acceptable EPA 624 ------------------------------------------Acceptable EPA 624 -------------------------------- Acceptable EPA 624 -------------------------------- Acceptable EPA 62 4 ----------------------------------------- 47.0 -108 57 .2 -98 .1 Acceptable EPA 624 ------------------------------------------ 34 .0 -61.5 38.5 -56 .9 Acceptable EPA 624 ------------------------------------------ 19.8 -110 Acceptable EPA 624 ------------------------------------------ 35 .7 -75 .5 42.4 -68 .8 Acceptable EPA 624 ---------------------------------------------------------------- µg/L 87 .2 75.0 52.0 -97.3 Acceptable EPA 624 -----------·--------------- - µg/L 74.4 73.1 46.5 -95.2 54 .6 -87 .1 Acceptable EPA 624 ----------------------------------------------------------- µg/L 46.4 43.3 17.3-69.3 -~1_8_9 _ ~ ._2:3.:: i_:r~c~l9r_9er_9e~n~ _________ . __ ~g!L _____ <_2:~0-___ _9 ~09 _ _ _ _ _ _ _ _ _ _ _ _ __________ A_c~e_P!a_b~e-_____ ~~~ ~2_4 ___ _ _ ~~2_? _ y~nyl_a_c~t~~e _______________ . __ ~9:l _____ <_ 1_9 ~0-___ .9 ~09 __ . _____________________ A_c~e_P!a_b~e ______ ~~~ ~2j ___ _ _ ~~3_? _ y~nyl _c~~o ~i~e-_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~9:l _____ <_2:~0 ____ .9 ~09 __ Acceptable EPA 624 ----------------------------------------- 5260 Xylenes , total µg /L < 6 .00 0 .00 Acceptable EPA624 All analytes are included in ERA's A2LA accred itation . Lab Code: 1539-01 Page 20 of 26 ~/,~ ENVIRONMENTAL f../li1 RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Value Value Limits Warning Limits Performance Evaluation Method Description PCBs in Water (Standard #1) 0040 Aroclor 1016 Acceptable EPA 608 -------------------------------- 8885 Aroclor 1221 ___________ A_c~e_p!a_b~e ______ ~~ ~ ~0_8 ___ _ 0042 Aroclor 1232 ___________ A_c~e_p!a_!)~e ______ ~~~~0_8 ___ _ 0040 Aroclor 1242 Acceptable EPA 608 µg /L µg/L µg/L µg/L µg/L < 0.5 < 0 .5 < 0.5 < 0 .5 < 0.5 0 .00 0 .00 0.00 0 .00 0.00 ---·--------------------------------------- 0044 Aroclor 1248 0045 Aroclor 1254 µg /L < 0.5 0.00 ------------------------------0046 Aroclor 1260 PCBs In Water (Standard #2) 0040 Aroclor 1016 8885 Aroclor 1221 0042 Aroclor 1232 µg /L 3.40 4 .54 2 .45 -5 .92 µg /L µg /L µg/L < 0.5 < 0.5 < 0 .5 0.00 0 .00 0.00 ___________ A_c~e_p!a_!)~e ______ ~~~ ~0_8 ___ _ Acceptab le EPA 608 -------------------------------- 3 .03 - 5 .35 Acceptable EPA 608 Acceptable EPA 8082 -------------------------------- Acceptable EPA 8082 --------------------------------Acceptable EPA 8082 -------------------------------- 0040 Aroclor 1242 µg /L < 0.5 0.00 Acceptable EPA 8082 -------------------------------------------------------------------------------------------- 0044 Aroclor 1248 µg/L 2 .40 3.18 1.31 -4 .44 1.83 -3.92 Acceptable EPA 8082 ---- - --- --- -- -------------- -- -- - - - - -- - -- -- - --- ---------------------------------------· ------- 0045 Aroclor 1254 0046 Aroclor 1260 µg/L µg/L < 0.5 < 0.5 0.00 0.00 All ana lytes are included in ERA 's A2LA accreditation. Lab Code: 1539-01 Page 21 of 26 Acceptable EPA 8082 ------------------------· --- Acceptable EPA 8082 I i,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Organochlorine Pesticides WP-138 Final Complete Report EPAID: ERA Laboratory Code: TX01484 A1160-01 09/21/06 Report Issued: Study Dates: Units Reported Assigned Acceptance Value Value Limits 07/17/06 -08/31/06 Warning Limits Performance Evaluation Method Description 0047 Aldrin µg /L 1.4 1.13 0.343 -1.59 0.552 -1.38 Check for Error EPA 608 ---------------------------------------------------------- 7110 alpha-BHC µg/L 5. 7 7 .45 3.24 -10 .2 Acceptable EPA 608 ----------------------------· ---------------------· ----------------------------------------- 7115 beta-BHC µg /L 7.4 6 .87 2 .84 -9.37 Acceptable EPA 608 ------------------------------------------------------------------------------------------- 7105 delta-BHC µg /L 10 .9 13.4 5 .15 -18.7 Acceptable EPA608 ------------------------------------------------------------------------------------------ _ ~1_29 _ 9~~~~-~~~_(~i~~a_n~)_ _ _ _ _ _ _ _ _ _ _ µ_g~L-____ !~:~ _____ 1~.9 __ 5.81 -19 .1 Acceptable EPA 608 ----------------------------------------- _ ~~49 _ ~I_P~~-~~l~r_?~ri_e_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µ_g~L-_____ ~ _____ ~~3_9 __ 3.73-11 .1 Acceptable EPA608 ------· -----• --------- ------------------ ---- -~~4~ -9~~r_:i~-S:!J~o~d!~E:. -------------µ_g~L------~ -----! ~23 ---~-~~-:. ~-~8. -----------_A~~_P!a_b~e------~PA_ ~0_8 _ 0049 4 ,4'-DDD µg /L 8.1 8.37 3.06 -11.9 4.53 -10.4 Acceptable EPA 608 -------------------------------------------------------------------------------------------- 0050 4.4'-DDE µg /L 6 .2 5.21 2.30 -6 .79 3.05 -6 .04 Check for Error EPA 608 ------------------------------------------------------------------------------------------- 0051 4.4'-DDT µg /L 4.7 3.87 1.45 -5.57 2 .14 -4.89 Acceptable EPA 608 ------------------------------------------------------------------------------------------ 0048 Dieldrin µg /L 9.3 8.67 4.25 -11.8 5.51 -10.5 Acceptable EPA 608 ----------------··--------------------------------------------------------------------------- 7540 Endrin µg /L 4 .7 3.82 1.46 -5.80 Acceptable EPA 608 ------------------------------------------------------------------------------------------ 7530 Endrin aldehyde µg /L 6.9 6 .69 1.83 -10 .3 Acceptable EPA 608 -------------------------------------------------------------------------------------------- 7535 Endrin ketone µg/L 5 .6 5 .75 3.16 -8 .34 Acceptable EPA 608 ------------------------------------------------------------------------------------------- 751 O Endosulfan I µg /L 4.7 6 .92 1.85 -9 .85 Acceptable EPA 608 ------------------------------------------------------------------------------------------ 7515 Endosulfan II µg /L 12.4 13 .1 4.03 -17.4 Acceptable EPA 608 -------------------------------------------------------------------·------------------------ 7520 Endosulfan sulfate µg /L 10 .6 10.2 -----------------------------~<!_53 _ H~et~~h~o_r _______________ _ µg/L 3.4 2 .62 --------------------- 0078 Heptachlor epoxide (beta) µg/L 1.2 2 .41 ---------------------------- 7810 Methoxychlor µg /L 5.5 4.68 Chlordane 005 3 Chlordane , technical µg /L 20 20.4 Toxaphene 8250 Toxaphene µg /L 18.9 39 .0 All ana lytes are in cl uded in ERA's A2l..A accred itation. Lab Code: 1539-01 Page 22 of 26 3.85 -14 .9 Acceptable EPA 608 ------------------------------------------ 0.853 -3.65 1.32 -3.18 Check for Error EPA 608 1.14-3.44 1.16 -7 .58 7.66 -29.4 3.90 -70 .6 1.53 -3.06 Check for Error Acceptable 11 .3-25.8 Acceptable Acceptable EPA 608 EPA 608 EPA 608 EPA 608 '"\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Base/Neutrals 5500 Acenaphthene ---------------------------- 5505 Acenaphthylene ---------------------------- 5545 Aniline WP-138 Final Complete Report EPAID: ERA Laboratory Code: TX01484 A1160-01 Report Issued: Study Dates: 09/21/06 07/17/06 -08/31/06 Un its Reported Assigned Acceptance Warning Limits Performance Evaluation Method Description Value Value Limits µg /L 34 .8 49 .8 20 .7 -60 .6 Acceptable EPA 625 ----------------------------------------------------------------µg /L 25 .2 31 .3 11 .7-39.7 Acceptable EPA 625 --------------------------------µg /L 0 .00 µg /L <5 0.00 Acceptable EPA 625 --------------------------------------------------------------------------------------------5555 Anthracene µg /L 28.2 38.2 5595 Benzidine ---------------------------- -~~7_!i _ B~f!z_oiaJ~n!h!~c_e~: _________ _ 5585 Benzo(b)fluoranthene µg/L < 25 0.00 16.6 -49 .2 µg/L 60.4 79 .7 36 .1 -101 ---------------------· --------- µg /L 29 .7 41 .9 14 .7 -57.5 ___________ A_c~_p!a_b~e ______ ~~"'._ ~2_5 ___ _ ___________ A_c~e_p!a_b~e-_____ ~~ "'._ ~2_5 ___ _ Acceptable EPA 625 --------------------------------- ---------------------------------------------------------- -5600 _ Benzo(k)fluoranthene _________ . __ ~g~L-____ ~1_-~ ____ ~~-~ __ . _ ! O_: ~ :_ ~8~~ _ ___________ A_c~_p!a_b~e ______ ~~ "'._ ~2_5 ___ _ Acceptable EPA 625 --------------------------------5590 Benzo(g ,h,i)perylene --------------------------- _ 5580 _ Benzo(a)pyrene ____________ _ µg/L 16 .6 24.4 4.90 -36 .8 ------------------------------- µg /L < 5 0.00 Acceptable EPA 625 ----------------------------- Acceptable EPA 625 _ ~~3_9 _ ~~'22Y ~ a~~o~~I -________________ ~g~L-_____ <_5 _____ _9 ~0_9 __ ---------------------------- Acceptable EPA 625 -----------------------------------------5660 4-Bromophenyl-phenylether ----------------------------- -~~70 __ Butyl~~ri_zyl_p~t~~lat: _________ _ 5680 Carbazole µg /L µg /L µg /L <5 <5 <5 0 .00 0.00 0 .00 Acceptable EPA 625 -------------------------------- Acceptable EPA 625 -------------------------------- ----- ---· - ------ --------- --- ------- - - ----- - ---- -- - ---___________ A_c~e_p!a_b~e-_____ ~~"'._ ~2_5 ___ _ --------------------------------------------------------------0.00 µg /L <5 Acceptable EPA 625 5745 4-Chloroaniline ---------------------------- 5760 bis(2-Chloroethoxy)methane ---------------------------- -~~6_!i _ ~i:>t2:~h~o!~e_t~YD~t~i:r ________ _ __ ~g~L-____ ~~-~ _____ 1 _J 1 _ _ _ _ ~~-! : ! ~5-_ _ __________ A_c~_p!a_b~e-_____ ~~ "'._ ~2_5 ___ _ µg/L 11 O 171 45.0 -206 Acceptable EPA 625 _ ~~8_9 _ ~i~t2:~h~o!~i~o_p!o_pylle!~e! _________ ~g~L-_____ <_5 _____ .9 ~09 ________________________ A_c~e_p~a_b~e-_____ ~P"'._ 62_5_ _ _ 5790 1-Chloronaphthalene ---------------------· ------------------------------------------ µg/L 0.00 ---------------------------- 5795 2-Chloronaphthalene ----------------------------µg/L 95 .9 146 45.0 -176 Acceptable EPA 625 ---------------------· -------------------------------------------5825 _ 4-Chlorophenyl-phenylether ____ _ µg/L 72.5 97.5 36 .6 -122 Acceptable EPA 625 ---------------------5855 Chrysene µg /L 60.9 79 .7 ------------------------------------------------- -~~9_!i _ !)!b~~~(~.~)_a~t~~a_ci:n_e ____________ ~g~L-_____ <_5 _____ .9~09 __ 5905 Dibenzofuran µg/L 58.4 82.8 ----------------------------· --------------------- µg/L 76.8 100 µg/L µg /L <5 <5 0.00 0.00 31.6-104 29.3 -104 32 .8 -131 Acceptable EPA 625 -------------------------------- -__________ A_c~_p!a_b~e-_ _ _ _ ~~"'._ ~2_5 _ _ _ Acceptable EPA 625 - --· ---- - - --- - - --------- ----· ----- Acceptable EPA 625 -------------------------------- -__________ A_c~e_p!a_b~e ______ ~~ "'._ ~2_5 ___ _ Acceptable EPA 625 -------------------------------- 4610 1,2-Dichlorobenzene 4615 1,3-D ichlorobenzene 4620 1,4-Dich lorobenzene 5945 3 ,3'-Dichlorobenzidine µg/L 35 .4 87 .2 8.72 -105 Acceptable EPA 625 ------ ---- - - - ---- --- -. - ------ - ----- -.. -· --------------- ----------- ---------------------------- -~C?_7_9 _ !)!e~h_yp~~h~I~~ ____________ _ 6135 Dimethylphthalate ----------------------------6185 2 ,4-Dinitrotoluene µg/L < 10 0.00 --------------------- µg/L 108 141 --------------------- µg/L 87 .2 124 --------------------- µg/L 90 109 Acceptable EPA 625 ---------------------------------------- 26.6 -191 Acceptable EPA 625 --------·----- ------ ---- - ----- ----- - ------ - 12.4 -179 Acceptable EPA 625 ----------------------------------------- 40 .6 -135 Acceptable EPA 625 6190 2 ,6-Dinitrotoluene µg/L 129 169 ------------------------------------------------- -~~0_9 _ !)~-~-9~t~le~t~~l~t: ___________ . __ ~g~L-____ ~~-! _____ 1~ ! __ 71 .1 -211 --------- 27 .7 -207 -------------·-·------------------------- Acceptable EPA 625 ------------------------------- Acceptable EPA 625 µg/L 48.3 62.2 _ ~~5_!i _ ~i:>~2:~t~y~~e~~l)_p~t~~l~t: _ _ _ _ _ _ _ _ _ ~g~L-____ ~~-! _____ 1~~ ____ ~~-~: ! ~1 -_ 6265 Fluoranthene 28 .2 -77.4 Acceptable EPA 625 -------------------------------- Acceptable EPA 625 ··--------------- All analytes are included in ERA's A2LA accreditat ion . Lab Code : 1539-01 Page 23 of 26 I I,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® WP-138 Final Complete Report Tamara Welch EPAID: TX01484 A1160-01 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr ERA Laboratory Code: Report Issued: 09/21/06 07/17/06 -08/31/06 Study Dates: Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Units Reported Assigned Acceptance Warning Limits Performance Method Value Value Limits Evaluation Description Base/Neutrals (Cont.) 6270 Fluorene µg/L 123.0 157 70.0 -183 Acceptable EPA 625 ------------------------------ 6275 Hexachlorobenzene µg/L 58 .2 84.6 36.6 -104 4835 Hexachlorobutadiene µg/L 49 .3 111 ---------------------_ ~~.~ = !~2-______________ A_c~e_P!a_b~e _ _ _ _ EPA 625 6285 He xachlo rocyclopentadiene µg/L < 5 0.00 Acceptable EPA 625 ------------------------------------------------------------------------------------------ - 4840 Hexachloroethane µg /L 26.9 65 .5 6315 lndeno(1 ,2,3-cd}pyrene µg/L 30.5 44 .5 -------------------------------------------------- 6320 lsophorone µg/L < 5 0.00 -------------------------------------------------6385 2-Methylnaphthalene µg/L 33 .9 57 .8 -------------------------------------------------5005 Naphthalene µg/L 75.4 127 -------------------------------------------------6460 2-Nitroaniline µg/L < 5 0.00 6465 3-Nitroaniline 6470 4-Nitroaniline 5015 Nitrobenzene ---------------------------- 6525 N-Nitrosodiethylamine ---------------------------- µg/L µg/L <5 <5 0.00 0.00 µg/L 82.8 116 ---------------------µg/L < 5 0 .00 _ 6530 _ N-Nitrosodimethylamine ___________ 1:_g~L-____ ~~ ! _____ 1_9! __ 6535 N-Nitrosodiphenylamine ----------------------------6545 N-Nitroso-di-n-propylamine ---------------------------- 6590 Pentachlorobenzene 6615 Phenanthrene ---------------------------- 6665 Pyrene ---- -- --------------------· -- 5095 Pyridine ---------------------------- 6715 1,2 ,4 ,5-Tetrachlorobenzene 5155 1,2 ,4-Trichlorobenzene µg/L <5 0.00 µg/L < 5 0.00 --------------------- µg /L < 5 0.00 µg/L <5 0.00 µg/L 37 .1 45 .4 --------------------- µg/L < 5 0.00 µg /L µg /L <5 63.5 0.00 120 All analytes are included in ERA's A2LA accreditation . Lab Code: 1539-01 Page 24 of 26 _ ~.~~-:_ ~8~~ _ _ __________ A~~_P!a_b~e-_____ ~~A_ ~2_5 ___ _ 9.40 -60.9 Acceptable EPA 625 ------------------------------------------ Acceptable EPA 625 ------------------------------------------ _ ~.~~-:_ ~2~~ _ _ __________ A~~_P!a_b~e ______ ~~A_ ~2_5 ___ _ _ ~~. ! = ! ~o ______________ A~~_P!a_b~e-_____ ~~A_ ~2_5 ___ _ Acceptable EPA 625 ---------------------------------------- Acceptable EPA 625 -------------------------------- __________ f~~_P!a_b~e-_____ ~~A_ ~2_5 ___ _ 36.1-141 Acceptable EPA 625 -------------------------------- __________ f ~~e_P!a_b~e-_____ ~~A_ ~2_5 ___ _ 10.1 -120 Acceptable EPA 625 -------------------------------- Acceptable EPA 625 _ _ _ _ _ _ _ _ _ _ __________ A~~_P!a_b~e ______ ~~~ ~2_5 ___ _ Acceptable EPA 625 ------------------------------------------ Acceptable EPA 625 ----------------------------------------- 14.8 -65 .0 Acceptable EPA 625 ----------------------------------------- Acceptable EPA 625 ----------------------------------------- Acceptable EPA 625 ---------------------- - -------------· ---· -- - 26 .8 -142 Acceptable EPA 625 I I,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® WP-138 Final Complete Report Tamara Welch EPAID: TX01484 A1160-01 09/21/06 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr ERA Laboratory Code: Report Issued: Study Dates: 07/17/06 -08/31/06 Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. Units Reported Assigned Acceptance Warning Limits Performance Evaluation Method Description Value Value Limits Acids 5610 Benzoic acid µg/L < 50 0.00 Acceptable EPA 625 -------------------------------------------------------------------------------------------5700 4-Chloro-3-methylphenol µg/L 79.7 107 41.5 -138 Acceptable EPA 625 -------------------------------------------------------------------------------------------- 5800 2-Chlorophenol µg/L 60 .6 93 .8 27.6 -118 Acceptable EPA 625 ------------------------------------------------------------------------------------------ 6000 2 .4-Dichlorophenol µg/L 38 .9 55 .8 16 .7 -72 .1 Acceptable EPA 625 ------------------------------------------------------------------------------------------- 6005 2 .6-Dichlorophenol µg /L 105 35.4 -132 ------------------------------------------------------------------------------------· ------ 14.1 -96.3 Acceptable EPA 625 -----------------------------------------~1_3? _ 2 ~4:C?_i~:t~~l~h_e:1~1 -_ _ _ _ _ _ _ _ _ _ _ _ 1:9:L _____ ~q_-~ _____ 7~-! __ 6360 4,6-Dinitro-2-methylphenol µg/L 117 128 43 .5 -181 Acceptable EPA 625 ----------------------------------------------------------------------------------------- 6175 2 ,4-Dinitrophenol µg/L 117 144 14.4 -197 Acceptable EPA 625 ------------------------------------------------------------------------------------------ -~"..O? _ ~:_~e_t~Y~P~:ri_o~ ________________ i:9:L _____ ?3_-1_ _____ 1?? ____ ~~-~: 1_ 3_2 ______________ A~~_P!a_b~e-_____ ~f"._~ ~2_5 ___ _ 641 O 4-Methylphenol ---.. - --·-- ------------ - - - - - -- 6490 2-Nitrophenol --------- -------------------- -~~O? -~:N~t~O_P~E:_n_o~ --- --- - --- --- - 6605 Pentachlorophenol ---------------------------- 6625 Phenol µg/L 35.7 54 .5 --------------------- µg /L 92.6 125 µg/L µg/L 32.2 75 .6 106 106 µg/L 48.1 145 -------------------------------------------------- 6735 2 ,3 ,4 ,6-Tetrachlorophenol ----------------------------6835 2 ,4 ,5-Trichlorophenol ---------------------------- 6840 2 ,4.6-Trichlorophenol µg/L 35 .5 45 .2 µg/L µg/L 45 .6 60.4 74 .3 87 .3 All analytes are included in ERA's A2LA accreditation. Lab Code : 1539-01 Page 25 of 26 5.45 -73 .0 Acceptable EPA 625 ----------------------------------------- 29.8 -163 Acceptable EPA 625 ------------------------------------------ 10 .6-144 27 .2 -147 __________ Acceptable _____ ~f"..~ ~2_5 ___ _ Acceptable EPA 625 -------------------------------- 14 .5-194 Acceptable EPA 625 ------------------------------------------4.52 -61.5 27.5 -97 .2 27 .9-111 Acceptable EPA 625 Acceptable EPA 625 -------------------------------- Acceptable EPA 625 ~,,~ ENVIRONMENTAL V/lliJ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 Anal. Analyte No. BTEX & MTBE in Water 4375 Benzene 5000 tert-Butyl methyl ether (MTBE) ---------------------------- 5140 Toluene 5260 Xylenes , tota l WP-138 Final Complete Report EPAID: TX01484 ERA Laboratory Code: A 1160-01 Report Issued: 09/21/06 Study Dates: 07/17/06 -08/31/06 Units Reported Assigned Acceptance Warning Performance Method Value Value Limits Limits Evaluation Description µg/L µg/L 38 68.6 33.2 55 .3 µg/L 46.8 45 .3 --------------------- µg/L 22 .5 22 .1 µg/L 77.0 73 .6 23 .4 -42 .8 34 .8 -78.0 31.1-57.8 15.4 -28.3 41 .7-100 Acceptable EPA 602 --------- - - -- -·-- --- ---- - - ------- Acceptable EPA 602 -------------------------------- __________ Acceptable _____ ~~"'._ ~0_2 ___ _ Acceptable EPA 602 -------------------------------- Acceptable EPA 602 All analytes are included in ERA 's A2LA accreditation . Lab Code: 1539-01 Page 26 of 26 Tamara Welch Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 SOIL-58 Soil Study Open Date: 04/23/07 Close Date: 06/07/07 Report Issued Date: 06/28/07 Final Report June 28 , 2007 Tamara Welch Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 Enclosed is your final report for ERA's Soil Proficiency Testing (PT) Study , SOIL-58 . Your final report includes an evaluation of all results submitted by your laboratory to ERA. Data Evaluation Protocols : ERA's SOIL-58 PT standards contain every analyte included in every state and national PT program . If the analyte is included in the National Environmental Laboratory Accred itation Conference (NELAC) PT Field of Testing list (June , 2000), the evaluation was completed by comparing the reported result to the acceptance limits generated using the criteria contained in the NELAC standards. If the analyte is not included in the NELAC Fie lds of Testing list, the reported result has been evaluated using the procedures outlined in ERA's Standard Operating Procedure for the Generation of Performance Acceptance Limits (SOP 0260). Corrective Action Help : As part of your accreditation(s), you may be required to identify the root cause of any "Not Acceptable" results , implement the necessary corrective actions, and then satisfy your PT requirements by participating in a Supplemental (QuiK™ Response) or future ERA PT study . ERA's technical staff is available to help your laboratory resolve any technical issues that may be impairing your PT performance and possibly affecting your routine data quality. Our laboratory and technical staff have well over three hundred years of collect ive experience in performing the full range of environmental analyses . As part of our technical support , ERA offers QC samples t hat can be helpful in help ing you work through your technical issues . Thank you for your participation in ERA's Soil Proficiency Testing Study , SOIL-58 . If you have any questions , please contact Shawn Kassner , Proficiency Testing Manager, or Curtis Wood , Quality Assurance Director , at 1-800-372-0122 . Sincerely , Shawn Kassner Proficiency Testing Manager attachments smk 6000 West 54th Av e., Arvada , CO 80002 Curtis J. Wood Quality Assurance Director 800-372 -0 122 fa x (303 ) 421-0159 www.eraq c.co m Report Recipient Contact/Phone Number Reporting Type Arkansas Jane Hurley/ 501-682-0938 All Analytes Florida Steve Arms/ 904-791-1599 All Analytes Kansas Jack McKenzie / 785-296-1639 All Analytes Louisiana Karen Varnado/ 225-219-9800 All Analytes Oklahoma David Caldwell/ 405-702-1024 All Analytes Texas Max Phillips/ 512-239-3518 All Analytes Utah Lorna Ward/ 801-584-8469 All Analytes SOIL-58 Definitions & Study Discussion Study Dates: 04/23/07 -06/07/07 SOIL Study Definitions The Reported Value is the value that the laboratory reported to ERA. The ERA assigned value for the Organic Proficiency Testing Standards is equal to 100% of the parameter present in the standard as determined by gravimetric and/or volumetric measurements made during standard preparation as applicable . The ERA assigned value for the Inorganic Proficiency Testing Standards, with the exception of the TCLP Metals in Soil , is equal to the maximum amount of the parameter available in the standard by applicable EPA methodologies. The ERA assigned value for the TCLP metals is equal to the mean of ERA's internal analytical analyses. All NELAC parameters not added to a standard are given an assigned Value of "O", per the guidance issued by the NELAC Board of Directors , on December 14 , 2000. Non-NELAC parameters not added to a standard may be given an assigned value of less than a minimum verified concentration as determined in the background soil for applicable EPA methodologies . The acceptance limits are established per the NELAC PT program criteria or ERA's SOP for the Generation of Performance Acceptance Limits r M as applicable . The Performance Evaluation : Acceptable = Reported Value falls within the Acceptance Limits . Not Acceptable = Reported Value falls outside the Acceptance Limits . No Evaluation = Reported Value cannot be evaluated . Not Reported = No Value reported . The Method Description is the method the laboratory reported to ERA . Report Issued: 06/28/07 SOIL Study Discussion ERA's Proficiency Testing (PT) Soil study, SOIL-58 , has been reviewed by ERA Senior Management and certified compliant with the requirements of the National Environmental Laboratory Accreditation Conference (NELAC), Proficiency Testing Program Standards , Chapter 2 , July 2003 . Per the requirements of the NELAC Proficiency Testing Program , a full review of all homogeneity, stability , and accuracy verification data was completed. All analytical verification data for all analytes in the SOIL-58 study standards met the acceptance criteria contained in the NELAC Proficiency Testing Program Standards, Chapter 2 , July 2003 . If the analyte is included in the NELAC Fields of Testing list the acceptance limits were calculated based on the NELAC Profic iency Testing Program Standards , Chapter 2 , July 2003 . If the analyte is not included in the NELAC Fields of Testing list , the acceptance limits were calculated using the procedures outlined in ERA's Standard Operating Procedure for the Generation of Performance Acceptance Limits (SOP 0260 , Rev . 2 .0). The data submitted by participating laboratories was also examined for study anomalies. There were no anomalies observed during the statistical review of the data. ERA's SOIL-58 Proficiency Testing Soil study reports shall not be reproduced except in its entirety and not without the permission of the participating laboratory. The report must not be used by the participating laboratories to claim product endorsement any agency of the U. S. government. If you have any questions regarding ERA's SO IL Proficiency Testing program, please contact Shawn Kassner , Proficiency Testing Manager, or Curtis Wood, Quality Assurance Director, at 1-800-372-0122. Study: SOIL-58 ERA Laboratory Code: A116001 Laboratory Name: Accutest Gulf Coast Page1 of10 Tamara Welch Qua lity Ass urance Office r Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 ANna l. Ana lyte o . Me tals in Soil 1000 Alumin um M -~ <' V , .. .. -.. -,-V > -•• ----V --- 1005 A_nti~ony .. . .. -.. ,. -~ -.. .. --.. 1010 A rsenic 1015 Barium --VN, . . --.. N N • -----H -W N --•• " ¥ N H N --.,, -.,, " N N N N 1020 Beryllium 1025 Boron 1030 Cadm ium 1035 Cal c ium 1040 Chrom ium 1050 Coba lt .. . .. . ., •. . . . 1055 Copper . '. 1070 Iron .. .. 1075 Lead .... . . -.,, V -H V N N " -.,, .,, .,, .,, N -,. ,,_.,, ------- 1085 Mag nesium 1090 Mangane~e .. 1095 SOIL-58 Final Complete Report EPA ID: ERA Laboratory Code: Report Issued : TX0 1484 A116001 06/28/07 Study Dates : 04/23/07 -06/07/07 Un its Reported Ass ign ed Acce ptan ce Value Value Li mits mg/~~ 10401 .70 12100 4120 -17000 . . ... . .. V H -' y V •• . rngtkQ 87 .81 246 0 .00-246 ' .. . . .. mg/kg_ 11 0 .41 163 93.5 -17 3 .... ~ .. 9!~9 ..... 196.15 233 163 -289 -,.,, __ . __ -.,, ... . h h V, .,, V V N -H h mg/kg 95 .78 126 88 .3 -146 mg/kg 112.20 149 68 .7 · 182 mg/kg ...• ,84 .05 117 76 .7 -129 .. mg/kg 7783 .64 9880 7210 -12000 mg/kg 190.61 242 164 -273 ~g/kg_ ... 114.50 144 95 .9 -170 . . '""' '. ' . . rngt k,g_ 137 165 116-194 -. . " . .. ~-g/kg_ 16306.24 18700 10300 • 26 700 -· •• !1:gj k,g __ . 137 .63 184 121-215 N "N ~ --.,, .,, V .,, W N N N -.,, ---.,,,. NN V .. .,,, mg/kg 45 52.46 507 0 3580 -6100 mg/kg 437 .31 514 402 -618 7 .1 6 .26 3.54 -8.92 Performance Evaluation Accepta_ble Acceptable Acceptable ... ~C':_epta_bl~ Acceptable Acceptable Ac':_eptable Acceptable Acceptable Acceptable . Acceptable Accep table _ • ~~c_epta_b!e Acceptable Accepta ble .. .. Met hod Des c ripti on E PA 6010B E PA6010B E PA6010B EP A 601 0B .. ---. E PA 6010B EPA6010B EPA 601 0B EPA6010B E PA6010B EPA 6010B E PA6010B E PA6010B . E PA 6010B .. --------·- E PA6010B EPA6010B E PA6010 B .. ~i:r~~ry-... . .. ... "' ---... -"' -.. -"' . ----·-~-g/~g-.. . .. .. .. .... . . .. ---.,.,.,,., .. ~~ceptable .. . . 1100 Molybdenum 1105 Nickel 11 25 Potass ium 1140 Selenium 1150 Si lver 1155 Sodium .. 1160 Stronti um 1 165 Tha ll ium . ''. . " .. . .... . V V •• .. V •• <• 1175 Tin . .. . ' .. 1180 Titaniu m 1185 Vanadi um •• V VV ----...... " --.. "V •• 1190 Zinc 1780 lgnitability/Flashpoint mg/kg mg/kg mg/kg mg/kg mg/kg m_g/kg_ mg/kg rngtkg m_gl~g- mg/kg rngt ~g mg/kg mg/kg mg/kg "F 91.71 101 .31 4784 .3 1 .. '' 78 .07 68.41 647.26 158 .50 129.58 . ....... 84 .32 . .. 415 .15 107 .45 237 .86 82 102 Page 2 of 10 131 135 5860 106 87 .7 831 206 173 12 5 447 142 294 83 .1 < 25 .0 111 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 78 .2 -144 84 .0 -154 3810 -6800 61.3-127 52 .4 -110 548 -1050 143 -241 109 -196 ... 69.1-148 0.00 -851 87 .5-158 •• V •• 200 -360 29 .8-119 97 .8 -127 Acceptable Acceptable Acceptable Acc eptable Acceptable Acceptable Acceptable Acc_epta_ble Acc_ep!able .. Acceptable Accepta ble Acceptable Acceptable Not Reported Acceptable E PA60 10B E PA 6010B E PA60 10B EPA60108 EPA 60108 EPA 60108 E PA6010 B EPA6010B EPA6010B EPA 6010B EPA 601 08 E PA6010 B EPA 90 12A EPA 1010 Study: SOIL-58 ERA Laboratory Code: A116001 Laboratory Name: Accutest Gulf Coast Page 3 of 10 Tama ra Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713 -271-4700 An al. Analyt e No . Volatiles in Soil 4315 Acetone 4320 Acetonitrile 4325 Acrolein 4375 Benzene -.. ¥ ,, .. ., "' "' " .. - 4395 Bromodichloromethane ... 4400 Bromoform 4950 Bromomethane ... _,..,., -.. --"' ---" "· 4410 -... --.. ·---.,,_., N _, .... "' "' "' ' "' a• N - 2:~~tan?~~ (ME~) "" --"' ... . .. -" 5000 t~rt-_B_utY_I _rn_e_t~yl _ether (M:r.8.~) •. . . . . --' . ., . 4450 Ca rbon disul fide -.... "' ... ........ -----. -"'"' -"' "' "'"' ----W A"' "' -¥ ¥ -N N 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane ----, 4485 Chloroethane 4500 2-Chloroethylvinylether 4505 Chloroform -.. . . .. ... ··--.. 4960 Chloromethane 4570 1 _.2-D!br<:>mo :~-chlor.opr?~~n e (D~C P) . ... 4585 \~-!)!~r<:>i:n.?.e!h_an.e _(~!)_B) ... ----· "'"'"'"'. -.. - 4595 Di b ro momethane -.. 4610 1,2-Dichlorobenzene .. ,., ... , . .. 4615 1,3-Dic_h loro~':!nze_ne 4620 1,4-Dichlo robenzene 4625 Dichlorodifluoromethane 4630 1, 1-Dich loroethane 4635 1,2-Dichloroethane 4640 1: 1-Dichloroethylene 4645 cis-1 ,2-Dichl<:>roethylene 4700 trans-1,2-D ichloroethylene 4655 1 .. ~-D!c_h!~r<:>p~op~~~ ·--N -...... --"' -. -.. 4680 cis-1 ,3:[?i~~l<:>ropropY_le ne 4685 trans-1 ,3-D ichloropropyle ne SOIL-58 Final Complete Report EPA ID: ERA Labo ratory Code: Repo rt Is s ued : TX0 1484 A116001 06/28/07 Study Dates : 04/23/07 · 06/07 /07 Reporte d Assi gn ed Acceptance Val ue Valu e Li mits Un its µg/kg . 180 186 8.08 -310 µg/kg < 10 0 .00 µg/kg < 50 0.00 ... .JJ9!1<_9_ .• 23.1 23.3 15 .6-31 .9 ... ---.. .. ... .. µg/kg 7 1.2 71 .1 49.7 -98.7 µg/kg <5 0 .00 --.P!J!kg _ . 194 196 39 .8-330 , N N -"'"'"'' ... . ... ----.,,. N Na' .. P9!~9 174 177 53.4 -273 . . ... . . . . µg !k_g_ 118 74.4 -168 ... • y" •• ... ... ... .. . __ .JJ9!k_9_ ... < 10 0 .00 -. ,, -. -.. -· ........ ---.. --- µg/k!;j 148 138 88.4 -20 1 µg/kg 47.7 47.1 32.5-62 .1 µgik_g 37 .0 22 .2-50 .8 ,NN N . , . -.. . -· . µg/kg <5 0 .00 µg/kg 0 .00 -.. .JJ!:l!k_g,. -.. 186 175 120 -233 --.. . .. -"'' ... . . ,, -· . µg/kg <5 0 .00 µg(k g_ <5 0.00 ... .. .. -.JJJJ!kg_ ... <5 0 .00 --.. .,,. ...... -·. ""'"' ---··,' ,, -· µg/kg <5 0 .00 -. jJQik_g 76.2 77.5 47.3 -107 µg/kg <5 0 .00 - µg /kg 128 124 73 .1 -173 µg/kg <5 0 .00 µg/kg 213 190 120 -265 µg/kg <5 0.00 µg/kg 4.6 0 .00 µg/kg <5 0 .00 µg/kg 70.2 69 .3 41 .4-101 .JJ_gik_g_ 31 .8 31.2 21 .0-41 .9 ... . -·- µg!kg 62 .3 59.0 39 .9-81 .3 µg/kg 97.0 84 .1 51.7-123 Page 4 of 10 Performan ce Eva lu at io n Meth od De sc riptio n Acceptable EPA 8260 B Acceptable EPA8260B Acceptable EPA 8260B .. A,ccept~ble EPA8260B Acceptable EPA8260B Acceptable EPA 8260B .. .. A,c_cep!ab le EPA8260B ·-.. Accept~b}e EPA 8260B N<:>~ Reported . . . . _ .. A,cceptab le EPA8260B -. ·-··-·- Accepta_ble EPA 8260B Acceptable EPA 8260B r:,Jot Reported . .. ·- Acceptable EPA 8260B Not Reported Accept~ble EPA 8260B - Acceptable EPA 8260B Accep!able EPA 8260B . A,c_cep!abl~ _ EPA 8260B ·--- Acceptable EPA 8260B Acce ptable EPA 826 0B Acce_ptable EPA 8260B Acceptable EPA 8260 B Acceptable EPA 8260B Acceptable EPA8260B Acceptable EPA8260B Not Acceptab l.e EPA8260B Acceptable EPA 8260B Acceptable EPA 8260B Accep!able EPA 8260B Acceptable EPA 8260B Acceptable EPA8260B All analytes are included in ERA's A2LA accreditation . Lab Code: 1539-01 SOIL-58 Final Complete Report Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 Anal. Analyte No. Volatiles in Soil (Continued) 4765 Units . . . . E_th,:lbenz_ene . .. ... , , pg/kg_, .. 4860 2-Hexanone pg(kg . . .. . . .. . --.. . . .. . 4975 Methylene chloride µg/kg 4995 4:Methyl-2:pen1anone _(M~8 K) -_µgtk,9 _. -. -. . 5005 Naphthalene pg/kg ... 5100 Styrene µg/kg .. 5105 1, 1, 1,2-Tetrachloroethane _µ_g (kg _. -V --~-·A Y•NNN --V,Y.YN # N -, Y, -V, Y N ff N 5110 1 ! 1_,2 ,.2-Tetrachloroethane µg/kg 5115 Tetrachloroethylene µg/kg 5140 Tolu e ne --_µg(k_g_ '' N .,,.. ____ ..., y # N N --... -~ ----.. --- 5160 1, 1, 1:Tric~~orC>EJt~c1~e, _ p,9/kg_ .. .. .. ---. ... 5165 1, 1,2-Trich loroethane .. _µ_glkg ., v V v ,, y y v . • y .. ·- 5170 . T_ri?~lo:C>Elt~,:h~~El ____ . -p_g (k_g_ .. ---. ,y N N .... " -Y -Y N N , 5175 Tri chlorofluoromethane µg/kg 5180 1,2 ,3-Trichl_oropropane (TCP ) µg/kg _. 5225 Vinyl acetate •. _µ_g(kg _ -. • AA"AY·' Y. Y . . . -.. 5235 Vinyl chlo ride µg/kg 5260 Xylenes, to tal µg/kg EPAID: ERA Laboratory Code: Report Issued: TX01484 A116001 06/28/07 Study Dates: 04/23/07 -06/07 /07 Reported Assigned Acceptance Value Value Limits 95 .6 90 .8 61.4-120 . . 186 193 72 .5 -290 ·-. -. ... 74 .7 74.2 37 .6 -108 143 152 89 .5 -211 ··-.. -.. .. ... .,, . <5 0 .00 .. <5 0.00 182 164 110 -229 ,.. ff ff A . -. . ... --. 82.4 79 .8 43 .8-114 52 .3 49 .2 23 .1 -75 .6 61 .5 61 .0 39 .6 -78.7 ----., .,. y N N -A A• --y - 94 .6 94.5 60 .6 -136 ... -. 66.9 64 .2 42 .7 -89 .8 .. y" ••• 147 128 83.8 -184 --. ' ~ Y. -,, y .Y ,, ' N ~ ----NNNNA" 181 159 66 .2 -274 35 .2 57 .7 18 .0 -92.8 < 25 0 .00 . .. .. -,, . .. .. AY,V <5 0.00 215 211 137 -268 Page 5 of 10 Performance Evaluation Method Description Acceptable EPA 82608 .. Acceptable EPA 82608 Acceptable EPA 826 08 i:,~cepta_ble EPA 82608 .. Acceptable EPA 82608 Acceptable EPA 82608 i:,ce:ep)a_blE: EPA 8260B . . . Acceptable EPA 82608 Acceptable EPA 82608 Acceptab_le EPA 82608 Acceptable EPA 82608 .• i:,cc_ep!a_ble EPA 82608 __ i:,~cepta_b_lE: __ . EPA 826 08 . --- Acceptable EPA 8260 8 Acceptable EPA 82608 i:,~c_eptable EPA 8260 8 . --. Acceptable EPA 82608 Acceptable EPA 82608 All analytes are included in ERA's A2LA accreditation . Lab Code: 1539-01 @ SOIL-58 Final Complete Report Tamara Welch EPAID: ERA Laboratory Code: Report Issued : TX01484 A116001 06/28/07 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Study Dates: 04/23/07 -06/07/07 Suite 150 Houston , TX 77036 713-271-4700 Anal. Analyte No. Base/Neutrals and Acids in Soil 5500 A_ce~<_3ph t~ElnEl ., •, -0 -•• V •• V V 5505 A_c~~<.3p~t~y1~~: _ •. . . 5145 2-Amino-1-methylbenzene . (o-tol uidine) .. 5545 Aniline Units _µg(kg .. .. µg/kg_ pg/kg --' V ., N .. "" ..._ ........ -...... -................ --.. ......... _,, __ ,, ... _µ§l(k_g_ • - 5555 Anthracene µg(~g . .. --..... -. . - 5595 Benzidine µg/kg 5610 Benzoic acid µg(k_g_ . -.......... -.. -,;,v.•, .. 5575 Benzo(a)a nthracene µg /kg 5585 Benz9(b )f)u_orant_hene µg/kg 5600 B_e_n~o(k)flu_o_rant~e ~El ••.•.. __ . ' ' ' _µ§1(~9 •. . ..._ ... VA ... v ........ 5590 B_enzo(g,h ,i)pery(en~ µg!kg_ . . .. 5580 Benzo(a)pyrElne _µ§Jlk_g . 5630 13_e_n~yl_ a.1~~h_o! • _____ • _ • _ ,. ____ •••.... _ • . , .• _µ9(k9_ •• 5760 bis(2-Chloroethoxy)methane .. µg/kg .. 5765 bi~(?~Chloro:!hyl)El~h~r _ . _ ..... µg/kg_ -. . . -.. 5780 b!s_(2-_G_~l<:1r9(s9p~o_pil:~h~~ __ • .• _µ9(~9 ... . .............. ........... 5660 4-Bromophenyl:phenylethe r µg/kg 5670 Butylbenzylp_hthalate _µ9/kg 5680 Carbazole -pg/kg_ --.. .. ............ W" "' " ¥ V ,• N .. - 5745 4-Chloroan iline µg/kg 5700 4-Chloro-3-methylphenol µg/kg 5790 1-Chloronap~thalene µg(kg -~ .. 5795 2-Chloronaphthalene µg/kg 5800 2-Ch lo~o_ph_e~ol_ µ9/kg_' . ---.. 5825 4~Chloro_phenyl-i:>heny)ether µg/kg . . .. 5855 Chrysene .. µg/kg 5895 Dibenz_(a.~)anthracene . _µi;i!kg -... 5905 Dibenzofuran pg/kg_ . . .. . -...... .. 5925 Di-n-butylphthalate µg/kg 4610 1,2-Dichlorobenzene µ9/kg ... -.. ,. .. ' 4615 1,3-Dichlorobenzene µ9/kg 4620 1,4-Dichlorobenzene µg/kg Reported Ass igned Acceptance Value Value Lim its 1510 2260 830 -2490 ... 1760 2360 794 -2720 . .. 0.00 < 830 0 .00 ...... ,.. ............. ---.. ... -N -A. ' 4380 5620 1720-7110 . .. . ' " ... < 830 0 .00 < 830 0.00 , -V ,.• A ... ,. ., ....v.-... .. ........ 1350 1850 732 -2230 2 800 3520 1390 -4300 .. .. 1410 1730 676 -2120 , ............ ,. .... ... -, ~ VS, V ---. < 170 0.00 .. . 942 1190 498 -1440 ... < 170 0.00 "N N "~ 0 V ' .. ......... < 170 0 .00 1310 2600 309 -2980 1550 3140 734 -3440 ·--...... ..... .......... V ·A ........ .. 4360 5550 1870 -6990 2860 3990 1080 -5470 ... , 7920 8700 1960 -11500 ......... -.. ' . < 170 0 .0 0 6820 9290 2220 -11000 3260 762 -3850 3070 3610 907 -4800 4620 8680 859 -10200 •• •• V 2080 3010 11 30 -3550 . 999 1270 501 -1640 < 170 0 .00 3750 4480 14 10 -5080 4010 6110 1270 -8330 < 170 0 .00 , .. ,, . . .. < 170 0 .00 < 170 0 .00 Page 6 of 10 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Performance Ev aluation A cceptable Acceptable Not Reported ~cceptable Acceptab_le Acceptable A ~c_eptable Acceptable A cce.ptable -~~cep!a.blEl ... Acceptab le Acceptable Accep!able Acceptable A~ceptable ~ccep!able - Acc.eptab le Accepta_ble A~c eptab_le - Acceptable Acceptable Not Reported Acceptable Acceptable Acc_eptable Acceptab le Acceptable Acceptable Acceptable Acc_eptable .. Acceptable Acceptable Method Descript ion EPA 8270C EPA 8270C EPA8270C . . .. EPA8270C . .. EPA 8270C EPA 8270C - EPA 8270C EPA 8270C EPA 8270C . .. ,., .. EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C -. . -. .. EPA 8270C EPA 8270C EPA 8270C EPA8270C EPA 8270C EPA 8270C EPA 8270C EPA 82 70C EPA8270C EPA 8270C . EPA 8270C EPA 8270C SOIL-58 Final Complete Report Tamara Welch EPA ID : ERA Laboratory Code: Report Issued : TX01484 A 116001 06/28/07 Qual ity Assurance Officer Accutes t Gulf Coast 10165 Harwin Dr Study Dates : 04/23/07 -06/07 /07 Su ite 150 Houston , TX 77036 713-271-4700 Anal. Anal yte No . Un its Base/Neu trals and Acids in Soil (Continued) 5945 3,3'-Dichlorobenzidine µg/kg 6000 2,4-Dichlorophenol pg/kg_ , . - 6005 2,6-Dichlorophenol µg/kg 6070 D_i:t~y lp~!h_a!at: ___ • ____ --.PJi (k_g_ , -" " ... y " h " " y " A " ....... ~ N N " 6130 2:4-IJi~ethylp~e~ol µg/kg _ 6135 D imeth ylphthalate µg/kg 6175 22~-IJ!n_il_r?~~e no! ___ . -_p9(kJi . ........... y .. ---...... #NHN 6185 2,4-Dinitrotoluene µg/kg . . ' . 6190 2,6-Dinitrotoluene µg/kg , , . y.. y y •• . --. 6200 Di -:_n:oi::tylp~~hala_te _p9/kg _ --......... ,._ -. . 6255 bis(2-Ethylhexyl)phthalate µg/kg 6265 Fl uora nthene µg(kg 6270 Fluorene • P9!k_g_ •• .. ·-· .... v "" y" • ---y,-N,.• >' ---, 6275 Hexach lorobenzene µg/kg 4835 Hexachlorobutadiene µg/kg . ". 6285 H_e_x_a 7hl?ro_cy 71_op~~t_a9~e,n~. _pg (k_g_ . .. v y y -............. y -"" , - 4840 Hexachloroethane µg/kg 6315 lnd eno( ~ ,?,_3~cd)pyr_ene . µg (~g-... 'y Re ported Assi gn ed Ac ce ptan ce Valu e Valu e Li mits < 330 0.00 4 570 6750 1380-7720 , . 5010 1430 -5260 2280 3060 1020 -3780 "" = ,v .............. --··-, -.,. .. _ .... y ,.,,, .... , < 170 0.00 . 6470 8730 2140 -11000 1300 4940 0.00 -4940 NN NA .... ......... --, ..... 4 550 6060 2020 -7090 < 170 0 .00 5190 6390 1020 -9420 y" "" ---y v,, .... ·-.. - 5990 8290 1550 -11 700 , 2300 3090 1320 -3590 < 170 0.00 '""" ........... " -. ----•A•· v,-,.,. ,. ... , 1930 26 70 997 -3180 < 170 0.00 . - < 170 0.00 ... .,". ------. 377 4630 39.2 -4810 1740 2200 444 -2620 , -. 6320 l~o_p_ho!?n_e __ .. _ • µJiik_g_ .. 6220 8420 1670 -10600 -----. ---........ y ··---"" ............ ,. -, ""'. Y YN YN 6360 4 ,6-Dini tro-2 -methylphenol µg/kg < 330 0.00 6385 2-M~thy(nap htha len_e µg/kg < 170 0 .00 .. , 6400 2-Methylphe~ol µgik _g_ < 170 0.00 -- 6412 3&4-Methylphenol µg/kg 3780 8740 349 -8740 5005 Naphthalene µg/kg 724 1760 380-2000 6460 2-Nitroani line µg/kg < 170 0.00 6465 3-N itroaniline µg/kg < 170 0 .00 6470 4-Nitroaniline _pg/k~ < 170 0.00 .. , .. ••• y. 5015 Nitrobenzene µ9/kg 2970 5570 915-6270 . .. ........ ,, --. -· 6490 2-Nitrophenol µg/kg 3290 5520 1160-5740 6500 4 -t::Ji.tr_op~e~?I p9ikg 6300 9400 0.00 -11600 -.. ----............. --. ---. -. 6525 N-J\Jitro_so9iet hylamine _ µ9/k_g < 170 0 .00 6530 N-Nitrosod imethylamine µg/kg 2200 3990 388 -4320 Page 7 of 10 All analytes are included in ERA's A2LA accreditation. Lab Code : 1539-01 Pe rformance Eva luati on Acceptable Acceptab le Not Reported -Accept~b_l~ _ Acceptable Acceptab le Accept~b le Acceptable Acceptable . ~ccep!~ble Acceptable Acceptab le ~~cep!~ble Acceptable Acceptable Acc_eptable Acceptab le Acceptable . . Acce pt~b le Acceptable Acceptable Acceptable Acceptable Acceptable Acceptable Acceptab le Acceptable Acceptable Acceptable Acceptable Acceptable Acceptab le Meth od Description EPA 8270C EPA 8270C EPA 8270C -.. EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C .. - EPA 8270C EPA8270C EPA 8270C ------.. EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 82 70C EPA 8270C EPA 8270C E PA 8270C EPA 8270C E PA 8270C EPA 82 70C EPA 8270C EPA 8270C EPA 8270C E PA 8270C Tamara Welch Qua lity Assurance Office r Accutest Gulf Coast 10165 Harwin Dr Su ite 150 Houston , TX 77036 7 13-271-4700 Anal. An a lyte No. Base/Neutrals and Acids in Soil (Continued) 6535 N-Nitrosod iphe ny l~min e 6545 N-Nitroso-di-n-prop~lamine 6590 Pentachlorobe nzene 6605 P_e_ntachlo_r()J:l~E;n_o} • ...... ¥ .. y --.. -" ..... -• " -- 6615 Phenanthrene . . .,. -. .. . " 6625 Ph enol 6665 . . SOIL-58 Final Complete Report Units µg/kg_ µg/kg µg/kg p_g!k_g_ ... µg[kg_ . µg/kg EPA ID: ERA Laboratory Code: Report Issued : TX01484 A116001 06/28/07 Study Dates : 04/23/07 -06/07/07 Reported Ass ign ed Ac ceptan ce Val ue Va lue Lim its < 170 0.00 -- 5190 7530 1660 -8640 .. < 170 0 .00 3850 5390 0 .00 -5590 ,, -·• -.. ---·. --. ' y -· < 170 0 .00 7590 10700 1180 -12500 < 170 0.00 Pe rforman ce Eval uati on Acc_eptable Accep!able A cceptable __ ~cc_ep)able Acceptable . . A cceptab le Acceptable Metho d Descri pt ion EPA 8270C EPA 8270C EPA 8270C EPA8270C - EPA 8270C EPA8270C EPA 8270C P_Y!E;~e ··--¥. ---y --.... y y.-, ...... y ' -µJ;i/k_g --· .. . . 5095 Pyrid~ne µg/kg_ < 170 0.00 A cceptable EPA 8270C . ' . ~ ~ , ' . -.. ' -· .. ' -- 6715 1,2,4 ,5-Tetrach lorobenzene µg/k_g < 170 0.00 Acceptable EPA 82 70C '' • y -~ ' 6735 . 2,~·~·-6: TE:t~~c_hl°.r()J:)~e~o! ••. _p_glkg_ . 67 90 8680 1070 -10100 Acceptable EPA 82 70C .. ·• .. y .. --. ---. ' . .. 5 155 1 ,2,4-Trich lorobenzene µg/kg 1040 2550 395 -2980 Acceptable EPA 8270C ' . 6835 2,4 ,5-fochl_orophenol µg/kg 5220 7420 1490 -8620 Acceptable EPA8270C '. 6840 2,4 ,6-Trichlorophenol µg/kg 3780 4670 1170 -5220 Acceptable EPA 8270C 0 raanoc hi orme p . "d . s ., est1c1 es m 01 7025 Aldrin µg/kg 261 361 96.1-469 Acceptable EPA808 1A 7110 a!pha:~HC: __ µ_g/kg_. 185 289 46 .3 -392 Acceptable EP A 8081A --Y#a-Y . --... -... . .. .. 7115 beta-BHC µg/kg 182 306 61 .2 -404 Acceptable EPA 8081A 7105 delta-BHC µg/kg 121 178 32.7 -246 Acceptab le EPA 8081A 7120 9,3!1:n::'~·-B_H_C(~(n_d_ane l • .Pfl !k_g_ . 10 1 184 29 .9 -244 Acce_ptable EPA 8081A .. --.. ' y --------......... --. , ----' . - 7240 alph_a-Chlo~dan_e µg!kg 314 402 94 .9-538 Acc_eptab le EPA8081A . --.. 7245 ga_mrTJa-C_h lordane: µg!~9 3 5 .1 56 .1 18 .4 -71 .7 Acceptable EPA 8081A .. .... .. 7355 4,4'-DD D µ_g !k_g_ 249 342 71 .5 -500 Accep!able EPA 8081A ·---. ---~ y ---........ -........ y --.. -. . . 7360 4,4'-DDE µg/kg 252 3 16 96 .7 -434 Acceptable EPA8081A 7365 4 ,4'-DDT µg/kg 106 170 34 .0 -246 Acceptable EPA 8081A .. - 7470 Dieldrin •• .P.9 !~9 •.• 50.7 70.0 23.4 -88.2 Acc_ep!ab!e EPA8081A .. ----,. __ , ... --· ., --......... ,. ----· ...... ,.. .... ,, ,, ... -., ... , . ---. --.. 7540 Endri n µg/kg 152 219 53 .1 -317 Acceptable EPA8081A 75 30 End_rin aldehyde µg/kg 246 479 0 .00 -602 Acceptable EPA 8081A 753 5 Endrin ketone _pg t,k_g_ 313 439 35.4 -623 Acceptable EPA8081A -Y. --Y# NM . . '. . .. . . . . .. ... " . ' 7510 Endosulfan I µg/kg 72 .1 232 0 .00 -250 Acceptable EPA 8081A 7515 Endosulfan II µg/kg 126 440 0 .00-458 Acceptable EPA8081A 7520 Endosu lfa n su lfate µg/kg 277 409 24 .0 -604 Acceptable EPA 8081A . ' 7685 Heptachlor µg/kg 53 .3 75.4 16.2 -106 Acceptable EPA 8081A 7690 Heptachlorepoxide µg/kg 121 174 45 .6-230 Acceptable EPA8081A ' .. 7810 Methoxych lor µg/kg 177 214 17 .7-348 Acceptable EPA 8081A Chlordane in Soil I 7250 !chlordane, technica l µg/kg 139 204 3 1.4-306 Acceptable EPA 8081A µg/kg 236 289 3 .98 -425 Acceptable EPA 8081A Page 8 of 10 All analytes are included in ERA's A2LA accreditation . Lab C ode : 1539-01 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston , TX 77036 713-271-4700 Anal. Analyte No . Chlorinated Acid Herbicides in Soil 8505 Acifluorfen .. " -y ••• 8530 Bentazon 8540 Chloramben 8545 2 ,4-0 ... y •. N N - 8560 2,4-DB 8550 Oacthal diacid (DC PA) 8555 ' . . .. Dalapo_n ... ... . ___ # __ .... ___ -·. 8595 Dicamba -·· .. ,. .. . 8600 3,5-Dichlorobenzoic acid -. . -... .. . .. 8605 D_i~~l<_>r_P:O~ _ .. .... .... --. ,. . ---...... _ • N N .... -.... y -N N N 8620 Dinoseb . ' ··-.. ...... 7775 MCPA '. .. . . .... . . 7780 MCPP "" --NA ,.., ............... ,,. ,,,.,,,, ........ -----------· ---- 6500 4-Nitr?phenol 6605 Pen_tachlorophen_ol .. 8645 Picloram .. ·-. .. . ... . . 8655 2,4,5-T 8650 2 ,4 ,5-TP (Silvex) PCBs in Soil 8880 Aroclor 1016 8885 A ro clor 1221 .. . ---·· .. 8890 Aroclor 1232 ·----. A • "' "N • N N N .. ----.. . ---............ - 8895 Aroclor 1242 8900 Aroclor 1248 . -. ·-. •• • N 8905 Aroclor 1254 -·-. -........ --.. --....... ,,,,,..,, ..... .... .... .... Y. N N N O N .... . 8910 Aroclor 1260 Gasoline Range Organics (GRO) in Soil 9408 Gasoline Range O rgani cs (GRO) .. 4375 Benzene in GRO 4765 Ethylbenzene in GRO 5140 Toluene in GRO , .. .. . -. .. . 5260 Xylenes , total in GRO anics DRO in Soil 9369 Diesel Range Organics (ORO ) SOIL-58 Final Complete Report Units µg/kg µg/kg µg/kg • _µg !~g- µg/kg µg/kg ,. . µ~(k_g _ •. , µg/kg_ .... µg(kg _ •. JJ~!k_g_ .. µg !~g ... µg/kg ..• JJ~!k_g_ . µg/kg pg/kg _µg/~g- µg/kg µg/kg mg/kg rn_g1~g .. --• rn~/kg_ . - mg/kg mgjkg rn_g!~g ..• mg/kg mg/~g mg/kg mg/kg !1:g!kg . . mg/kg mg/kg EPA ID: ERA Laboratory Code: Report Issued: Study Dates: TX01484 A116001 06/28/07 04/23/07 · 06/07/07 Reported Assigned Acceptance Value Value Limits Performance Evaluation Method Description 776 0.00 -1100 Not Reported 690 0 .00 -1210 Not Reported 474 0.00 -624 Not Reported 37 .5 105 0.00 -197 Accep!a_ble EPA 8151A ,_ .,. --. ' ... -" .... . ,-. -. ,. . . .. 94.5 259 0 .00 -566 Acceptable EPA8151A . ' 289 46 .4 -402 Not Reported < 33 0 .00 .. _ ~~c_ep!~b!e EPA 8151A , M N N " ft • .. .. N N A" ... ft " ----·····-., .. " . . . . 40.3 265 0.00 -453 Acceptable EPA8151A 674 0 .00 -1020 Not Rep~rted . . 77 .8 323 0 .00 -520 A~c.ept~ble EPA8151A __,. ,._ . ___ ,,_ . . .. . -. . .. <7 295 0.00-400 Acceptable EPA 8151A • •• 4 < 170 0.00 Acceptable EPA 8151A < 170 0.00 Accep!~ble EPA 8151A '-------.... ..... ,.,, ,. -.. ---,. -. .. 1170 3710 0.00 -4470 Acceptable EPA8151A 2570 4930 590 -5130 Acceptable EPA 815 1A <7 605 0 .00 -869 ~ccept~ble EPA 8151A . . . .. , '" 41 .9 349 0 .00 -586 Acceptable EPA8151A 50 .3 203 0 .00 -350 Acceptabl e EPA 8151A < 0.017 0 .00 Acceptable EPA8082A . 8 .0 9 11 .9 0 .588 -17.3 ~cceptable EPA 8082A - < 0 .017 0.00 Acc_ep!able EPA 8082A . .... .... .. -.. .. . . .. . .. < 0 .017 0 .00 Acceptable EPA 8082A < 0 .017 0.00 Acceptable E PA 8082A ..... < 0 .017 0 .00 Acc_eptable EPA 8082A .......... ,, ·---,,. -.......... ·-·· -. . < 0.017 0.00 Acceptable EPA 8082A 1190 1130 9 .22 -1660 Acceptable EPA 80156 7 .10 0 .107-7.10 Not Reported 31.3 8 .21 -36.0 Not Reported 88 .2 0 .00 -95.2 Not ~epC?rt~d ... . .. .. . .. . -" " -... 126 34.2-154 Not Reported 11 10 2120 202-3150 Acceptable EPA 8015 Page 9 of 10 All analytes are included in ERA's A2LA accreditation . Lab Code : 1539-0 1 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 713-271-4700 ANnal. Analyte 0. BTEX & MTBE in Soil 4375 Benzene -. . --... . . 5000 . . -•• ¥-. . t~~-B_utyl _11:et~yl _eJ~E:_r _(MTB_~). ---., -.. - 4765 Ethylbenzene 5140 Toluene .. -------·. --~ .... ... .. 5260 Xylenes, total Texas Low-Level Fuels TPH in Soil 2050 Total Petroleum Hydrocarbons Texas Hi h-Level Fuels TPH in Soil 2050 Total Petroleum Hydrocarbons ... SOIL-58 Final Complete Report Units µg/~g-.. _!Jg[k_g_ . µg/kg EPAID: ERA Laboratory Code: Report Issued : TX01484 A116001 06/28/07 Study Dates: 04/23/07 -06/07 /07 Reported Assigned Acceptance Value Value Lim its 129 124 95.0 -160 " . " ... 69 .1 73.7 49 .8-97.2 --.. ' . 1 67 172 105-232 Performance Evaluat ion Acceptable ~cceptable Acceptable Method Description EPA 8021B EPA 8021B EPA 8021 B .• -JJJJ(k_g_ .. 95 .2 95 .8 69.2 -122 Acceptable EPA 8021B --. , .,_ .. , .. µg/kg 251 255 165 -330 Acceptable EPA8021B mg/kg 63 .6 81 .6 8.16 -1 70 Acceptable TNRCC 1005 mg/kg 3720 4530 1830 -7190 Acceptable TNRCC 1005 Page 10 of 10 All analyt_es are inclu ded in ERA's A2LA accred itation . Lab Code : 1539-01 @ l 11~ 8\MRONMENTAL ~ RESOURCE ASSOCIATES ® Study: SOIL-56 ERA Laboratory Code: A 1160-01 Laboratory Name: Accutest Gulf Coast Report Type: Complete Report Method: Method A Page 3 of 12 l it\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES 0 Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 Anal. No. Analyte Metals in Soil 1000 Aluminum -----------------------------1005 Antimony ----------------------------- SOIL-56 Final Complete Report EPA ID: ERA Laboratory Code: TX01484 A1160-01 Report Issued: Study Dates: 12/22/06 10/20/06 -12/04/06 Reported Assigned Acceptance Performance Method Units Value Value Limits Evaluation Description _ _m_g~k~ ___ 1_1 ~ ~o..:~2_! ___ 1_0~~0-__ ~8_09 : ~ ~~09 ___ A_c:e_p!a_bl_e _____ E_P_A _ 6.0J Of!. _ mg/kg 93.184 258 0.00 -286 Acceptable EPA 6010B ----------------------------------------------------- 1010 ~~s~~i~------------------------_ mg/kg ____ 2~~-~~4 ___ '}~~----!~3_-_3_5? ____ A_c:e_p!a_b~e _____ E_P_A_6_0~~E!_ __ 1015 §~r~u_m_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _m51~k~ ____ 4?~-~~5-___ 5~~ ____ ~~8---~~ _ _ _A_~~!a_b~e-_ _ _E_P_A_6_9~~E!_ __ 1020 §~ryl~~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _m51~k~ ____ ~6~9_0~ _ _ _ _5~-~ ____ 3_7J _-_6'}~5-__ A_c~_p!a_b~e-_ _ _E_P_A_6_0~~E!_ __ 1025 §~r912 ___________________________ _m_g~k~ ____ ~6~~6~ _ _ __ 1 ~ ~ ____ ~9~~ -_ ~3_5 _ _ _A~_p!a_b~e-_ _ _E_P_A_6_9~ ~E!_ __ 1030 Cadmium mg/kg 156.309 206 136 -230 Acceptable EPA 6010B --------------------------------------------------------------------------------1035 Calcium mg/kg 6675 .360 7110 5360 -9080 Acceptable EPA 601 OB -----------------------------------------------------1040 Chromium mg/kg 129 .358 155 104 -176 Acceptable EPA 6010B ------------------------------------------------------ -mg/kg ____ ~9~~0'} _ 1050 Cobalt 122 82 .9 -137 Acceptable EPA 6010B -------------------------- 1055 Copper - --- --- --- --- ----- - - - --- -·------ - - - - _ _m9~k~ ____ 1~!-~~4-___ 1~~ ___ .. ~6~~ -_ 1_6'} _ Acceptable ---------·- 1070 Iron mg/kg 15915 .627 17400 5520 -26300 Acceptable EPA 6010B EPA 6010B EPA 6010B EPA6010B -------------------------------------------------------------------------- ~ _19~5-_ ~e_a~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _mg/kg ____ ~5~0_3_? _ _ _ ?~-~ ____ 5_0:8_-_9_'.1}_ Acceptable ---------- _19~~ 'Y1~Qn_e~i~f!1 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _m51~k~ ___ ~~7_3~93! ___ ~~4.0 ___ ~~~0_-_3_!~~ Acceptable _ _ 19~0-_ 'Y1~12g_a:i~s_e _______________________ _m_g~k~-___ 3~~-~~9-___ 3~~ ____ ~~1 _-_43~ _ _ Acceptable _ _ _E_P_A_6_0~~E!_ __ _ _!'-_c~_p!a_b~e_ _ _ _E_P_A_6_0~ ~E!_ __ _ 19~5-'Y1~~c~ry _________________________ mg/kg _____ 8~~6-____ ~:¥~ ____ 4..:~6_-_13 ~2_ 1100 _ Molybdenum _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _m_g~k~ ____ ~2~0_1_'.I _ _ _ ~!-~ ____ ~7?_ -_ ~03 _ _ Acceptable ____ E_P_A_6_0~ ~E!_ __ 1105 Nickel mg/kg 138.198 173 115 -191 Acceptable EPA6010B EPA 6010B EPA 6010B --------------------------------------------------------------------------- 1125 Potass ium mg/kg 2928.407 3120 1940-4000 Acceptable ---------------------------------------------------------------------------1140 Selenium mg/kg 144.065 167 109-217 Acceptable ----------------------------------------------------- 1150 Silver _ _m51~k~-___ 1~~-~~3-___ 1~~ ____ ~7~~--1_7~-___ A_c:e_p!a_b~e _____ E_P_A_6_0~~B -_ 1155 Sodium _ _m9~k~ ___ ! ~ 3'}~2.?~ ___ ! ~6.0 ____ 8!?:] ~o_o_ _ _A_c:e_p!a_b~e -____ E_P_A_6_0~ ~E!_ __ _ _m51~k~ ____ 1~~-~~4__ ___ 1~~ ____ ~9 :1_ -_ ~7'} ___ _A_c:e_pJa_b~e _ _ _ _E_P_A_6_0~~E!_ __ 1160 Strontium - --· ------ -----· ----- -------- ------- - 1165 Thallium mg/kg 165 .254 203 129 -245 Acceptable EPA 6010B ------------------------------------------------- 1175 Tin - ---· ----- --- - - - - -- --------- ---- ---· -_ !'1iJ~k~ ____ 1 ~!-~~2-____ 1 ?~ ____ ! ~6_-_2?~ ____ A_c~e_p!a_b~e ____ E_P_A _6_0~ ~E!_ __ 1180 Titanium _ _m9~~ ____ 5~!-~~o_ _ __ 5~~ ____ !~2_-_B.O~ ____ A_c:e_p!a_b~e _____ E_P_A_6_9~~E!_ __ _ _m_g~k~ ____ 1 !~-~ ~3-___ 29~ ____ ! ~4_-_2'}~ _ _ _A_c~e_p!a_b~e-_ _ _E_P_A_6_0! ~E!_ __ 1185 Vanadium ----------------------------------1190 Zinc mg/kg 311.438 382 252-435 Acceptable EPA6010B Cyanide in Soil _1~~~ <?ta_n~d~~ t9~a~ ___________________ _ mg/kg 142.00 145 56.3 -212 __ A3~_p!a_b~e __ EPA 9012 --------------------------------·---·--- 1640 Reactive Cyanide mg/kg < 25 .0 lgnitability!Flashpoint 1780 J 1gnitability/Flashpoint OF I 98 I 112 87 .3 -125 Acceptable EPA 1010 :A.II analytes are included in ERA's A2LA accreditation . Lab Code: 1539-01 Page · 4 of 12 I /;~ ENVIRONMENTAL Vi1 RESOURCE ASSOCIATES ® SOIL-56 Final Complete Report Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr EPAID: ERA Laboratory Code: TX01484 A1160-01 Report Issued: Suite 150 Study Dates: 12/22/06 10/20/06 -12/04/06 Houston, TX 77036 Anal. No. Reported Assigned Acceptance Performance Method Analyte Units Value Value Limits Evaluation Description Volatiles in Soil EPA 8260B 4320 Acetonitrile __ µ9/k9 ____ ~ ]q.~ _ _ _ 9._o~ ___________ . __ ~~~et~~1e_ _ _ _ ~~~ ~~6_o~ 4325 Acrolein __ ~()_l~g__ ___ ~ ~~-~ _ _ _ 9._o9 _ _ _ _ _ _ _ _ _ _ _ _ Acceptable _ _ _ ~~~ ~~6_0~ -------------------------------- 4375 Benzene 4395 4400 4950 Bromodichloromethane Bromoform Bromomethane µ9/k9 21 .6 µ9/kg 26.9 --------------- µ9/k9 83 .1 --------------- µ9/k9 86 .9 --------------- ___ 4! ~ ~ __ ~:8_u!a_n9~e-(~_E_!<l _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µg/k9 ____ ~ ~q .~ _ __ 5_0~~ __ !e_rt_:-~u_t~ ~~!hyl_ e!~e~ i~~B_E) _ _ _ _ _ _ _ _ _ µg/k9 _____ <_5~0-_ 4450 Carbon disulfide µ9/k9 < 10 .0 ----------·--------------------------------------- 23 .3 13 .9-28 .1 Acceptable --------- __ ~~-~ ____ !6~ ! : ~8~5-___ ~~~et~~1e_ _ __ ~~-~ _ _ _ ~~-~: !~0-_ _ ~c-~et~~le_ _ 96.0 9.1 O -150 Acceptable --------------------------- 0.00 0.00 -- --- - - --- -~c-~et~~le_ - ----------~~:~~~e__ --9._09 --------------~c-~et~~le_ - EPA 82608 EPA 8260B ------------ EPA 82608 EPA 8260B EPA 8260B EPA 8260B EPA 8260B _ __ 1~~ ____ !~~ :_ ~6_9 _ _ _ ~c-~et~~le_ _ _ _ ~~~ ~~6_0~-__ -4~~~ .. _ ~_'.1~b_?~ !e~r~~hlo!i~: _ _ _ _ _ _ _ _ ______ ~Q_l~g-____ ] ~6_.q _ _ _ 4!?~ __ ~-h~o~o_b~~z_e ~e_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µ9/k9 _____ !6J __ ~ .J 4575 Chlorodibromomethane _ __ 1 ~~ ____ ~~-~: ~~9-_ _ ~~c:et~~le_ _ _ _ ~~~ ~~6_0~ __ _ ~ -- - -------· - - ---- ----- ---- --------- 4485 Chloroethane 4505 4960 Chloroform Chloromethane µ9/k9 108 103 63.3 -147 Acceptable -----------·-------------- µ9/k9 < 5.0 ---------------0 .00 _ Acceptable _ µ9/k9 < 25 .0 -----------------9:..09 --------------~~~et~~1e_ - __ ~()_/~9 ______ <_5~o_ _ _ _ 9._o 9 _ _ _ _ _ _ _ _ _ _ _ _ _ ~~:et~~1e_ _ --~()_/~9_ - -- -_<_5~0--- --9._o9 --------------~~c:et~~le_ - EPA 8260B EPA 82608 ------------ EPA 8260B EPA 8260B EPA 82608 ___ 4_5?~ __ 1 :_2~~i~r9~9-_3:<:!119~op~op~n_e_ (~~~~l -_ _ _ µ9/k9 _____ <_5~0-_ 0 .00 Acceptable EPA 82608 __ 4_:5~~ __ 1,2-Dibromoethane (ED8) _ _ _ _ _ _ _ _ _ _ _ _ ~!!'~9-_____ <_5~0-_ -------------------------------------- 0 .00 Acceptable EPA 8260B ---------------------------------------4595 Dibromomethane µ9/k9 < 5.0 0 .00 Acceptable EPA 8260B ---------------------------------------------------------------------------------------- 4610 1 ,2-Dichlorobenzene 4615 1 ,3-Dichlorobenzene ---------------------------------- 4620 1 ,4-Dichlorobenzene 4625 4630 4635 Dichlorodifluoromethane 1 , 1-Dichloroethane 1 ,2-Dichloroethane __ ~!!'~9-____ ~~2:q _____ 1 ~~ ____ ~!-~ = !~3-___ ~~~et~~1e_ _ µg/k9 < 5.0 0.00 Acceptable ------·------------------------------------ µ9/kg 174 .0 165 88.6-225 Acceptable ----------------------------------------- --~Q_/~9-----_<_5~0-- - -9._o~ --------------~~c:et~~le_ - µ9/k9 < 5.0 0.00 Acceptable --- --- ----------·----·-- --- - -- - - ------ ------ µ9/k9 < 5.0 0 .00 --------------------------------Acceptable -------- ___ 4~~~ __ 1 c 1.:-~i~~<?.r~e_t~y~e_n: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~Q_/~9-_____ ?-~ _ _ _ _ 9:..09 ____________ t-!_o_t ~~c_ept~~I: -_4~~~ --~i_S-:\2_:-~i~~l~r9e_t~y~e_n~ - --- - - - - - -- --µ9/kg -- - -_<_5~0-- - -9:..09 --------------~~c~et~~le_ - EPA 8260B EPA 8260B EPA 8260B ------------ EPA 8260B EPA 8260B EPA 8260B EPA 8260B EPA 8260B 0.00 Acceptable EPA 8260B -------------------------------------- - -_4_6~~ - -1 :_2~~i~h~<?.r~p!~~a~~ -- ---- - - - - - - - ---~!!'~9--- - -_<_5~0-- - -9._o~ --------------~~c:et~~l e_ - ___ 4~~~ __ ci_S :\3_:-~i~~l<?_r9er9ey~e_n: _ _ _ _ _ _ _ _ _ _ _ _ ~!!'~9-____ ]~2:q _ _ __ 1 ~~ ____ ~~-~: !~2-___ ~~~et~~le_ _ _ _ 4~~~ __ !r~~S_:-!,~-~~C~l_?~Op~optlE:n_e ____________ ~Q_i~9 _____ ]~1_:q _____ 1~~ _ _ _ ~q.~: ~!8 ____ ~c-~et~~le_ _ ___ 4_!~~ __ E!h_y~b:~Z~~e_ ____________________ ~9}~9-____ ]~5:q _ _ ___ 1~~ ____ ?~-~: ~~1 -___ ~~~et~~le_ _ 4860 _ ?:_H_e_?<~n_o~E: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _____ ~Q_/~9-____ ~ ~q -~ ____ 9._o~ ___________ _ Acceptable --------- __ 4_9'.~ __ M_e!h_y ~e~e_ ~h~<?.r~: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~Q_l~g-_____ 3!~3-____ ~~-~ ____ !6~~ -_ ~5_:6_ _ _ ~~~et~~le _ _ _ _ 49?5 __ 4:~e_t~y~-~-p~~t~n_o~: i ~I~~)_ _ _ _ _ _ _ _ _ _ ~()_/~9 ______ <_ 5_0_ _ _ _ 0.00 _ _ _ _ _ _ _ _ _ ~~ceet~ble . I analytes are included in ERA's A2LA accreditation . Lab Co de : 1539-01 Page 5 of 12 EPA 8260B EPA 8260B EPA 8260B ------------ EPA 8260B EPA 8260B EPA 8260B EPA 8260B I /,~ ENVIRONMENTAL ~ RESOURCE ASSOC1ATES e SOIL-56 Final Complete Report Tamara Welch EPAID: TX01484 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr ERA Laboratory Code: A 1160-01 Report Issued: 12/22/06 Study Dates: 10/20/06 -12/04/06 Suite 150 Houston, TX 77036 Anal. No . Reported Assigned Acceptance Performance Method Analyte Units Value Value Limits Evaluation Description Volatiles in Soil (Cont.) __ 5_1~~ __ S!Y~E:_n~ ________________________ ~!!_~9-_____ ~ ~ _____ 9·~~ ___________ _ 5105 5110 1 , 1, 1,2-Tetrachloroethane 1 , 1 ,2 ,2-Tetrachloroethane µ9/kg 79 .8 71 .6 45.0 -100 -------------------------------- µ9/kg 101.0 90.9 46 .6 -133 Acceptable --------- _ Acceptable _ Acceptable EPA 8260B EPA 8260B EPA 8260B ----------------------------------·------------------·-- ___ 5_1 '.~ __ T:~~c~l_?~O~thyl~~e-_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~9}~9-____ ~~5_.Cl_ _ _ __ 1?~ ____ ?~:~ :. ~~4-___ ~~~et~~~ _ __ 5}~~ __ T9l_u:n__e ________________________ ~!!_1~9-_____ 5_1 ~3-_ _ _ ~~.~ ____ ~9_.~-:_ ~5~5-_ _~~~et~~~_ 5160 1 , 1 , 1-Trichloroethane --------------------------------- 5165 1 , 1,2-Trichloroethane 5170 Trichloroethylene -------------------------------- 5175 Trichlorofluoromethane --------------------------------- -_5}~~ __ 1~2~3_:-~r~c~19~op~op~n__e ___________ _ _ ... _ 53~~ __ V!n_y~ a_c~~~e-________________ _ __ ~!!_!~9 _____ ~~o_.o_ _____ 1~~ ____ ~~.~ = ~~o ____ ~~~et~~1~ _ __ ~!!_!~g-_____ <_5~o. _ _ _ 9~o~ _______________ ~cc~et~~1'=-_ __ ~!!_l~g-____ ~~5_.Cl_ ____ 1~~ ____ ~~.~: !~9-__ Acceptable _ µg/kg < 5.0 --------------- µ9/kg < 5.0 µg/kg < 25 .0 --------------- 0.00 0 .00 0 .00 ---------------- _ Acceptable _ Acceptable --------- 5235 Vinyl chloride µg/k9 141 .0 120 32 .2 -234 _Acceptable _ Acceptable --------------------------------------------------------- EPA 8260B EPA 8260B EPA 8260B EPA 8260B ------------ EPA 8260B EPA 8260B ------------ EPA 8260B EPA 8260B EPA 8260B 5260 Total , Xylenes µ9/k9 196 .0 187 109-255 Acceptable EPA 8260B V :--......................................... __ ............. ___ .......................... _ ............... __ .............., ____ I Base/Neutrals & Acids in Soil 5500 Acenaphthene µ9/kg 2320 3000 1090 -3310 Acceptable EPA 8270C ------------------------------------------------------------------· ---------------------- 5505 Acenaphthylene µg/kg 2430 30 40 958 -3260 Acceptable EPA 8270C ---------------------------------------------------------------------------------·----- 5145 2-Amino-1 -methylbenzene (o-Toluidine) µg/kg 0 .00 ---- ------------ ----------------------------------------------------------- ------- -------- 5545 Aniline µg/kg < 830 0.00 Acceptable -------------------------------------------------------------------------- 5555 Anthracene µg/kg 7270 ------------------------------------------------__ ~~5_!) ____ 2_!~Cl_-:_ ~4_6~ _ _ ~~c:et~~I~ _ 5595 Benzidine µg/kg < 830 0.00 Acceptable --------------------------------------------------------------------------- 5610 Benzoic acid µ9/kg < 830 -----------------------------------------------__ 9~0~ _ _ _ _ _ _ _ _ _ _ _ _ _ ~~~et~~I~ _ __ 5_5?~ __ B~~2:_o!a)':n_t~r~~e~: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~!!_l~g-_____ 1 ?~0-_ _ _ ! ~9_!) ____ ~2_3 _-_1 ~~Cl_ _ _ ~~c~et~~I~ _ 5585 Benzo (b)fluoranthene µg/kg 6650 7040 2370 -8910 Acceptable --------------------------------------------------------------------------- 5600 Benzo(k)fluoranthene µg/kg 5220 5320 1710 -6810 Acceptable ------· --------------------------------------------------------------------- EPA 8270C ------------ EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C ------------ EPA 8270C -__ 5_:5~~ __ _8~~2:_019_.~.i)P_e_ry~e_n~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~g_l~g-____ ~ _1?Cl_ ____ 9~0~ _ _ _ _ _ _ _ _ _ _ _ _ _ ~~~et~~I~ ____ ~f:'~ ~~7_0_s: __ _ _ _ _ 5_5~~ ___ B~~z_o!a)eY!"._n~ ___________________ ~!!_1~9 ______ ~2~ _ _ _ _ ! ~ 4_!) ____ ~0~0--_ 1_2~~ ___ ~~c~et~~le __ EPA 8270C ___ 5~~~ __ B~~ZJ~ ':l~o_h~I -_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~!!_l ~g-____ : _1?Cl_ ____ 9·_?~ _ _ _ _ _ _ _ _ _ _ _ _ _ ~~~et~~I':_ _ EPA 8270C __ 5!~~ __ ?~S~2_:~~l~r~~t~o_xy)!11_e!h!1~~ ___________ ~!!_1~9-____ : _1 ?Cl_ ____ 9·_?~ _ _ _ _ _ _ _ _ _ _ _ _ ~~~et~~I~ ____ ~F:'~ ~~7_0_s: __ _ _ _ 5!~~ __ b~s t2_:-~~~r~E:_t~YD~~:r _______________ ~!!_l~g-____ ~ ~?O. _ 5780 bis(2-Chloroisopropyl)ether µg/k9 < 170 ------------------------------------------------ 0.00 0 .00 Acceptable EPA 8270C --------------------- Acceptable EPA 8270C __ 5_6~~ __ ~:B_r~n,~p_h~~y~-~~e!1yl~t~:r ____________ ~g_l~g-____ : _1?Cl_ ____ 9._09 ______________ ~~c~et~~I':_ ____ ~f:'~ ~~7_0_s: __ _ _ _ 5~?~ __ B_uo/l_b~~z_ylp~t~~l~t~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~!!_l~g-_____ 7~~0-____ ~~9_!) ___ ] ~O_O_-_1 ~~CJ_O ___ ~~c~et~~I~ _ 5680 Carbazole µg/kg < 170 0 .00 Acceptable ------------------------------------------ µg/kg < 170 0.00 Acceptable -----------------------------------------___ 5! ~~ __ 4-:_~h~o__r~a!1~i~':_ _______________ _ µg/kg 6700 9480 2160 -9540 Acceptable -------------------------------------------___ 5!9~ __ ~=~h~o__r~-~-_m_e!hJlp~"._n_o~ _________ _ 5790 1-Chloronaphthalene µg/kg 0 .00 ----------------------·----------------------------------------- I analytes are in cl uded in ERA's A2LA accreditation . Lab Code: 1539-01 Page 6 of 12 EPA 8270C EPA 8270C EPA 8270C ------------ EPA 8270C I i,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® SOIL-56 Final Complete Report Tamara Welch EPAID: TX01484 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr ERA Laboratory Code: A1160-01 12/22/06 10/20/06 -12/04/06 Report Issued: Suite 150 Study Dates: Houston, TX 77036 Anal. No. Reported Assigned Acceptance Performance Method Analyte Units Value Value Limits Evaluation Description Base/Neutrals & Acids in Soil (Cont.) __ 5!?~ __ 2~~h~o_r~n_ap~t~~':n_e _______________ ~Q_/~9-____ ~ _1?~ ____ 9·-9~ __________ _ Acceptable Acceptable EPA 8270C EPA 8270C EPA 8270C 5800 2-Ch lorophenol --------------------------------µ9/k9 566 --------------- µ9/k9 < 170 --------------- __ 5~?~ __ D~b_e!:1~(~.~~a!:l~h~a~~~e-_ _ _ _ _ _ _ _ _ _ _ _ _ µ9/k9 ____ ~ _1?~ _ 5905 Dibenzofuran µ9/k9 4380 - --- -·----- - ------ ----- - -- ------ -- - -- --------- 5925 4610 Di-n -butylphthalate 1,2-Dichlorobenzene µ9/k9 1080 --------------- µ9/k9 < 170 --------------- 1050 0 .00 0.00 5870 180-1050 1810-6650 --------- Acceptable --------- Acceptable --------- Acceptable --------- EPA 8270C EPA 8270C 1320 474 -1690 Acceptable EPA 8270C ----------------------------· ------------ -_ 9 :...0~ _ _ _ _ _ _ _ _ _ _ _ _ _ ~~~~t~~I': _ _ _ ~~~ ~~7_0~-__ 4615 1,3-Dichlorobenzene µ9/k9 1840 7860 80 .0 -8000 Acceptable Acceptable EPA 8270C EPA 8270C --------------------------------------------------------------- 4620 1,4-Dichlorobenzene µ9/k9 1350 5230 136 -5400 ----------------------------------------------------------------- -_ 5_?~~ __ .:3 c3~-':)i~~l~r9~1:_n!i~~n~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~9}~9-____ : _3~~ _ _ _ 9-_9~ _ _ _ _______ _ --------- Acceptable --------- -----------·- EPA 8270C Acceptable EPA 8270C __ 6_09~ __ 2c4~~i~h~o_r~~h~~~I -_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µ9/k9 ____ !?!O_ _ _ _ ?~19 ____ 1!?~: ~9_19 _ ---------------------- 6005 2 ,6-Dichlorophenol µ9/k9 9250 131 O -9590 --------------------------------------------------------------- -_6_?!~ __ D!e!~Y!.P~~h~l~~e _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µ9/k9 _____ 2??0_ _ _ _ ~~8_9 _ _ _ ~8_5_-_3~~~ _ Acceptable EPA 8270C ------------ __ 6_1 ~~ __ ~c4~~if!i~l_!lt1e~e_n~I -____________ _ µ9/k9 < 170 ---------------0.00 Acceptable EPA 8270C 6135 Dimethylphthalate ---------------------------------µ9/k9 7520 8670 2030 -10300 Acceptable -------------------------EPA 8270C µ9/k9 < 830 --------------- 6175 2 ,4-Dinitrophenol ---------·------------------------0.00 Acceptable EPA 8270C ---------------------------------------- 6185 2 ,4-Dinitrotoluene - -~Q_/~9_ - - --_8~~0----_1_0?~0--3~0_0_-_13?~0-Acceptable EPA 8270C 6190 2 ,6-Dinitrotoluene µ9/k9 7890 8740 2660 -10100 Acceptable Acceptable EPA 8270C ----------------------------------------------------------------6200 Di-n-octylphthalate --------------------------------3610 1020 -4780 __ µ9/k9 _____ 2~~0-_ ------------ EPA 8270C -_6J~~ __ b~s~2~~t~~~e.'.'t1)_p~~h~l~~e _________ _ 6265 Fluoranthene µ9/k9 6170 --------------- µ9/k9 8270 --------------- 7470 2090 -9230 ---------------- 8890 2790 -11200 Acceptable ----------------------EPA 8270C Acceptable ----------· ------------EPA 8270C 6270 Fluorene µ9/k9 2070 -----------------------------------------------2540 964-3080 Acceptable EPA 8270C 6275 Hexachlorobenzene µ9/k9 4530 ------------------------------------------------ -_4~~~ __ H~~~c~l_?~O_?~t~~i~~e-_______________ ~Q_/~9 ______ 19~0 __ 5440 2100 -6140 Acceptable EPA 8270C ----------------------------------------- 2590 537 -2820 Acceptable EPA 8270C --------------------------------------- 6285 Hexachlorocyclopentadiene --------------------------------µ9/k9 5190 ---------------Acceptable EPA 8270C ---------------------- 9550 260 -11700 ----------------- 4840 Hexachloroethane __ ~Q_t~9 ______ 1 ~~o __ 6820 270 -7050 Acceptable EPA 8270C µ9/k9 < 170 0 .00 Acceptable EPA 8270C --------------------------- 6320 lsophorone µ9/k9 4460 5870 1400 -6890 Acceptable ----------------------------------------------------------------------------EPA 8270C 6_3~~ __ ~:6:[)i~it_r~-?-_~e!hJI_Phi:n_o! ____________ ~Q_/~9-_____ 3~~0-_ _ _ ?~4_9 _____ ~.qo_-_7_3~~ ___ ~~c~~t~~': _ . __ ~~~ ~~7_0~-__ _ _ _ 6_3~~ __ 2~~e_t~y~n_ap~t~~li:n_e _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~9}~9 _____ : _1 ?q _ 6400 2-Methylphenol µ9/k9 1270 ___ 6~~~ __ }_&_~~~l_!ltle~e_n~I -________________ ~Q_/~9-____ : _1?~ _ ___ 5_?~~ ___ N_ap~t~~':n!l _____________________ ~Q_/~9-_____ ~9~ __ 6460 2-N itroaniline µ9/k9 < 170 -------------------------------- 6465 3-Nitroaniline µ9/k9 < 170 --------------- II analytes are included in ERA 's A2LA accreditation . Lab Code : 1539-01 Page 7 of 12 0.00 5200 0.00 0.00 -5200 Acceptable Acceptable Acceptable 1930 481 -2120 Acceptable -------------------------- 0.00 0.00 Acceptable Acceptable EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8270C 1 1, .. ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® SOIL-56 Final Complete Report Tamara Welch EPAID: ERA Laboratory Code: TX01484 A1160-01 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Report Issued: Study Dates: 12/22/06 10/20/06 -12/04/06 Houston, TX 77036 Anal. No. Reported Assigned Acceptance Performance Method Analyte Units Value Value Limits Evaluation Description Base/Neutrals & Acids in Soil (Cont.) 6470 4-Nitroaniline µ9/k9 < 170 0.00 -------------------------------- µ9/k9 < 170 0.00 -------------------------------- 5015 Nitrobenzene -------------------------------- -_6~~~ __ ~=N~t~O_P~~~O! ________________ _ µ9/k9 1910 3180 593 -3410 -------------------------------- __ 6_59~ _ _ 4=~it~O_P~~~O! _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~!!'~9-____ ~ _1 ?~ _ 0.00 0.00 __ 6_5~~ __ N~~i!_r~s_o~i~~h~l~~i!l~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µ9/k9 ____ ~ _1 ?~ _ __ 6_5~~ __ N-Nitrosodimethylamine __________ _ µ9/k9 < 170 0.00 --------------------------------- __ 6_5~~ __ N-Nitrosodiphenylamine __________ _ µ9/k9 < 170 0.00 -------------------------------- Acceptable Acceptable --------- Acceptable --------- EPA 8270C EPA 8270C EPA 8270C Acceptable EPA 8270C --------------------- Acceptable EPA 8270C ---------------------- Acceptable EPA 8270C --------------------- Acceptable EPA 8270C --------------------- Acceptable EPA 8270C ___ 6_5~~ __ N~~i!_r~s_o=d~-~-_p~o_p~l~~i!l~ _ _ _ _ _ _ _ _ _ _ _ ~!!'~9 _____ ~ _1 ?~ ____ 9 :0~ __ 6590 Pentachlorobenzene µ9/k9 < 170 0.00 --- --·--------------. ------ - ------ .. ----· -- -·---- -- --------- ---- ----- - --- --- ------ --- -- - ----· -- 6605 Pentachlorophe nol ·-------------·-----------·----- 66 15 Phenanthrene 66 2 5 Phenol µ9/k9 3040 --------------- µ9/k9 3240 ---------------- µ9/k9 8620 --------------- 4020 3550 15900 Acceptable EPA 8270C ------·--------------------------- 0 .00-4390 1460-4120 1170 -16500 Acceptable EPA 8270C ------·---·. ------------ Acceptable EPA 8270C ----------- EPA 8270C ------------__ 6_6~~ __ Py~e.':1 ~ ____________________ _ µ9/k9 8190 9190 2520 -11600 Acceptable EPA 8270C 5095 Pyridine -------------------------------------------------------- --------------------------------- _ µ9/k9 ____ ~ _1 ?~ _ _ _ 9._?g ______________ ~c-~~t~~IE: _ 6715 1 ,2,4 ,5-Tetrachlorobenzene ---------------------------------µ9/k9 < 170 --------------- 6735 2 ,3,4 ,6-Tetrachlorophenol µ9/k9 < 170 --------------- 5155 1 ,2 ,4-Trichlorobenzene µ9/k9 2930 ----------------------------------------------- -_6_8~~ __ 2~4.'.5_:-"!:r~c~l9~op~e_n9 ~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ µ9/k9 _____ 2~~0-_ 6840 2 ,4 ,6-Trichlorophenol µ9/k9 1550 Organochlorine Pesticides in Soil 0.00 0.00 5750 1170 -6010 3300 678 -3520 ----------------- 2200 514 -2390 7025 Aldrin __ ~!!'~9-_____ 9_8~9-_____ 1?~ ____ ~~.~: !~4-_ __ 7_1 ~ ~ ___ alp~~-~1::1 ~ __________________ _ µ9/k9 285 .0 391 21.9 -530 Acceptable --------- Acceptable Acceptab le --------- Acceptable --------- Acceptab le Acceptable --------- Acceptable EPA 8270C EPA 8270C ------------ EPA 8270C EPA 8270C EPA 8270C EPA 8270C EPA 8081A EPA 8081A ------------------------------------------------------7115 beta-BHC Acceptable EPA 8081A --~~/~9-- ----~2J _ -- --3~ 1 ---~~.~ = ~~9------------------------ 7105 delta-BHC µ9/k9 345 43 3 22.8 -619 -----------------------------------------------------------------Acceptable EPA 8081A -_7_1~~ __ 9~~1!1~--B~.S:i L~~d_a~E:_) ___________ _ µ9/k9 256 385 29 .1 -511 Acceptable EPA 8081A ------------------------------------------------------ 327 49 .7 -422 Acceptable EPA 8081A ___ 7!~~ __ alp~~-~~19~d_a~e-_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~!!'~9-_____ ~43 __ ---- ------------·-------- ----· . ---·----- - - --__ 7J~~ __ 9~~f!l_a-_C_h~o~d3l~~ _________________ ~!!'~9-_____ ~1 ~ __ 297 48.7 -373 A cceptable 7355 4 ,4'-DDD __ ~!!'~9-_____ 3_73 _ _ _ _ ~~! ____ ~~.~ = ~~o ____ ~c_c~~t~~IE: _ 7360 4,4'-DDE __ ~~/~9-_____ ~6~ _ _ _ _ }~q ____ ~~.~ = ~3_0 ____ ~c_c~~t~~E: _ 7365 4 ,4'-DDT __ ~~/~9-_____ ~7~ ______ 2!~ ____ ?3_·~ : ~~8-_ _ ~c_c~~t~~I E: _ 7470 Dieldrin µ9/k9 155 ---------------204 37 .1 -267 Acceptable ----·------ 751 ~ ___ E!l~o_s_u ~a_n _I _ _ __________________ ~!!'~9-_____ 9_!3 :3 ______ 29~ ____ ~·-9 ~ = ?4_5 __ Acceptable --------- ___ 7_5~~ ___ E!l~o_s_u lfa_n _ll _____________________ ~~/~9-_____ 6_0? _____ 1~~ ____ ~·}~ = !3_7 __ Acceptable -------- 7520 Endosulfan sulfate µ9/k9 316 452 47.4 -601 -------------------------------------------------------------·---------Acceptable --------- __ 7_5~~ __ E!l~r~n __________________________ ~9}~9 ______ ~5~ __ 203 12 .1 -284 Acceptable --------- __ 7_5~~ ___ E!l~r~n-a~d_e~~d_e _______________ _ µ9/k9 151 ---------------28 1 6 .80 -3 15 Acceptable -----------------·-------- II analytes are included in ERA's A2LA accreditation . Lab Code : 1539-01 Page 8 of 12 EPA 8081A EPA 80 8 1A EPA 8081A EPA 8081A EPA 8081A EPA 8081A EPA 8081A EPA 8081A EPA 8081A EPA 80 8 1A I i,\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES® SOIL-56 Final Complete Report Tamara Welch EPAID: ERA Laboratory Code: Report Issued: TX01484 A1160-01 12/22/06 Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Study Dates: 10/20/06 -12/04/06 Suite 150 Houston, TX 77036 Anal. No. Reported Assigned Acceptance Performance Method Analyte Units Value Value Limits Evaluation Description Organoch/orine Pesticides in Soil (Cont.) 75 35 Endrin ketone µg/kg 190 272 16.0 -376 --------------- 7685 Heptachlor µg/kg 187 236 22 .0 -310 ------------------------------------------------------------------ 7690 Heptachlor epoxide ----------------------------------_ ~9}~9 ______ ~2J _____ !?~ ____ ?~· ~ : ~~9-_ 7810 Methoxychlor µg/kg 157 183 19.1 -279 Chlordane in Soil 7250 Chlordane , Technical µg/kg 308 406 51 .2 -523 Toxaphene in Soil 8250 Toxaphene µg/kg 323 416 0 .00 -571 Chlorinated Acid Herbicides in Soil 8505 Acifluorfen 8530 Bentazon 8540 Chloramben µg/kg µg/kg --------------- µg/kg --------------- 2230 1030 1080 0 .00 -3810 0 .00 -1360 0.00 -1080 8545 2 ,4-D µg/kg 233 .0 479 0.00 -653 ------------------------------------------------------------------ -_ 8_5~~ --2~4=~~ --- - - ---- -- --- - - -- -- - - - -~l!_l~g-- - --~ ?~-~ - - --9 ._o~ ----- --- --- - __ 8_5~~ __ D_a~~~l _d~a~i9 J~~f:~) ___________ _ __ 8_5~~ __ D_a~ap~n-___________________ _ 8595 Dicamba 8600 3,5-Dichlorobenzoic acid -------------------------------- 8605 Dichlorprop --------------------------------- µg/kg --------------- µg/kg < 33.0 --------------- µg/kg 18 .5 --------------- --µg/kg - - - --- --- µg/kg 507 .0 --------------- 0 .00 ---------------- 0 .00 2390 763 0 .00-3540 0.00-1100 Acceptable --------- Acceptable --------- Acceptable --------- Acceptable Acceptable Acceptable EPA 8081A EPA 8081A EPA 8081A ----------·-- EPA 8081A EPA 8081A EPA 8081A Acceptable EPA 8 151A ---------· -----------·- Acceptable Acceptable EPA 8151A EPA 8151A EPA 8151A Acceptable EPA 8151A --------------------- 8620 Dinoseb __ ~l!_l~g-.. ___ !~2_:D_ ____ !~2_D ____ D_.D_O_ -_ 1_7~q ___ ~':_~~t~~I ~ _ EPA 8151A EPA 8151A 7775 MCPA __ ~l!_l~g-____ <_ ~7_D :_O_ _ _ p._o~ _ _ _ _ _ _ _ _ _ _ _ _ _ ~c-~~t~~I~ _ __ _7!~~ __ M_C_P_P_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ~g_l~g-____ <_ ~7_D :_O ____ P:...O~ ___________ _ ___ 6_59~ __ .4 :~it~o_P~~~o~ ___________________ ~l!_l ~g-____ ~0_8~._o ___ !~8_D ____ o_.o_o_-_2_3?q _ 8645 Picloram -------· ------------------------- 8655 2 ,4 ,5-T 8650 2 ,4 ,5-TP (Silvex) PCBs in Soil µg/kg 111 .0 --------------- µg/kg 90 .10 238 152 0.00 -380 0 .00 -255 Acceptable EPA 8151A --------------------- Acceptable EPA 8151A Acceptable --------- Acceptable EPA 8151A EPA 8151A EPA 8151A 8880 Aroclor 1016 mg/kg < 0.017 0 .00 Acceptable EPA 808 2A EPA 8082A ------------------------------------------------ 8885 Aroclor 1221 mg/kg < 0 .017 0 .00 ----------------------------------------------- -__ 8~~~ __ A~o_c~o~ !~3_? _____________________ ~9_1~11_ ____ !·_1~o_ ____ ~-!~ ___ p._o~~5_-_4~o_o_ 8895 Aroclor 1242 mg/kg < 0 .017 --------------- 8900 Aroclor 1248 mg/kg < 0 .017 --------------- 8905 Aroclor 1254 mg/kg < 0 .017 --------------- II analytes are includ ed in ERA's A2LA accreditation . Lab Code : 1539-01 Page 9 of 12 0 .00 0.00 0 .00 Acceptable Acceptable EPA 8082A --------------------- -~c-~~t~~I~ _. __ ~~~ ~D_8_2~-__ Acceptable Acceptable -------- EPA 8082A EPA 8082A ,1,~ ENVIRONMENTAL Vi1 RESOURCE ASSOCIATES ® SOIL-56 Final Complete Report Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 Anal. No. Analyte PCBs in Soil (Cont.) 8910 Aroclor 1260 --- Units mg/kg -- Gasoline Range Organics (GRO) in Soil 9408 Gasoline Range Organics (GRO) mg/kg ------------------------------------------ 4375 Benzene in GRO mg/kg ----------·------------------------------- 4765 Ethylbenzene in GRO mg/kg ~----------------------------------------- 5140 Toluene in GRO mg/kg ----------------------------------------- 5260 Xylenes , total in GRO mg/kg -- - --- Diesel Range Organics (DRO) in Soil 9369 Diesel Range Organics (ORO) mg/kg - BTEX & MTBE in Soil 4375 Benzene µg/kg ---------------------------------------- 5000 tert-Butyl methyl ether (MTBE) _______ µg/kg ---------------- 4765 Ethylbenzene µg/kg ------------------------------------------ 5 140 Toluene --~Q_l~g------------------ --- --- --· ------- ---- - 5260 Xylenes , total µg/kg -------------------- Texas Low-Level Fuels (TPH) in Soil 2050 Total Petroleum Hydrocarbons mg/kg ----- Texas High-Level Fuels (TPH) in Soil 2050 Total Petroleum Hydrocarbons mg/kg - II analyte s are in cl uded in ERA's A2LA accred itation . Lab Code : 1539-01 EPA ID: TX01484 ERA Laboratory Code: A1160-01 Report Issued: 12/22/06 Study Dates: 10/20/06 -12/04/06 Reported Assigned Acceptance Performance Method Value Value Limits Evaluation Description < 0.017 0.00 Acceptable EPA 8082A ----- ---- 872 781 0.00-1280 Acceptable EPA 8015 ---------------------------------------------- 4 .90 0.00-7 .54 --------------------------------------------- 21 .6 4.84-32.0 ------------------------------- ------------- 61.0 0.00-79 .2 ---------------------------------------------- 87.0 24.5 -127 ------------- --- 4620 3840 612 -5570 Acceptable EPA 8015 --- 165 147 86.4 -196 Acceptable EPA 80218 ---------------------------------------------- 136 116 57 .6 -176 Acceptable EPA 80218 --------------------------------------------- 88.5 72 .5 44 .5 -108 Acceptable EPA 80219 -------------------------------------------- 32 .8 27 .6 16 .3 -40.3 Acceptable EPA 80218 -----------·----------------------· ------------ 419 352 272 -440 Acceptable EPA 80219 ------ 84 .3 90.7 0.00 -190 Acceptable TNRCC 1005 6190 6790 2750 -10800 Acceptable TNRCC 1005 Page 10 of 12 ,/;~ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Study: SOIL-56 ERA Laboratory Code: A 1160-01 Laboratory Name: Accutest Gulf Coast Report Type: Complete Report Method: Method B Page 11 of 12 I I!\ ENVIRONMENTAL ~ RESOURCE ASSOCIATES ® Tamara Welch Quality Assurance Officer Accutest Gulf Coast 10165 Harwin Dr Suite 150 Houston, TX 77036 Anal. No. Analyte Cyanide in Soil 1635 Units mg/kg SOIL-56 Final Complete Report EPAID: ERA Laboratory Code: TX01484 A1160-01 12/22/06 Report Issued: Study Dates: 10/20/06 -12/04/06 Reported Assigned Acceptance Performance Method Value Value Limits Evaluation Description 142 145 56 .3 -212 Acceptable EPA 335 .3 - - --s;~a_n~d~c l:>l_a ~ ____________________ ---------------------------------------------------1640 Reactive Cyanide mg/kg < 25 .0 All analytes are included in ERA 's A2LA accreditation . Lab Code : 1539-01 Page 12 of 12 Method :CV AA Instrument: Leeman2-hot block digestion Analyst: Analyte Name Date Mercury Sample ID Cone 1/4/2006 T12246 0.20 7470A Analvte Name Date Sample ID Cone Mercury 7471 4/5/2006 T12482 0 .03 Analyte Name Date Sample ID Cone Hg IDL 1/5/2006 T12244 0 .00 ~nalyte Name Date Sample ID Cone 0 Hg LR 1/512006 LRA 0 .18 Accutest Laboratories -Houston Method Detection Limit Determination ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 ug/1 0.1320 0 .2180 0.1870 0.1890 0.1300 0.1180 0.1120 mg/ka mg/kg ma/kg mg/kg ma/kg mg/ka malka 0.0216 0.0208 0.0204 0 .0249 0.0252 0.0183 0.0207 uo/1 uo/1 uo/1 uq/1 ug/1 ug/1 ug/1 -0 .0260 0.0230 0.0140 -0 .0010 -0.0270 -0 .0010 ##### Cone Cone Cone Cone Cone t;orrelation Coe 0.2 0 .5 1 5 10 0.97 3.00 4 .92 5.75 9 .54 0.914820701 Matrix: Water/Soil X-Bar Std Dev MDL Spike/MDL Mean/MDL Verification ua/1 ug/1 ua/1 Ratio Ratio ug/1 0 .1551 0.0419 0 .1316 1.5 1.2 0.164 X-Bar Std Dev MDL Spike/MDL Mean/MDL Verification mo/ko mg/kg mg/kg Ratio Ratio mg/kg 0.0217 0.0025 0 .0079 4 .2 2.8 0.0308 Calculated IDL ug/1 ug/1 ug/1 -0 .0040 0 .0000 -0 .0040 0.048501546